#------------------------------------------------------------------------------
#$Date: 2018-01-23 18:47:37 +0200 (Tue, 23 Jan 2018) $
#$Revision: 362 $
#$URL: svn://172.16.1.111/rod/cif/1/00/00/1000008.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000008
loop_
_publ_author_name
'Neeway, J'
'Abdelouas, A.'
'Ribet, S'
'El Mendili, Y'
'Shumacher, S'
'Grambow, B'
_publ_section_title
;
 Effect of Callovo-Oxfordian clay rock on the dissolution rate of the
 SON68 simulated nuclear waste glass
;
_journal_name_full               'Journal of Nuclear Materials'
_journal_page_first              291
_journal_page_last               300
_journal_volume                  459
_journal_year                    2015
_chemical_compound_source        'hydration product'
_chemical_formula_structural     'Ca5 H O13 P3'
_chemical_formula_sum            'Ca5 H O13 P3'
_chemical_name_mineral           Hydroxylapatite
_chemical_name_systematic        'pentacalcium triphosphate hydroxyl'
_space_group_IT_number           176
_symmetry_cell_setting           hexagonal
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                120
_cell_formula_units_Z            2
_cell_length_a                   9.40(3)
_cell_length_b                   9.40(3)
_cell_length_c                   6.93(3)
_raman_determination_method      experimental
_[local]_chemical_compound_color blue
_[local]_chemical_compound_state Solid
_raman_measurement_device.location 'IMMM Maine university'
_raman_measurement_device.company 'HORIBA Jobin Yvon'
_raman_measurement_device.model  T64000
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 100
_raman_measurement_device.microscope_numerical_aperture 0.90
_raman_measurement_device.excitation_laser_type Argon-Krypton
_raman_measurement_device.excitation_laser_wavelength 514
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 2
_raman_measurement_device.power_on_sample 2
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 0.8
_raman_measurement_device.diffraction_grating 600
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 600
_raman_measurement.range_min     51.6213
_raman_measurement.range_max     2227.3
_rod_data_source.file            Apatite.rod
_rod_data_source.block           1000005
_rod_database.code               1000008
loop_
_raman_complementary.id
_raman_complementary.method
1 EDX
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 Silicon_wafer
2 Diamond
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 1011242 COD http://www.crystallography.net/cod/1011242.html
;
no XRD analysis data.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
51.6213 10225.5
56.4497 10212
61.2756 10213
66.0969 10261
70.918 10539.5
75.7368 11246
80.5508 12699
85.3648 13344
90.174 12845.5
94.9809 12628
99.7877 12726.5
104.59 12827
109.39 12921.5
114.187 13016.5
118.984 13035.5
123.777 13035.5
128.567 13071
133.355 13107.5
138.14 13074.5
142.923 13008
147.702 12936.5
152.48 12997
157.256 12959
162.03 13018
166.799 13014.5
171.567 12954.5
176.332 12944.5
181.096 12931.5
185.855 12920.5
190.615 12933
195.37 12978
200.122 13002
204.875 12927.5
209.622 12924.5
214.368 12846.5
219.111 12814.5
223.852 12778.5
228.59 12790
233.326 12765
238.06 12795
242.791 12841.5
247.521 12762.5
252.245 12792.5
256.97 12859
261.692 12814
266.409 12807.5
271.127 12877.5
275.84 12899
280.552 12890
285.261 12852.5
289.967 12879
294.673 12940.5
299.374 12906
304.073 12970
308.77 12979
313.464 13015
318.156 12998.5
322.846 13139.5
327.533 13070
332.219 13121
336.902 13047
341.58 13079
346.258 13113
350.934 13159
355.606 13127.5
360.277 13167.5
364.944 13086.5
369.611 13186
374.273 13187.5
378.934 13159
383.594 13170.5
388.249 13203.5
392.902 13160.5
397.553 13210
402.202 13242.5
406.849 13213.5
411.493 13246.5
416.135 13213.5
420.774 13285.5
425.412 13440
430.045 13520
434.678 13504
439.308 13602.5
443.934 13971.5
448.56 15165.5
453.182 18522.5
457.804 22148
462.421 24020.5
467.036 20520.5
471.651 16321
476.261 14496.5
480.869 13869
485.475 13692.5
490.079 13561.5
494.68 13504
499.279 13450
503.876 13429.5
508.471 13406
513.064 13368.5
517.654 13397
522.24 13317.5
526.826 13291.5
531.407 13332
535.989 13318.5
540.566 13292.5
545.143 13325
549.715 13367
554.288 13317.5
558.856 13312
563.422 13280.5
567.986 13310
572.547 13300.5
577.107 13326.5
581.664 13330
586.219 13348.5
590.771 13356
595.322 13405.5
599.87 13442
604.416 13570.5
608.958 13791
613.5 14231.5
618.037 15473.5
622.574 16653.5
627.107 15849
631.641 14807
636.169 14543
640.696 14317
645.222 14086
649.744 14421.5
654.264 14734
658.782 14134
663.297 13541
667.811 13445
672.322 13364
676.831 13373.5
681.338 13383.5
685.841 13361
690.343 13432
694.842 13372
699.34 13355
703.836 13325
708.328 13399
712.817 13303.5
717.307 13362
721.792 13325.5
726.276 13305
730.757 13375.5
735.235 13327
739.714 13288
744.189 13334.5
748.659 13299
753.13 13360.5
757.598 13381.5
762.064 13358.5
766.528 13405.5
770.988 13473
775.447 13434
779.903 13505
784.358 13475
788.809 13498.5
793.26 13477.5
797.707 13501
802.152 13501
806.597 13524.5
811.037 13511
815.476 13569
819.912 13484
824.346 13553.5
828.778 13564.5
833.208 13597
837.636 13551.5
842.06 13653
846.483 13706.5
850.905 13733
855.322 13754
859.74 13787
864.153 13808.5
868.566 13857
872.975 13864
877.384 13805
881.789 13878
886.191 13883
890.592 13923
894.99 13954.5
899.387 14036.5
903.781 14070.5
908.173 14163
912.564 14212.5
916.952 14306
921.338 14262
925.722 14269
930.101 14300
934.481 14174.5
938.857 14270
943.232 14269
947.604 14159.5
951.975 14150.5
956.343 14153.5
960.708 14173.5
965.071 14200
969.432 14377.5
973.794 14546
978.151 14774.5
982.503 15656
986.856 19458
991.207 39595
995.556 52353.5
999.903 33498.5
1004.25 17919.5
1008.59 15229
1012.93 14662
1017.27 14537.5
1021.6 14364
1025.93 14261
1030.26 14272.5
1034.59 14254.5
1038.92 14220.5
1043.24 14175.5
1047.57 14201.5
1051.89 14201.5
1056.2 14187
1060.52 14215.5
1064.83 14218.5
1069.15 14234.5
1073.46 14296
1077.76 14327.5
1082.07 14505
1086.37 14851
1090.67 14928
1094.97 14697
1099.27 14444.5
1103.56 14575
1107.85 14511
1112.14 14522.5
1116.43 14489.5
1120.72 14403
1125 14377
1129.28 14464
1133.56 14461.5
1137.84 14652.5
1142.12 14855
1146.39 15400.5
1150.66 15637.5
1154.93 15599
1159.2 15242
1163.46 14887
1167.73 14758
1171.99 14840
1176.24 14807
1180.5 14865
1184.76 14706
1189.01 14557
1193.26 14432
1197.51 14393
1201.75 14374.5
1206 14341.5
1210.24 14343.5
1214.48 14343
1218.71 14340
1222.95 14364
1227.18 14340
1231.42 14347
1235.64 14403.5
1239.87 14371
1244.1 14355.5
1248.32 14324
1252.54 14340.5
1256.76 14413
1260.98 14423.5
1265.19 14471
1269.4 14435.5
1273.61 14499.5
1277.82 14485.5
1282.03 14534
1286.23 14527.5
1290.43 14657
1294.63 14654.5
1298.83 14635.5
1303.03 14678.5
1307.22 14621.5
1311.41 14604.5
1315.6 14720.5
1319.79 14666
1323.98 14721.5
1328.16 14697.5
1332.34 14712.5
1336.52 14721
1340.7 14758.5
1344.87 14651.5
1349.05 14695.5
1353.22 14688.5
1357.39 14743
1361.55 14739.5
1365.72 14742
1369.88 14772.5
1374.04 14755
1378.2 14761.5
1382.36 14805
1386.51 14753.5
1390.67 14815.5
1394.82 14855
1398.97 14823
1403.11 14850
1407.26 14906
1411.4 14940
1415.54 14908.5
1419.68 14871.5
1423.82 14883.5
1427.95 14863.5
1432.08 14971.5
1436.21 14916
1440.34 14936
1444.47 15022.5
1448.59 14921.5
1452.72 14919.5
1456.84 14911.5
1460.96 14938
1465.07 14922
1469.19 14966
1473.3 14936
1477.41 14953
1481.52 14989.5
1485.62 14979
1489.73 14963.5
1493.83 14905.5
1497.93 15009
1502.03 15036.5
1506.13 15031.5
1510.22 15032
1514.31 14971
1518.4 15019.5
1522.49 15024.5
1526.58 15049
1530.67 15055
1534.75 15017
1538.83 15116.5
1542.91 15205.5
1546.98 15174.5
1551.06 15134
1555.13 15172.5
1559.2 15216
1563.27 15288.5
1567.34 15279.5
1571.4 15312
1575.46 15294
1579.52 15315
1583.58 15316.5
1587.64 15318
1591.7 15309
1595.75 15377.5
1599.8 15402.5
1603.85 15308.5
1607.9 15386
1611.94 15394.5
1615.98 15347
1620.02 15330
1624.06 15407
1628.1 15364.5
1632.13 15324.5
1636.17 15294.5
1640.2 15393.5
1644.23 15275.5
1648.26 15313.5
1652.28 15291.5
1656.31 15336
1660.33 15283
1664.35 15294.5
1668.37 15251.5
1672.38 15303.5
1676.39 15375
1680.41 15324.5
1684.42 15225
1688.42 15313.5
1692.43 15402
1696.43 15311
1700.44 15407.5
1704.44 15368
1708.44 15342
1712.43 15441
1716.43 15326.5
1720.42 15390
1724.41 15396.5
1728.4 15423.5
1732.39 15445
1736.37 15415.5
1740.35 15429
1744.34 15415.5
1748.31 15510.5
1752.29 15479
1756.27 15501.5
1760.24 15521.5
1764.21 15489.5
1768.18 15568.5
1772.15 15598
1776.12 15591.5
1780.08 15548.5
1784.04 15582.5
1788 15638.5
1791.96 15543
1795.92 15568
1799.87 15562
1803.82 15466
1807.77 15535
1811.72 15539
1815.67 15537.5
1819.61 15566
1823.56 15497.5
1827.5 15528.5
1831.44 15541
1835.37 15454
1839.31 15516
1843.24 15498.5
1847.17 15487.5
1851.1 15546
1855.03 15490
1858.96 15510.5
1862.88 15520
1866.81 15551.5
1870.73 15522.5
1874.64 15619
1878.56 15572.5
1882.48 15604
1886.39 15574.5
1890.3 15614.5
1894.21 15613
1898.12 15562
1902.02 15596.5
1905.92 15562.5
1909.83 15572.5
1913.73 15636.5
1917.63 15594
1921.52 15588.5
1925.42 15648.5
1929.31 15649.5
1933.2 15638
1937.09 15689
1940.97 15743
1944.86 15696.5
1948.74 15654.5
1952.62 15654.5
1956.5 15724.5
1960.38 15709
1964.26 15770
1968.13 15724
1972 15760
1975.87 15732.5
1979.74 15760
1983.61 15765.5
1987.47 15798
1991.33 15780
1995.2 15789
1999.06 15796.5
2002.91 15778
2006.77 15843.5
2010.62 15839
2014.47 15789.5
2018.33 15849
2022.17 15789.5
2026.02 15811.5
2029.86 15847
2033.71 15787.5
2037.55 15810
2041.39 15794.5
2045.22 15827
2049.06 15787.5
2052.89 15878
2056.72 15862
2060.55 15838.5
2064.38 15914.5
2068.21 15858
2072.03 15873.5
2075.86 15901.5
2079.68 15875.5
2083.5 15904
2087.31 16012
2091.13 15940.5
2094.94 15913.5
2098.75 16021
2102.56 16001.5
2106.37 16047.5
2110.18 16033
2113.98 16053.5
2117.79 16109
2121.59 16075.5
2125.39 16010.5
2129.18 16075.5
2132.98 16139.5
2136.77 16125
2140.57 16112.5
2144.36 16217.5
2148.15 16167
2151.93 16139
2155.72 16195
2159.5 16178
2163.28 16186.5
2167.06 16170.5
2170.84 16243.5
2174.62 16185.5
2178.39 16230
2182.16 16218
2185.93 16318.5
2189.7 16257.5
2193.47 16270.5
2197.23 16249.5
2201 16288
2204.76 16373.5
2208.52 16379.5
2212.28 16347
2216.04 16464.5
2219.79 16395.5
2223.54 16441
2227.3 16477.5