#------------------------------------------------------------------------------ #$Date: 2018-01-23 18:47:37 +0200 (Tue, 23 Jan 2018) $ #$Revision: 362 $ #$URL: svn://172.16.1.111/rod/cif/1/00/00/1000014.rod $ #------------------------------------------------------------------------------ # # This file is available in the Raman Open Database (ROD), # http://solsa.crystallography.net/rod/ # # All data on this site have been placed in the public domain by the # contributors. # data_1000014 loop_ _publ_author_name 'El Mendili, Y' 'Abdelouas, A.' 'Ait Chaou, A' 'Bardeau, Jf' 'Schlegel, Ml' _publ_section_title ; Carbon steel corrosion in clay-rich environment ; _journal_name_full 'Corrosion Science' _journal_page_first 56 _journal_page_last 65 _journal_volume 88 _journal_year 2014 _chemical_compound_source 'corrosion product' _chemical_formula_structural 'Cl0.675 Fe4 O8' _chemical_formula_sum 'Cl0.675 Fe4 O8' _chemical_name_mineral Akaganeite _space_group_IT_number 12 _symmetry_space_group_name_Hall '-I 2y' _symmetry_space_group_name_H-M 'I 1 2/m 1' _cell_angle_alpha 90 _cell_angle_beta 90.24 _cell_angle_gamma 90 _cell_length_a 10.600 _cell_length_b 3.0339 _cell_length_c 10.513 _raman_determination_method experimental _[local]_chemical_compound_color white _[local]_chemical_compound_state Solid _raman_measurement_device.location 'IMMM Maine university' _raman_measurement_device.company 'HORIBA Jobin Yvon' _raman_measurement_device.model T64000 _raman_measurement_device.optics_type microscope _raman_measurement_device.microscope_system dispersive _raman_measurement_device.microscope_objective_magnification 100 _raman_measurement_device.microscope_numerical_aperture 0.90 _raman_measurement_device.excitation_laser_type Argon-Krypton _raman_measurement_device.excitation_laser_wavelength 514 _raman_measurement_device.configuration simple _raman_measurement_device.resolution 2 _raman_measurement_device.power_on_sample 2 _raman_measurement_device.direction_polarization unoriented _raman_measurement_device.spot_size 0.8 _raman_measurement_device.diffraction_grating 600 _raman_measurement.environment Air _raman_measurement.environment_details ; The sample was measured in air. ; _raman_measurement.temperature 300 _raman_measurement.pressure 100 _raman_measurement.background_subtraction no _raman_measurement.background_subtraction_details ; No background subtraction method was applied. ; _raman_measurement.baseline_correction no _raman_measurement.baseline_correction_details ; No baseline correction method was applied. ; _raman_measurement.integration_time 600 _raman_measurement.range_min 81.4356 _raman_measurement.range_max 2250.63 _rod_data_source.file Akaganeite.rod _rod_data_source.block 7200001 _rod_database.code 1000014 loop_ _raman_complementary.id _raman_complementary.method 1 EDX loop_ _raman_measurement_device_calibration.id _raman_measurement_device_calibration.standard 1 Silicon_wafer 2 Diamond loop_ _rod_related_entry.id _rod_related_entry.code _rod_related_entry.database _rod_related_entry.uri _rod_related_entry.description 1 9001319 COD http://www.crystallography.net/cod/9001319.html ; no XRD analysis data. ; loop_ _raman_spectrum.raman_shift _raman_spectrum.intensity 81.4356 528 86.2491 474.5 91.058 527 95.8667 571 100.671 610 105.475 667 110.274 745 115.071 798 119.868 871 124.66 796 129.45 763 134.237 847.5 139.022 939 143.805 959.5 148.585 861 153.363 778.5 158.138 769.5 162.911 737 167.68 723 172.448 708 177.215 709 181.978 712.5 186.737 701.5 191.496 702 196.251 692 201.005 690 205.755 692 210.502 711.5 215.249 689 219.992 693 224.732 689 229.471 710.5 234.206 720 238.939 795.5 243.67 825.5 248.399 876 253.125 925 257.849 966 262.571 1020 267.288 1064 272.005 1107.5 276.72 1243 281.43 1394 286.14 1695 290.846 2065 295.549 2329.5 300.252 2483.5 304.951 2565.5 309.647 2543 314.343 2471 319.035 2317 323.724 2244 328.411 2156 333.096 2003 337.779 1837.5 342.459 1729 347.137 1650 351.81 1550 356.483 1540.5 361.154 1554 365.821 1570.5 370.487 1706.5 375.149 1800.5 379.811 1870 384.469 2061 389.126 2121 393.779 2075 398.429 1949.5 403.078 1925.5 407.724 1803 412.37 1777.5 417.011 1730 421.65 1638.5 426.285 1544.5 430.92 1502.5 435.552 1391 440.182 1361.5 444.81 1312 449.434 1252 454.057 1239 458.678 1197.5 463.295 1207 467.91 1190 472.524 1225 477.134 1223 481.744 1274 486.35 1318.5 490.953 1333 495.554 1325 500.153 1317 504.749 1308 509.344 1299 513.936 1298 518.526 1319.5 523.113 1365 527.699 1399.5 532.28 1431 536.861 1424 541.439 1386 546.014 1286 550.588 1210.5 555.158 1086 559.728 1049 564.294 1013.5 568.857 944 573.42 964 577.979 940 582.536 973.5 587.09 1010.5 591.643 1060 596.193 1167 600.741 1246 605.286 1332 609.83 1299 614.371 1299 618.908 1254 623.445 1201 627.98 1237.5 632.51 1226.5 637.041 1235.5 641.567 1273.5 646.09 1274.5 650.614 1323.5 655.134 1435 659.651 1505 664.166 1584.5 668.681 1666 673.192 1736 677.701 1756 682.207 1825 686.71 1857 691.212 1949.5 695.712 2058 700.21 2188 704.703 2332.5 709.197 2535 713.686 2712.5 718.175 2812 722.66 2789 727.145 2553 731.626 2260.5 736.104 1952.5 740.583 1681.5 745.057 1513.5 749.529 1328 753.999 1249.5 758.467 1209.5 762.932 1139.5 767.396 1081 771.855 1060.5 776.314 1028 780.771 1001.5 785.226 1013.5 789.677 977.5 794.128 962.5 798.574 952.5 803.021 942.5 807.463 948 811.903 934 816.343 902 820.779 909.5 825.213 958.5 829.645 904 834.074 936.5 838.502 937 842.927 923.5 847.35 922 851.771 940.5 856.19 948 860.605 927.5 865.02 924 869.433 908 873.841 936 878.25 921 882.654 933 887.057 926 891.459 960 895.857 984 900.253 988 904.647 1026 909.041 1068.5 913.43 1033.5 917.818 1018.5 922.202 1013 926.585 991.5 930.967 948.5 935.346 913 939.723 858 944.096 895.5 948.47 863 952.839 865 957.208 856 961.572 849.5 965.937 835 970.298 848 974.657 849.5 979.013 831 983.368 818 987.723 845 992.073 848.5 996.419 823 1000.77 827 1005.11 835 1009.45 815.5 1013.79 811.5 1018.13 821 1022.46 830 1026.8 847.5 1031.13 841 1035.46 846.5 1039.78 851 1044.11 822 1048.43 842.5 1052.75 843.5 1057.07 863.5 1061.38 851.5 1065.7 841 1070.01 854 1074.32 856 1078.63 869 1082.93 862 1087.23 844 1091.54 874 1095.84 882 1100.13 903.5 1104.43 889 1108.72 892.5 1113.01 905 1117.3 953.5 1121.58 918.5 1125.87 958 1130.15 954 1134.43 949 1138.7 978 1142.98 1004 1147.25 988.5 1151.52 1006 1155.79 974 1160.06 992.5 1164.33 967 1168.59 1018 1172.85 958 1177.11 979.5 1181.36 940 1185.62 918 1189.87 922 1194.12 898.5 1198.37 885 1202.61 870 1206.86 896 1211.1 863.5 1215.34 873 1219.58 872.5 1223.81 866 1228.05 846 1232.28 863.5 1236.5 869.5 1240.73 863 1244.96 882.5 1249.18 851.5 1253.4 879 1257.62 886 1261.84 883 1266.05 904.5 1270.26 929.5 1274.48 922 1278.68 966.5 1282.89 946 1287.09 967 1291.29 1010 1295.49 1029.5 1299.69 1014 1303.89 1058 1308.08 1066 1312.28 1050 1316.46 1091.5 1320.65 1058 1324.84 1105 1329.02 1097 1333.2 1132 1337.38 1135 1341.56 1155 1345.73 1158 1349.91 1136 1354.08 1157.5 1358.25 1169 1362.41 1194 1366.58 1190.5 1370.74 1221 1374.9 1205 1379.06 1187.5 1383.22 1208.5 1387.38 1221 1391.53 1195 1395.68 1221 1399.83 1252 1403.97 1214 1408.12 1236 1412.26 1215.5 1416.4 1233 1420.54 1203 1424.68 1198 1428.81 1190 1432.94 1169 1437.07 1141 1441.2 1120 1445.33 1113 1449.46 1093.5 1453.58 1084 1457.7 1021.5 1461.82 999 1465.93 977 1470.05 955.5 1474.16 940.5 1478.27 924 1482.38 914.5 1486.49 868.5 1490.59 872.5 1494.69 891 1498.79 877 1502.89 845.5 1506.99 846.5 1511.08 833.5 1515.18 837.5 1519.26 816 1523.35 807 1527.44 821.5 1531.52 817 1535.61 818.5 1539.69 801 1543.77 797 1547.84 770 1551.92 824 1555.99 780 1560.06 799.5 1564.13 791 1568.2 804 1572.26 761 1576.32 756.5 1580.38 756.5 1584.44 769 1588.5 772.5 1592.56 766 1596.61 752 1600.66 746.5 1604.71 732 1608.75 724.5 1612.8 737.5 1616.84 733.5 1620.88 717 1624.92 728.5 1628.96 717 1633 699 1637.03 694 1641.06 731 1645.09 695 1649.12 680 1653.14 697 1657.17 677 1661.19 702 1665.21 681.5 1669.22 681 1673.24 677 1677.25 682.5 1681.27 656 1685.28 669 1689.29 675 1693.29 653.5 1697.3 678 1701.3 669 1705.3 665 1709.3 666 1713.29 676 1717.29 649 1721.28 645 1725.27 651 1729.26 631 1733.25 644.5 1737.23 645 1741.21 653.5 1745.2 653.5 1749.18 634 1753.15 638.5 1757.13 629 1761.1 620.5 1765.07 650 1769.04 633 1773.01 623.5 1776.97 621.5 1780.94 616 1784.9 619 1788.86 628 1792.82 623 1796.78 621.5 1800.73 617.5 1804.68 619 1808.63 611 1812.58 605 1816.53 610 1820.47 590.5 1824.42 558 1828.36 597.5 1832.3 602 1836.24 594.5 1840.17 613.5 1844.1 613 1848.04 602.5 1851.96 590 1855.89 579 1859.82 591 1863.74 586.5 1867.67 612.5 1871.59 594 1875.5 597.5 1879.42 600.5 1883.34 564.5 1887.25 578.5 1891.16 582.5 1895.07 598 1898.98 576 1902.88 560.5 1906.79 569 1910.69 549.5 1914.59 573 1918.48 564 1922.38 591.5 1926.28 569.5 1930.17 555 1934.06 572 1937.95 581 1941.84 553 1945.72 602.5 1949.6 572 1953.48 557 1957.36 579.5 1961.24 580 1965.12 575.5 1968.99 575.5 1972.86 585 1976.73 564 1980.6 572 1984.47 560 1988.33 564 1992.2 582 1996.06 575.5 1999.92 567 2003.77 561 2007.63 586 2011.48 561.5 2015.33 542 2019.19 593 2023.03 580 2026.88 566.5 2030.72 557.5 2034.57 593.5 2038.41 601 2042.25 575 2046.08 569.5 2049.92 568 2053.75 583.5 2057.59 555.5 2061.42 550 2065.24 569 2069.07 568.5 2072.89 583 2076.72 584.5 2080.54 547 2084.36 582.5 2088.17 586 2091.99 549.5 2095.8 568.5 2099.62 564.5 2103.43 572.5 2107.23 584.5 2111.04 555 2114.85 566.5 2118.65 568 2122.45 565.5 2126.25 548.5 2130.05 566 2133.84 562 2137.64 557 2141.43 567 2145.22 557.5 2149.01 542 2152.79 558 2156.58 540 2160.36 555 2164.14 562 2167.92 568 2171.7 543 2175.48 561 2179.25 554.5 2183.03 534 2186.8 552 2190.57 543 2194.33 548 2198.1 552.5 2201.86 564.5 2205.62 531 2209.38 562 2213.14 535.5 2216.9 567 2220.65 530.5 2224.41 552.5 2228.16 546 2231.91 548.5 2235.66 576.5 2239.4 562 2243.15 537 2246.89 518 2250.63 558