#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-04-26 13:11:50 +0300 (Thu, 26 Apr 2018) $
#$Revision: 464 $
#$URL: svn://172.16.1.111/rod/cif/1/00/00/1000030.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000030
loop_
_publ_author_name
'Gasperin, M.'
_publ_section_title
;
 Synthese et identification de deux oxydes doubles de tantale et d'etain
 Sample: synthetic
;
_journal_name_full
'Comptes Rendus Hebdomadaires des Seances de l Academie des Sciences'
_journal_page_first              2340
_journal_page_last               2342
_journal_volume                  240
_journal_year                    1955
_chemical_compound_source        R050546
_chemical_formula_sum            'O7 Pb2 Sb2'
_chemical_name_mineral           Bindheimite
_space_group_IT_number           227
_symmetry_space_group_name_Hall  'F 4d 2 3 -1d'
_symmetry_space_group_name_H-M   'F d -3 m :1'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_length_a                   10.40
_cell_length_b                   10.40
_cell_length_c                   10.40
_cell_volume                     1124.864
_exptl_crystal_density_diffrn    9.092
_cod_original_sg_symbol_H-M      'F d -3 m'
_cod_original_formula_sum        'Sb2 Pb2 O7'
_cod_database_code               9009948
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type helium-neon
_raman_measurement_device.excitation_laser_wavelength 780
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 12
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R050546.rod
_rod_data_source.block           3500000
_rod_database.code               1000030
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9009948 COD http://www.crystallography.net/cod/9009948.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
150.2309 18.18726
150.7131 0.2919920
151.1952 16.24805
151.6773 30.54834
152.1594 45.57739
152.6415 49.48047
153.1236 54.16040
153.6058 58.73706
154.0879 63.37109
154.5700 66.66797
155.0521 66.46533
155.5342 62.50635
156.0163 59.67017
156.4985 61.85229
156.9806 64.74390
157.4627 64.51709
157.9448 59.96118
158.4269 53.52075
158.9090 48.99023
159.3912 47.16357
159.8733 45.19287
160.3554 42.77905
160.8375 39.80151
161.3196 36.29395
161.8017 32.23145
162.2839 27.50317
162.7660 21.47974
163.2481 12.13086
163.7302 4.248779
164.2123 0.9924320
164.6944 4.589844
165.1766 7.594971
165.6587 10.43042
166.1408 13.38501
166.6229 18.01611
167.1050 24.97754
167.5871 32.86963
168.0693 42.85938
168.5514 53.57764
169.0335 62.16333
169.5156 66.41187
169.9977 66.70142
170.4798 70.36182
170.9620 79.31055
171.4441 88.97388
171.9262 97.66968
172.4083 105.3850
172.8904 112.4377
173.3725 118.9009
173.8547 124.9214
174.3368 131.2944
174.8189 137.4346
175.3010 144.2751
175.7831 152.9124
176.2652 163.4106
176.7474 174.2717
177.2295 184.9155
177.7116 195.0671
178.1937 204.0449
178.6758 210.4590
179.1579 216.0305
179.6401 223.5630
180.1222 233.7722
180.6043 243.8137
181.0864 251.4231
181.5685 257.6543
182.0506 264.2678
182.5328 272.1731
183.0149 281.0327
183.4970 290.1802
183.9791 301.4158
184.4612 309.8867
184.9433 312.1873
185.4255 310.8267
185.9076 310.1541
186.3897 313.4197
186.8718 320.1484
187.3539 324.9336
187.8360 324.7192
188.3182 325.8049
188.8003 331.3003
189.2824 339.5540
189.7645 347.0049
190.2466 350.5278
190.7287 349.8586
191.2109 351.5850
191.6930 358.8770
192.1751 365.4792
192.6572 368.6580
193.1393 369.2620
193.6214 370.0195
194.1036 373.5403
194.5857 380.4485
195.0678 384.9282
195.5499 387.0940
196.0320 387.3970
196.5141 384.3452
196.9963 378.9851
197.4784 374.9540
197.9605 375.9451
198.4426 382.8809
198.9247 388.4956
199.4068 391.4976
199.8890 393.9135
200.3711 397.9468
200.8532 403.5836
201.3353 408.2839
201.8174 409.4753
202.2995 406.9122
202.7817 404.5803
203.2638 403.4766
203.7459 402.0961
204.2280 398.2390
204.7101 391.4249
205.1922 385.2173
205.6744 383.5598
206.1565 385.4895
206.6386 386.6743
207.1207 386.6586
207.6028 385.1124
208.0849 381.5513
208.5671 375.7798
209.0492 368.0609
209.5313 357.9109
210.0134 345.9768
210.4955 334.3206
210.9776 323.3245
211.4598 312.9490
211.9419 303.2190
212.4240 294.6025
212.9061 286.1501
213.3882 277.3616
213.8703 268.3772
214.3525 259.2952
214.8346 250.5386
215.3167 241.9893
215.7988 232.7224
216.2809 222.6211
216.7630 212.0449
217.2451 200.2446
217.7273 188.1240
218.2094 177.2720
218.6915 168.8257
219.1736 162.4990
219.6557 156.5610
220.1378 152.2639
220.6200 146.8188
221.1021 138.8103
221.5842 129.3818
222.0663 120.3079
222.5484 112.7166
223.0305 106.4771
223.5127 100.6509
223.9948 95.04028
224.4769 90.22632
224.9590 87.20483
225.4411 85.09985
225.9232 82.45703
226.4054 78.20239
226.8875 72.40381
227.3696 67.02563
227.8517 62.51270
228.3338 57.88550
228.8159 52.48438
229.2981 46.93628
229.7802 42.38623
230.2623 39.67041
230.7444 38.58032
231.2265 36.72363
231.7086 33.02124
232.1908 29.77466
232.6729 27.70728
233.1550 26.50317
233.6371 25.52368
234.1192 24.39966
234.6013 23.16602
235.0835 22.04736
235.5656 20.90698
236.0477 20.01196
236.5298 19.05713
237.0119 18.36060
237.4940 19.03784
237.9762 22.15137
238.4583 26.62231
238.9404 27.57080
239.4225 22.26538
239.9046 17.18408
240.3867 14.70044
240.8689 14.12500
241.3510 13.70215
241.8331 12.50171
242.3152 11.00464
242.7973 10.68042
243.2794 11.96289
243.7616 13.45703
244.2437 14.52979
244.7258 15.34448
245.2079 16.43848
245.6900 18.26489
246.1721 20.16211
246.6543 20.77368
247.1364 19.63599
247.6185 18.66089
248.1006 19.08154
248.5827 20.48535
249.0648 21.28320
249.5470 20.23828
250.0291 19.35498
250.5112 21.90405
250.9933 28.48901
251.4754 34.51196
251.9576 36.96313
252.4397 36.57446
252.9218 36.62695
253.4039 37.74585
253.8860 39.84692
254.3681 42.72729
254.8503 46.37378
255.3324 50.32300
255.8145 54.48462
256.2966 58.80103
256.7787 62.67456
257.2608 65.20752
257.7430 68.36841
258.2251 74.12231
258.7072 82.11182
259.1893 89.86743
259.6714 94.84009
260.1535 97.81982
260.6357 103.7720
261.1178 115.4431
261.5999 127.1150
262.0820 134.4600
262.5641 138.7229
263.0462 143.7971
263.5284 152.4258
264.0105 164.1069
264.4926 176.2292
264.9747 189.3884
265.4568 201.9497
265.9389 212.6636
266.4211 222.2952
266.9032 232.2620
267.3853 243.1487
267.8674 255.0178
268.3495 268.4172
268.8316 283.9460
269.3138 300.2969
269.7959 318.1260
270.2780 336.1345
270.7601 352.1138
271.2422 364.2876
271.7243 374.2556
272.2065 387.0706
272.6886 403.1577
273.1707 421.6372
273.6528 444.3398
274.1349 468.1724
274.6170 488.9365
275.0992 504.5972
275.5813 517.4143
276.0634 532.9683
276.5455 553.0547
277.0276 572.7012
277.5097 589.9756
277.9919 606.9810
278.4740 625.7944
278.9561 647.2383
279.4382 670.1494
279.9203 692.8948
280.4024 716.2915
280.8846 737.3643
281.3667 753.2783
281.8488 768.7612
282.3309 787.7947
282.8130 811.1382
283.2951 835.8777
283.7773 857.7610
284.2594 875.9802
284.7415 893.1372
285.2236 907.9746
285.7057 922.9460
286.1878 939.7407
286.6700 958.3560
287.1521 977.6042
287.6342 996.4387
288.1163 1015.001
288.5984 1031.961
289.0805 1045.301
289.5627 1058.885
290.0448 1075.164
290.5269 1093.563
291.0090 1111.503
291.4911 1126.635
291.9732 1138.750
292.4554 1150.252
292.9375 1162.715
293.4196 1173.053
293.9017 1179.784
294.3838 1183.542
294.8659 1185.642
295.3481 1186.868
295.8302 1187.317
296.3123 1188.223
296.7944 1192.144
297.2765 1193.746
297.7586 1191.027
298.2408 1185.510
298.7229 1179.704
299.2050 1175.097
299.6871 1170.843
300.1692 1163.659
300.6513 1151.698
301.1335 1138.741
301.6156 1125.166
302.0977 1110.878
302.5798 1095.510
303.0619 1078.991
303.5440 1061.794
304.0262 1044.571
304.5083 1027.102
304.9904 1010.184
305.4725 995.5762
305.9546 980.4727
306.4367 961.7996
306.9189 939.1970
307.4010 915.3870
307.8831 894.2634
308.3652 877.1797
308.8473 859.3674
309.3294 839.5591
309.8116 820.0063
310.2937 802.4963
310.7758 786.8276
311.2579 771.4568
311.7400 755.0476
312.2221 737.3667
312.7043 719.0869
313.1864 696.5437
313.6685 676.9148
314.1506 664.5713
314.6327 657.6094
315.1148 651.0791
315.5970 641.3870
316.0791 628.8291
316.5612 617.4290
317.0433 608.6772
317.5254 599.3477
318.0075 587.9443
318.4897 575.7703
318.9718 564.7634
319.4539 555.9199
319.9360 548.8174
320.4181 542.0610
320.9002 535.5361
321.3824 529.7100
321.8645 524.8560
322.3466 520.5808
322.8287 516.4851
323.3108 512.4932
323.7929 508.6367
324.2751 505.0781
324.7572 502.0886
325.2393 498.8445
325.7214 495.3992
326.2035 491.5815
326.6856 486.9167
327.1678 481.5452
327.6499 476.2515
328.1320 471.8242
328.6141 468.2793
329.0962 465.6558
329.5783 465.8242
330.0605 465.0996
330.5426 461.9497
331.0247 456.4482
331.5068 449.1687
331.9889 440.2812
332.4710 430.0713
332.9532 422.3157
333.4353 419.6414
333.9174 416.4524
334.3995 411.5723
334.8816 405.6499
335.3637 399.6426
335.8459 394.1067
336.3280 388.8696
336.8101 383.6858
337.2922 378.2029
337.7743 373.3149
338.2564 370.6523
338.7386 367.6733
339.2206 361.2959
339.7028 350.9622
340.1849 339.8882
340.6670 333.5425
341.1491 335.6084
341.6312 333.1526
342.1133 322.6323
342.5955 311.2104
343.0776 302.5876
343.5597 296.9346
344.0418 292.5564
344.5239 288.2031
345.0060 283.9922
345.4882 278.3284
345.9703 269.4185
346.4524 260.6782
346.9345 252.4626
347.4166 244.9773
347.8987 238.6733
348.3809 234.1274
348.8630 230.9070
349.3451 226.9866
349.8272 222.2810
350.3093 216.3738
350.7914 208.4734
351.2736 200.0400
351.7557 192.3870
352.2378 185.8604
352.7199 180.2998
353.2020 176.0010
353.6841 173.9407
354.1663 169.9939
354.6484 161.9080
355.1305 153.4326
355.6126 146.4934
356.0947 141.2747
356.5768 137.0649
357.0590 133.6404
357.5411 131.1487
358.0232 127.4189
358.5053 121.8745
358.9874 115.8589
359.4695 109.2119
359.9517 102.5879
360.4338 97.39600
360.9159 94.94116
361.3980 93.94946
361.8801 90.29639
362.3622 82.95825
362.8444 75.79688
363.3265 69.69092
363.8086 64.33594
364.2907 59.83936
364.7728 56.39331
365.2549 53.31958
365.7371 49.54980
366.2192 44.84888
366.7013 40.36401
367.1834 36.01978
367.6655 32.32666
368.1476 29.77979
368.6298 28.32971
369.1119 27.40283
369.5940 27.67651
370.0761 28.46045
370.5582 26.01245
371.0403 17.98877
371.5225 10.35889
372.0046 8.038208
372.4867 9.423340
372.9688 10.44373
373.4509 9.429077
373.9330 7.119385
374.4152 4.191650
374.8973 0.5345460
375.3794 2.477051
375.8615 4.187988
376.3436 4.618286
376.8257 3.669434
377.3079 0.6781010
377.7900 2.008911
378.2721 2.330322
378.7542 0.7880860
379.2363 0.2458500
379.7184 0.1105960
380.2006 0.7224120
380.6827 4.2969000E-02
381.1648 1.848511
381.6469 3.904907
382.1290 6.430176
382.6111 8.696655
383.0933 9.487549
383.5754 8.654541
384.0575 7.099243
384.5396 5.280884
385.0217 3.336670
385.5038 2.155762
385.9860 1.819214
386.4681 2.107300
386.9502 3.581177
387.4323 5.703735
387.9144 6.603394
388.3965 5.082275
388.8787 2.209839
389.3608 0.9649660
389.8429 2.442627
390.3250 3.004883
390.8071 1.097046
391.2892 1.760498
391.7714 3.753418
392.2535 4.476929
392.7356 4.613770
393.2177 4.994751
393.6998 5.743530
394.1819 5.981812
394.6641 4.608521
395.1462 3.718506
395.6283 5.211060
396.1104 8.337280
396.5925 10.75488
397.0746 10.83386
397.5568 9.076782
398.0389 8.092529
398.5210 8.424805
399.0031 8.968506
399.4852 10.16052
399.9673 11.25012
400.4495 11.32458
400.9316 10.13660
401.4137 8.207886
401.8958 6.248901
402.3779 4.057129
402.8600 2.426270
403.3422 0.8665770
403.8243 0.1562500
404.3064 1.601318
404.7885 4.391113
405.2706 6.192139
405.7527 5.052734
406.2349 1.378784
406.7170 1.274536
407.1991 1.764160
407.6812 2.812622
408.1633 5.709229
408.6454 9.163818
409.1276 11.77112
409.6097 13.00244
410.0918 13.35095
410.5739 13.31482
411.0560 12.65234
411.5381 12.80090
412.0203 14.95227
412.5024 17.14392
412.9845 18.26660
413.4666 18.34656
413.9487 17.99353
414.4308 17.19751
414.9130 16.23694
415.3951 16.31470
415.8772 17.83313
416.3593 19.40674
416.8414 21.00293
417.3235 22.00684
417.8057 21.13025
418.2878 17.18835
418.7699 13.07751
419.2520 12.19189
419.7341 14.14050
420.2162 14.91162
420.6984 12.58032
421.1805 9.516235
421.6626 9.057373
422.1447 11.22705
422.6268 12.83447
423.1089 12.45483
423.5911 10.98193
424.0732 9.515869
424.5553 8.166748
425.0374 6.948120
425.5195 5.801636
426.0016 4.796997
426.4838 4.237793
426.9659 5.733887
427.4480 5.981445
427.9301 1.827759
428.4122 4.557373
428.8943 8.301880
429.3765 7.421265
429.8586 4.238403
430.3407 2.683228
430.8228 3.176880
431.3049 4.740967
431.7870 8.424561
432.2692 12.40674
432.7513 15.36804
433.2334 17.27319
433.7155 18.87317
434.1976 20.81323
434.6797 23.04895
435.1619 24.71790
435.6440 24.67493
436.1261 25.32300
436.6082 27.33191
437.0903 30.10510
437.5724 32.92383
438.0546 35.53809
438.5367 38.25098
439.0188 41.78406
439.5009 46.80017
439.9830 50.38745
440.4651 51.12952
440.9473 51.65173
441.4294 52.65540
441.9115 54.45081
442.3936 57.61401
442.8757 63.10547
443.3578 69.86877
443.8400 73.87756
444.3221 73.73779
444.8042 74.31653
445.2863 78.33777
445.7684 83.37769
446.2505 87.06128
446.7327 88.83582
447.2148 90.68164
447.6969 94.67029
448.1790 100.3674
448.6611 105.2905
449.1432 108.8167
449.6254 111.9303
450.1075 115.4241
450.5896 119.2079
451.0717 123.0908
451.5538 127.5620
452.0359 131.7128
452.5181 134.2410
453.0002 135.4033
453.4823 137.0120
453.9644 139.9585
454.4465 143.7509
454.9286 147.2975
455.4108 150.4243
455.8929 153.8005
456.3750 157.5332
456.8571 161.6084
457.3392 166.1287
457.8214 171.0657
458.3035 176.1587
458.7856 181.2220
459.2677 186.2531
459.7498 191.1621
460.2319 196.1732
460.7141 200.7615
461.1962 204.1490
461.6783 207.2450
462.1604 211.7155
462.6425 218.1455
463.1246 224.9974
463.6068 229.3392
464.0889 229.3533
464.5710 231.1705
465.0531 236.2279
465.5352 241.8047
466.0173 246.8453
466.4995 251.2131
466.9816 254.9888
467.4637 258.0950
467.9458 260.9833
468.4279 265.1984
468.9100 271.5796
469.3922 277.2413
469.8743 280.6394
470.3564 283.2565
470.8385 285.9399
471.3206 288.9126
471.8027 292.9944
472.2849 299.4711
472.7670 307.7107
473.2491 314.8763
473.7312 320.2129
474.2133 325.5713
474.6954 332.3971
475.1776 340.3005
475.6597 348.4335
476.1418 357.0984
476.6239 365.7618
477.1060 373.2488
477.5881 379.9354
478.0703 387.7463
478.5524 397.3738
479.0345 408.7080
479.5166 421.5459
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