#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-04-26 13:35:50 +0300 (Thu, 26 Apr 2018) $
#$Revision: 490 $
#$URL: svn://172.16.1.111/rod/cif/1/00/00/1000045.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000045
loop_
_publ_author_name
'Burns, P. C.'
'Hawthorne, F. C.'
_publ_section_title
;
 Edge-sharing MnO4 tetrahedra in the structure of akatoreite,
 Mn9Al2Si8O24(OH)8
;
_journal_name_full               'The Canadian Mineralogist'
_journal_page_first              321
_journal_page_last               329
_journal_volume                  31
_journal_year                    1993
_chemical_compound_source        R060230
_chemical_formula_sum            'Al2 H8 Mn9 O32 Si8'
_chemical_name_mineral           Akatoreite
_space_group_IT_number           2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                104.46
_cell_angle_beta                 93.81
_cell_angle_gamma                104.18
_cell_length_a                   8.337
_cell_length_b                   10.367
_cell_length_c                   7.629
_cell_volume                     613.285
_exptl_crystal_density_diffrn    3.501
_cod_original_formula_sum        'Mn9 Al2 Si8 O32 H8'
_cod_database_code               9004265
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type helium-neon
_raman_measurement_device.excitation_laser_wavelength 780
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 12
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R060230.rod
_rod_data_source.block           3500000
_rod_database.code               1000045
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9004265 COD http://www.crystallography.net/cod/9004265.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
150.1633 0.0000000E+00
150.6454 0.4808830
151.1275 1.761961
151.6096 2.867934
152.0917 3.210708
152.5739 3.347460
153.0560 4.063303
153.5381 5.646786
154.0202 7.518604
154.5023 8.404840
154.9844 7.660673
155.4665 6.840586
155.9487 6.666038
156.4308 6.468329
156.9129 5.300811
157.3950 2.512969
157.8771 0.4239520
158.3592 0.1959310
158.8414 1.331063
159.3235 3.271595
159.8056 3.522977
160.2877 2.943928
160.7698 2.161691
161.2519 1.431165
161.7341 0.7773450
162.2162 0.2734980
162.6983 0.1439650
163.1804 0.2817300
163.6625 0.6444550
164.1446 1.854926
164.6268 2.264209
165.1089 2.850398
165.5910 3.249234
166.0731 3.943012
166.5552 5.349291
167.0373 6.711784
167.5195 8.203841
168.0016 9.526497
168.4837 10.04401
168.9658 9.213970
169.4479 7.177158
169.9300 6.183330
170.4122 7.304406
170.8943 8.220446
171.3764 7.678873
171.8585 5.901634
172.3406 4.024498
172.8227 2.803493
173.3049 2.257541
173.7870 1.851809
174.2691 1.753109
174.7512 1.675474
175.2333 1.408917
175.7154 0.9433050
176.1976 0.3140840
176.6797 0.7368420
177.1618 0.4283590
177.6439 0.8887160
178.1260 0.1060010
178.6081 0.1179960
179.0903 0.7307590
179.5724 8.5859997E-03
180.0545 0.4867160
180.5366 0.5762280
181.0187 2.443045
181.5008 4.018884
181.9830 4.993026
182.4651 5.653056
182.9472 6.026671
183.4293 5.580131
183.9114 5.481110
184.3935 5.639323
184.8757 6.115969
185.3578 6.480125
185.8399 6.310510
186.3220 5.711729
186.8041 5.827202
187.2862 7.802588
187.7684 9.298315
188.2505 9.230165
188.7326 8.158444
189.2147 7.294571
189.6968 7.708323
190.1789 9.481561
190.6611 10.24924
191.1432 8.725724
191.6253 7.442186
192.1074 7.366882
192.5895 8.266453
193.0716 9.336280
193.5538 9.864581
194.0359 9.756757
194.5180 9.905652
195.0001 10.75772
195.4822 11.40995
195.9643 11.11001
196.4465 10.07122
196.9286 9.356560
197.4107 10.16024
197.8928 12.82716
198.3749 13.61710
198.8570 10.96768
199.3392 7.853415
199.8213 6.247087
200.3034 6.241060
200.7855 6.629351
201.2676 6.331791
201.7497 5.310903
202.2319 4.340888
202.7140 3.353688
203.1961 2.692360
203.6782 1.948693
204.1603 1.124872
204.6424 0.9532850
205.1246 2.275159
205.6067 4.701389
206.0888 6.647161
206.5709 7.768420
207.0530 8.245826
207.5351 8.332897
208.0173 8.109389
208.4994 7.440863
208.9815 5.798500
209.4636 3.629144
209.9457 1.892847
210.4278 1.042575
210.9100 0.8456530
211.3921 0.8861660
211.8742 1.374966
212.3563 1.624039
212.8384 1.107040
213.3205 0.1033020
213.8027 0.5392090
214.2848 0.4750020
214.7669 1.330495
215.2490 1.376739
215.7311 4.2626001E-02
216.2132 0.2859100
216.6954 0.3014930
217.1775 0.6514630
217.6596 0.7612670
218.1417 1.008986
218.6238 4.097953
219.1059 6.290557
219.5881 6.763998
220.0702 7.284277
220.5523 8.515095
221.0344 10.13114
221.5165 11.63605
221.9986 12.57623
222.4808 12.96296
222.9629 13.46358
223.4450 14.34099
223.9271 15.06814
224.4092 15.27283
224.8913 15.26885
225.3735 15.63787
225.8556 16.82335
226.3377 18.71222
226.8198 20.07445
227.3019 20.18892
227.7840 20.51359
228.2662 21.62733
228.7483 23.13449
229.2304 24.35367
229.7125 24.85117
230.1946 24.66357
230.6767 24.16384
231.1589 23.01474
231.6410 21.94560
232.1231 20.87295
232.6052 20.01717
233.0873 19.83951
233.5694 20.69315
234.0516 22.38864
234.5337 23.49866
235.0158 24.20713
235.4979 24.36254
235.9800 23.78604
236.4621 22.72042
236.9443 21.47596
237.4264 20.15219
237.9085 18.86864
238.3906 18.40988
238.8727 19.54527
239.3548 20.40518
239.8370 20.38854
240.3191 19.62432
240.8012 18.34033
241.2833 16.51270
241.7654 14.38003
242.2475 12.60161
242.7297 11.03212
243.2118 9.948164
243.6939 9.848536
244.1760 10.40574
244.6581 10.60448
245.1402 9.935820
245.6224 8.777063
246.1045 7.996860
246.5866 7.884768
247.0687 7.358274
247.5508 5.267716
248.0329 2.171856
248.5151 0.1265090
248.9972 0.1148900
249.4793 1.141132
249.9614 1.644446
250.4435 1.537551
250.9256 1.518186
251.4078 2.308198
251.8899 3.619440
252.3720 4.091639
252.8541 2.911374
253.3362 1.349643
253.8183 0.9895150
254.3005 1.818887
254.7826 2.366783
255.2647 1.222907
255.7468 0.4316500
256.2289 0.8105490
256.7110 0.1044650
257.1931 8.5545003E-02
257.6753 0.3934970
258.1574 5.9687000E-02
258.6395 0.3760120
259.1216 0.5479400
259.6037 0.4678770
260.0858 0.1635140
260.5680 0.5561320
261.0501 1.239136
261.5322 1.531872
262.0143 1.548679
262.4964 1.644862
262.9785 2.011863
263.4607 2.665687
263.9428 3.818590
264.4249 6.100437
264.9070 7.922154
265.3891 8.455242
265.8712 8.063169
266.3534 7.393168
266.8355 6.652634
267.3176 5.954398
267.7997 5.758496
268.2818 6.014599
268.7639 6.893910
269.2461 9.131856
269.7282 11.81070
270.2103 13.47802
270.6924 13.19259
271.1745 11.59827
271.6566 10.86907
272.1388 12.11869
272.6209 12.49611
273.1030 10.55609
273.5851 7.876154
274.0672 6.263547
274.5493 6.526726
275.0315 7.805679
275.5136 7.972400
275.9957 6.480333
276.4778 5.036365
276.9599 3.974206
277.4420 3.078800
277.9242 2.023791
278.4063 0.6967100
278.8884 0.4796660
279.3705 0.4897290
279.8526 1.298671
280.3347 2.388620
280.8169 1.742599
281.2990 0.7949180
281.7811 0.6823880
282.2632 1.646355
282.7453 3.015249
283.2274 3.872766
283.7096 4.239533
284.1917 3.978742
284.6738 2.091719
285.1559 0.4215460
285.6380 0.3744630
286.1201 1.912085
286.6023 3.711872
287.0844 4.089633
287.5665 2.362325
288.0486 1.958159
288.5307 4.405694
289.0128 6.699011
289.4950 7.197680
289.9771 6.171584
290.4592 5.061956
290.9413 5.259995
291.4234 6.919473
291.9055 7.830981
292.3877 7.385627
292.8698 6.816891
293.3519 6.338841
293.8340 6.046798
294.3161 6.081901
294.7982 6.598598
295.2804 7.531115
295.7625 7.998634
296.2446 7.352242
296.7267 6.921286
297.2088 7.146917
297.6909 7.708726
298.1731 8.111703
298.6552 8.079497
299.1373 7.725556
299.6194 7.475011
300.1015 7.228692
300.5836 7.239360
301.0658 7.762328
301.5479 8.452895
302.0300 8.977169
302.5121 9.198238
302.9942 9.158011
303.4763 8.921279
303.9585 8.237447
304.4406 7.737983
304.9227 7.129964
305.4048 6.870119
305.8869 7.552130
306.3690 9.202417
306.8512 11.11177
307.3333 12.27952
307.8154 12.40313
308.2975 12.50112
308.7796 12.65850
309.2617 12.73381
309.7439 12.55281
310.2260 12.16116
310.7081 11.81407
311.1902 11.78749
311.6723 12.16217
312.1544 12.29915
312.6366 12.08668
313.1187 11.77809
313.6008 11.13512
314.0829 10.41395
314.5650 10.34721
315.0471 11.55272
315.5293 13.78139
316.0114 14.33597
316.4935 11.84988
316.9756 9.167743
317.4577 6.478758
317.9398 4.079993
318.4220 2.397373
318.9041 1.659459
319.3862 1.539801
319.8683 0.9851950
320.3504 0.3410600
320.8326 0.8087060
321.3147 0.5695140
321.7968 0.2230950
322.2789 0.4805570
322.7610 0.3916350
323.2431 0.5913840
323.7253 0.5122230
324.2074 0.2672390
324.6895 0.2450040
325.1716 0.6408200
325.6537 0.2150260
326.1358 2.0241000E-02
326.6180 7.7432998E-02
327.1001 0.1548510
327.5822 3.9944001E-02
328.0643 0.6423870
328.5464 0.7999770
329.0285 0.1824260
329.5107 0.4981290
329.9928 0.1889670
330.4749 0.3004890
330.9570 0.3082300
331.4391 0.4601390
331.9212 0.5525790
332.4034 1.654474
332.8855 2.249524
333.3676 2.616503
333.8497 2.624232
334.3318 2.476465
334.8139 2.449263
335.2961 2.683141
335.7782 3.087771
336.2603 3.391422
336.7424 3.446447
337.2245 3.560252
337.7066 3.913500
338.1888 4.279467
338.6709 4.376052
339.1530 4.171878
339.6351 4.040682
340.1172 4.748532
340.5993 7.224442
341.0815 8.093765
341.5636 5.818308
342.0457 3.436659
342.5278 2.730985
343.0099 3.695814
343.4920 5.137590
343.9742 5.875426
344.4563 5.747337
344.9384 5.661523
345.4205 5.938485
345.9026 6.021144
346.3847 5.250361
346.8669 4.264075
347.3490 4.222312
347.8311 5.967594
348.3132 8.912923
348.7953 10.63589
349.2774 10.31832
349.7596 9.932922
350.2417 9.906790
350.7238 10.00361
351.2059 9.878849
351.6880 9.438595
352.1701 8.968137
352.6523 8.855129
353.1344 9.127222
353.6165 9.687465
354.0986 11.01991
354.5807 12.26416
355.0628 12.82899
355.5450 12.72525
356.0271 12.37903
356.5092 12.16566
356.9913 12.09192
357.4734 12.01882
357.9555 12.14536
358.4377 12.02835
358.9198 11.43686
359.4019 10.48541
359.8840 9.365721
360.3661 8.046856
360.8482 6.742169
361.3304 6.149014
361.8125 6.560715
362.2946 7.059773
362.7767 7.815073
363.2588 8.277514
363.7409 7.581646
364.2231 5.300605
364.7052 2.838005
365.1873 2.306102
365.6694 3.984377
366.1515 4.942852
366.6336 3.696909
367.1158 2.168149
367.5979 1.700154
368.0800 2.336534
368.5621 3.462209
369.0442 4.997481
369.5263 6.750061
370.0085 7.678946
370.4906 7.319113
370.9727 6.820721
371.4548 6.954683
371.9369 7.539951
372.4190 8.209991
372.9012 8.961893
373.3833 9.634757
373.8654 9.953424
374.3475 9.888115
374.8296 9.702461
375.3117 9.360031
375.7939 9.057022
376.2760 9.074793
376.7581 9.482345
377.2402 10.10285
377.7223 10.88151
378.2044 11.73300
378.6866 12.53249
379.1687 13.32248
379.6508 14.09334
380.1329 14.84197
380.6150 15.56859
381.0971 16.08855
381.5793 16.34966
382.0614 16.39074
382.5435 16.06294
383.0256 15.31313
383.5077 14.97698
383.9898 15.99343
384.4720 18.06696
384.9541 19.13890
385.4362 18.51048
385.9183 17.47052
386.4004 16.62475
386.8825 15.98344
387.3647 15.56343
387.8468 15.52040
388.3289 15.58161
388.8110 15.02170
389.2931 13.74445
389.7752 12.29810
390.2574 10.19924
390.7395 8.162712
391.2216 7.240893
391.7037 7.628477
392.1858 8.382881
392.6679 8.416214
393.1501 7.544964
393.6322 6.812128
394.1143 6.426524
394.5964 5.974892
395.0785 5.182766
395.5606 4.119891
396.0428 2.968119
396.5249 1.778890
397.0070 0.6813990
397.4891 0.3586910
397.9712 2.079397
398.4533 3.048641
398.9355 2.756339
399.4176 1.662053
399.8997 4.3573000E-02
400.3818 0.2468510
400.8639 1.703693
401.3460 2.404150
401.8282 1.353024
402.3103 0.4117670
402.7924 0.6391350
403.2745 1.067073
403.7566 0.8625220
404.2387 1.128523
404.7209 0.9086730
405.2030 0.4185210
405.6851 7.7846996E-02
406.1672 0.3270960
406.6493 0.2779070
407.1314 2.1800000E-02
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408.0957 1.003928
408.5778 0.6449300
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409.5420 1.906438
410.0241 2.180206
410.5063 1.297935
410.9884 0.5568480
411.4705 1.4367000E-02
411.9526 0.2059420
412.4347 0.1001000
412.9168 0.8463430
413.3990 1.652672
413.8811 2.298722
414.3632 2.799082
414.8453 3.221348
415.3274 3.601424
415.8095 3.811934
416.2917 3.639771
416.7738 3.300130
417.2559 3.035321
417.7380 2.827813
418.2201 2.871151
418.7022 3.632418
419.1844 4.992432
419.6665 5.715686
420.1486 5.096602
420.6307 4.141040
421.1128 4.222427
421.5949 5.325492
422.0771 6.270088
422.5592 6.490240
423.0413 6.369670
423.5234 6.357648
424.0055 6.499002
424.4876 6.908407
424.9698 7.886199
425.4519 9.227649
425.9340 9.739429
426.4161 8.438406
426.8982 7.372158
427.3803 7.851624
427.8625 9.199150
428.3446 10.01466
428.8267 9.774641
429.3088 8.821851
429.7909 7.653724
430.2730 5.763534
430.7552 4.773335
431.2373 5.405268
431.7194 6.376249
432.2015 7.005161
432.6836 7.226164
433.1657 7.252687
433.6479 7.202051
434.1300 7.109606
434.6121 7.466949
435.0942 8.717558
435.5763 9.921771
436.0584 11.14285
436.5406 12.15131
437.0227 12.49466
437.5048 12.06871
437.9869 11.56361
438.4690 12.23237
438.9511 14.69648
439.4333 16.30822
439.9154 16.03822
440.3975 15.79447
440.8796 16.54645
441.3617 18.06306
441.8438 19.50987
442.3260 20.21620
442.8081 20.53304
443.2902 21.78052
443.7723 24.55165
444.2544 26.76970
444.7365 26.86120
445.2187 26.53479
445.7008 27.48878
446.1829 30.11608
446.6650 32.97120
447.1471 34.66801
447.6292 35.43062
448.1114 36.49035
448.5935 37.96502
449.0756 39.87961
449.5577 42.63142
450.0398 45.89226
450.5219 48.67101
451.0041 50.75508
451.4862 52.19880
451.9683 53.11362
452.4504 53.46735
452.9325 52.93963
453.4146 51.21513
453.8968 48.73423
454.3789 46.35658
454.8610 43.99643
455.3431 41.97383
455.8252 41.15305
456.3073 40.27925
456.7895 37.47911
457.2716 32.72248
457.7537 28.13523
458.2358 25.49367
458.7179 24.77440
459.2000 24.19562
459.6822 24.48082
460.1643 24.27900
460.6464 22.57254
461.1285 20.30325
461.6106 18.82074
462.0927 18.58459
462.5748 19.10686
463.0569 19.66910
463.5391 20.51420
464.0212 20.67458
464.5033 19.54995
464.9854 18.39341
465.4675 17.60359
465.9496 17.24498
466.4318 17.40441
466.9139 18.19273
467.3960 19.36121
467.8781 20.22463
468.3602 20.62110
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