#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-04-26 13:36:53 +0300 (Thu, 26 Apr 2018) $
#$Revision: 506 $
#$URL: svn://172.16.1.111/rod/cif/1/00/00/1000059.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000059
loop_
_publ_author_name
'Basciano, L. C.'
'Groat, L. A.'
'Roberts, A. C.'
'Gault, R. A.'
'Dunning, G. E.'
'Walstrom, R. E.'
_publ_section_title
;
 Bigcreekite: A new barium silicate mineral species from Fresno County,
 California Locality: Fresno County, California, USA
;
_journal_name_full               'The Canadian Mineralogist'
_journal_page_first              761
_journal_page_last               768
_journal_paper_doi               10.2113/gscanmin.39.3.761
_journal_volume                  39
_journal_year                    2001
_chemical_compound_source        R060432
_chemical_formula_sum            'Ba H8 O9 Si2'
_chemical_name_mineral           Bigcreekite
_space_group_IT_number           62
_symmetry_space_group_name_Hall  '-P 2ac 2n'
_symmetry_space_group_name_H-M   'P n m a'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_length_a                   5.0453
_cell_length_b                   9.044
_cell_length_c                   18.366
_cell_volume                     838.035
_exptl_crystal_density_diffrn    2.739
_cod_original_formula_sum        'Ba Si2 O9 H8'
_cod_database_code               9004625
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type helium-neon
_raman_measurement_device.excitation_laser_wavelength 780
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 12
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R060432.rod
_rod_data_source.block           3500000
_rod_database.code               1000059
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9004625 COD http://www.crystallography.net/cod/9004625.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
108.3710 0.0000000E+00
108.8531 22.88696
109.3353 2.595459
109.8174 4.900635
110.2995 46.59570
110.7816 115.0308
111.2637 197.1697
111.7458 279.4529
112.2280 398.6812
112.7101 570.1167
113.1922 770.6602
113.6743 986.6416
114.1564 1216.071
114.6385 1445.523
115.1207 1578.583
115.6028 1603.988
116.0849 1567.528
116.5670 1453.517
117.0491 1278.748
117.5313 1085.793
118.0134 898.8245
118.4955 720.6570
118.9776 566.4773
119.4597 435.7971
119.9418 328.5801
120.4240 247.9280
120.9061 194.8589
121.3882 159.7610
121.8703 135.9919
122.3524 121.3225
122.8345 115.1116
123.3167 110.9099
123.7988 113.9238
124.2809 141.3254
124.7630 205.4529
125.2451 288.0693
125.7272 371.4390
126.2094 454.8828
126.6915 544.2764
127.1736 639.9612
127.6557 738.9915
128.1378 852.6143
128.6199 1015.998
129.1021 1192.910
129.5842 1355.262
130.0663 1485.007
130.5484 1597.481
131.0305 1704.688
131.5126 1812.702
131.9948 1895.344
132.4769 1941.507
132.9590 1943.211
133.4411 1911.354
133.9232 1837.742
134.4053 1727.474
134.8875 1621.818
135.3696 1528.781
135.8517 1434.977
136.3338 1337.104
136.8159 1238.934
137.2980 1136.295
137.7802 1030.935
138.2623 923.9871
138.7444 827.4167
139.2265 742.7559
139.7086 666.8384
140.1907 601.3965
140.6729 545.5215
141.1550 492.6621
141.6371 434.5004
142.1192 368.3787
142.6013 308.1158
143.0834 254.2053
143.5656 207.4049
144.0477 168.8710
144.5298 138.9653
145.0119 115.7502
145.4940 95.85034
145.9761 77.79578
146.4583 67.21826
146.9404 74.48828
147.4225 93.03601
147.9046 98.97180
148.3867 79.28760
148.8689 47.91418
149.3510 23.03198
149.8331 4.675537
150.3152 6.516235
150.7973 5.879517
151.2794 8.180420
151.7616 16.92822
152.2437 5.335938
152.7258 11.63831
153.2079 20.73853
153.6900 15.96667
154.1721 6.780151
154.6543 12.17761
155.1364 42.55920
155.6185 65.26721
156.1006 78.60559
156.5827 59.08228
157.0648 47.32410
157.5470 42.91699
158.0291 67.73999
158.5112 55.01697
158.9933 57.46021
159.4754 60.59680
159.9575 42.82202
160.4397 63.82874
160.9218 46.57104
161.4039 44.76135
161.8860 36.04138
162.3681 42.60437
162.8502 44.57434
163.3324 31.44092
163.8145 26.78735
164.2966 35.40173
164.7787 26.69092
165.2608 49.05164
165.7429 27.47705
166.2251 21.25464
166.7072 16.01135
167.1893 9.974487
167.6714 2.501953
168.1535 23.37415
168.6356 33.88245
169.1178 51.34155
169.5999 53.55530
170.0820 48.35010
170.5641 60.99194
171.0462 64.16235
171.5283 79.25562
172.0105 88.63574
172.4926 92.71509
172.9747 69.63489
173.4568 86.17932
173.9389 89.61316
174.4210 94.41614
174.9032 122.2184
175.3853 113.3125
175.8674 144.7687
176.3495 162.9021
176.8316 190.0360
177.3137 203.9774
177.7959 224.5997
178.2780 246.1620
178.7601 266.6497
179.2422 290.6115
179.7243 314.4943
180.2064 343.8417
180.6886 371.9738
181.1707 397.4795
181.6528 423.2852
182.1349 451.6753
182.6170 482.3309
183.0991 517.7976
183.5813 557.3467
184.0634 608.1417
184.5455 651.1267
185.0276 686.7102
185.5097 693.0374
185.9918 736.9240
186.4740 765.6384
186.9561 793.6050
187.4382 842.4357
187.9203 852.4602
188.4024 900.7412
188.8845 933.5818
189.3667 973.3352
189.8488 997.7521
190.3309 1026.699
190.8130 1070.711
191.2951 1106.185
191.7772 1128.329
192.2594 1167.749
192.7415 1205.117
193.2236 1256.526
193.7057 1313.494
194.1878 1390.738
194.6699 1460.361
195.1521 1511.523
195.6342 1548.731
196.1163 1582.731
196.5984 1621.691
197.0805 1665.744
197.5626 1715.533
198.0448 1777.052
198.5269 1838.414
199.0090 1893.157
199.4911 1942.883
199.9732 1993.605
200.4553 2051.209
200.9375 2116.394
201.4196 2188.036
201.9017 2275.688
202.3838 2361.099
202.8659 2427.113
203.3480 2475.026
203.8302 2526.245
204.3123 2607.973
204.7944 2738.191
205.2765 2848.681
205.7586 2926.677
206.2407 2993.787
206.7229 3068.331
207.2050 3153.612
207.6871 3238.704
208.1692 3310.519
208.6513 3369.695
209.1334 3412.521
209.6156 3430.845
210.0977 3434.428
210.5798 3435.095
211.0619 3436.890
211.5440 3434.136
212.0261 3414.409
212.5083 3372.996
212.9904 3328.559
213.4725 3286.128
213.9546 3243.530
214.4367 3199.020
214.9188 3151.812
215.4010 3099.543
215.8831 3031.600
216.3652 2944.706
216.8473 2871.488
217.3294 2834.940
217.8115 2821.697
218.2937 2792.803
218.7758 2731.270
219.2579 2663.759
219.7400 2634.966
220.2221 2648.056
220.7042 2670.138
221.1864 2686.310
221.6685 2698.682
222.1506 2717.899
222.6327 2753.477
223.1148 2791.601
223.5969 2817.064
224.0791 2825.484
224.5612 2834.737
225.0433 2864.775
225.5254 2911.024
226.0075 2939.363
226.4896 2933.346
226.9718 2906.741
227.4539 2877.144
227.9360 2845.528
228.4181 2810.422
228.9002 2770.358
229.3823 2725.536
229.8645 2676.759
230.3466 2627.888
230.8287 2571.821
231.3108 2500.085
231.7929 2409.229
232.2750 2314.853
232.7572 2236.181
233.2393 2175.385
233.7214 2107.375
234.2035 2011.380
234.6856 1912.479
235.1677 1830.999
235.6499 1773.185
236.1320 1723.508
236.6141 1663.573
237.0962 1591.621
237.5783 1519.987
238.0604 1445.367
238.5426 1375.912
239.0247 1320.123
239.5068 1281.439
239.9889 1247.963
240.4710 1200.913
240.9531 1133.285
241.4353 1076.694
241.9174 1043.208
242.3995 1020.905
242.8816 1003.607
243.3637 989.5824
243.8458 976.3032
244.3280 961.2019
244.8101 947.0244
245.2922 922.6489
245.7743 872.2083
246.2564 819.0764
246.7385 782.6254
247.2207 769.3174
247.7028 768.3590
248.1849 749.6199
248.6670 756.5803
249.1491 757.0010
249.6312 751.2970
250.1134 717.6101
250.5955 722.7446
251.0776 713.9658
251.5597 705.7421
252.0418 719.6956
252.5239 696.1201
253.0061 712.0884
253.4882 713.9160
253.9703 723.9261
254.4524 719.9333
254.9345 721.8018
255.4166 740.0310
255.8988 751.0280
256.3809 749.9855
256.8630 767.4902
257.3451 750.7825
257.8272 747.6619
258.3094 752.2833
258.7915 768.0940
259.2736 794.9395
259.7557 835.2898
260.2378 903.6741
260.7199 956.5918
261.2021 990.1372
261.6842 1010.348
262.1663 1014.212
262.6484 1002.832
263.1305 993.2407
263.6126 1020.510
264.0948 1120.638
264.5769 1187.813
265.0590 1188.173
265.5411 1177.692
266.0232 1201.565
266.5053 1269.276
266.9875 1355.251
267.4696 1417.054
267.9517 1438.751
268.4338 1470.113
268.9159 1506.572
269.3980 1549.376
269.8802 1603.683
270.3623 1670.216
270.8444 1748.704
271.3265 1836.302
271.8086 1940.274
272.2907 2036.825
272.7729 2121.854
273.2550 2204.785
273.7371 2291.597
274.2192 2383.349
274.7013 2477.060
275.1834 2570.572
275.6656 2665.650
276.1477 2754.457
276.6298 2841.251
277.1119 2917.900
277.5940 2976.032
278.0761 3015.763
278.5583 3046.758
279.0404 3082.575
279.5225 3129.717
280.0046 3162.740
280.4867 3190.198
280.9688 3200.230
281.4510 3182.515
281.9331 3138.073
282.4152 3077.725
282.8973 3013.347
283.3794 2944.871
283.8615 2872.206
284.3437 2800.782
284.8258 2722.294
285.3079 2628.437
285.7900 2521.323
286.2721 2409.950
286.7542 2304.492
287.2364 2205.721
287.7185 2103.280
288.2006 1990.942
288.6827 1881.215
289.1648 1782.765
289.6469 1692.743
290.1291 1599.510
290.6112 1490.465
291.0933 1362.665
291.5754 1257.966
292.0575 1199.101
292.5396 1142.328
293.0218 1068.230
293.5039 982.9926
293.9860 906.3916
294.4681 856.6897
294.9502 833.4852
295.4323 787.4385
295.9145 676.8798
296.3966 585.2378
296.8787 541.9526
297.3608 531.2914
297.8429 523.7504
298.3250 499.9934
298.8072 460.8109
299.2893 422.5687
299.7714 393.3469
300.2535 359.1077
300.7356 307.0690
301.2177 250.4838
301.6999 208.6779
302.1820 193.5455
302.6641 198.4302
303.1462 197.1763
303.6283 184.2560
304.1104 172.0771
304.5926 160.4236
305.0747 151.3519
305.5568 148.8243
306.0389 155.0894
306.5210 164.7928
307.0031 162.4031
307.4853 133.2523
307.9674 117.5228
308.4495 133.1261
308.9316 156.0265
309.4137 162.7220
309.8958 145.2123
310.3780 116.6575
310.8601 100.6519
311.3422 103.5649
311.8243 104.7108
312.3064 101.7814
312.7885 96.85400
313.2707 89.44409
313.7528 80.06750
314.2349 72.36377
314.7170 73.32751
315.1991 88.12646
315.6812 93.06665
316.1634 76.15771
316.6455 56.86652
317.1276 45.85797
317.6097 43.78076
318.0918 44.23871
318.5739 39.74341
319.0561 29.24109
319.5382 23.43781
320.0203 32.70557
320.5024 37.74530
320.9845 27.83374
321.4666 5.240662
321.9488 20.02252
322.4309 43.97247
322.9130 66.12616
323.3951 72.11078
323.8772 43.25494
324.3593 21.03723
324.8415 34.18939
325.3236 67.61493
325.8057 86.17853
326.2878 59.29071
326.7699 2.773560
327.2520 21.31824
327.7342 5.029968
328.2163 31.35345
328.6984 32.74347
329.1805 20.78809
329.6626 12.29443
330.1447 15.10223
330.6269 24.26355
331.1090 29.94238
331.5911 30.39984
332.0732 33.28217
332.5553 48.32794
333.0374 64.99384
333.5196 71.94946
334.0017 65.13623
334.4838 50.68347
334.9659 33.27710
335.4480 12.47449
335.9301 4.874512
336.4123 16.56439
336.8944 23.18146
337.3765 24.35089
337.8586 18.94244
338.3407 13.73358
338.8228 15.74481
339.3050 23.57330
339.7871 27.70380
340.2692 25.77570
340.7513 18.98749
341.2334 7.315796
341.7155 9.469727
342.1977 23.26807
342.6798 30.05145
343.1619 31.02319
343.6440 28.52362
344.1261 22.39972
344.6082 14.27844
345.0904 6.214294
345.5725 1.947937
346.0546 13.09235
346.5367 35.32263
347.0188 57.55664
347.5009 65.26251
347.9831 56.76654
348.4652 40.46228
348.9473 18.91913
349.4294 6.139832
349.9115 20.87665
350.3936 17.87347
350.8758 9.599609
351.3579 2.833069
351.8400 1.884155
352.3221 2.703857
352.8042 3.376221
353.2863 13.66034
353.7685 15.35089
354.2506 1.196167
354.7327 14.68903
355.2148 7.869446
355.6969 7.281738
356.1790 1.650024
356.6612 40.56323
357.1433 99.93042
357.6254 127.5616
358.1075 103.9069
358.5896 81.31812
359.0717 61.45514
359.5539 47.43817
360.0360 45.79871
360.5181 57.76898
361.0002 73.04858
361.4823 75.41876
361.9644 53.06958
362.4466 47.87238
362.9287 75.92572
363.4108 107.5206
363.8929 122.1251
364.3750 119.0621
364.8571 110.2587
365.3393 106.7830
365.8214 109.1122
366.3035 112.8887
366.7856 117.1058
367.2677 123.6060
367.7498 141.9177
368.2320 162.8955
368.7141 165.7340
369.1962 133.3771
369.6783 75.10339
370.1604 47.23218
370.6425 78.07898
371.1247 103.5703
371.6068 107.9753
372.0889 102.6160
372.5710 99.91931
373.0531 104.8588
373.5352 115.9918
374.0174 134.1180
374.4995 169.0635
374.9816 184.1877
375.4637 159.1634
375.9458 123.1495
376.4279 92.76654
376.9101 71.64417
377.3922 58.09204
377.8743 52.18597
378.3564 54.11847
378.8385 56.22412
379.3206 52.69830
379.8028 54.67859
380.2849 72.37292
380.7670 101.6700
381.2491 128.0515
381.7312 143.7552
382.2133 150.9783
382.6955 154.4091
383.1776 150.5883
383.6597 148.1813
384.1418 150.3550
384.6239 161.9358
385.1060 189.2546
385.5882 245.2574
386.0703 306.3376
386.5524 350.6852
387.0345 379.4482
387.5166 398.1796
387.9987 401.0082
388.4809 399.2739
388.9630 418.7998
389.4451 472.7124
389.9272 520.1768
390.4093 540.0043
390.8914 537.9642
391.3736 527.5886
391.8557 513.4804
392.3378 493.7432
392.8199 461.2393
393.3020 410.1465
393.7841 373.4303
394.2663 362.2637
394.7484 361.8564
395.2305 361.4749
395.7126 358.8158
396.1947 350.4691
396.6768 329.3793
397.1590 292.9225
397.6411 289.5996
398.1232 345.1953
398.6053 402.4612
399.0874 434.7595
399.5695 449.0823
400.0517 463.6635
400.5338 488.4885
401.0159 525.3362
401.4980 580.8439
401.9801 680.0273
402.4622 767.0754
402.9444 826.4452
403.4265 877.7149
403.9086 942.4910
404.3907 1026.224
404.8728 1115.766
405.3549 1186.301
405.8371 1221.420
406.3192 1290.348
406.8013 1443.453
407.2834 1589.041
407.7655 1687.394
408.2477 1738.452
408.7298 1760.067
409.2119 1768.880
409.6940 1761.518
410.1761 1708.419
410.6582 1588.914
411.1404 1455.099
411.6225 1328.834
412.1046 1207.896
412.5867 1086.739
413.0688 957.5193
413.5509 831.4209
414.0331 727.3626
414.5152 647.5327
414.9973 575.0082
415.4794 504.4647
415.9615 437.9962
416.4436 376.9221
416.9258 320.2092
417.4079 273.0447
417.8900 238.5082
418.3721 215.4811
418.8542 205.8878
419.3363 214.2868
419.8185 219.5389
420.3006 190.8588
420.7827 126.8551
421.2648 83.40491
421.7469 82.30841
422.2290 92.66571
422.7112 89.52063
423.1933 73.22083
423.6754 56.20392
424.1575 45.71942
424.6396 41.92719
425.1217 46.33508
425.6039 66.82800
426.0860 84.85779
426.5681 100.8360
427.0502 110.3983
427.5323 102.7458
428.0144 74.36005
428.4966 41.87488
428.9787 36.85223
429.4608 79.80481
429.9429 109.3681
430.4250 118.6143
430.9071 122.4578
431.3893 132.8734
431.8714 147.9357
432.3535 154.4353
432.8356 137.0701
433.3177 97.79132
433.7998 72.60468
434.2820 62.25269
434.7641 66.58441
435.2462 92.41644
435.7283 129.2233
436.2104 161.5945
436.6925 182.3986
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