#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-04-26 13:37:05 +0300 (Thu, 26 Apr 2018) $
#$Revision: 509 $
#$URL: svn://172.16.1.111/rod/cif/1/00/00/1000061.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000061
loop_
_publ_author_name
'Rosenzweig, A.'
'Ryan, R. R.'
_publ_section_title
;
 Kasolite, Pb(UO2)(SiO4)*H2O
;
_journal_name_full               'Crystal Structure Communications'
_journal_page_first              617
_journal_page_last               621
_journal_volume                  6
_journal_year                    1977
_chemical_compound_source        R060479
_chemical_formula_sum            'H2 O7 Pb Si U'
_chemical_name_mineral           Kasolite
_space_group_IT_number           14
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90
_cell_angle_beta                 104.22
_cell_angle_gamma                90
_cell_length_a                   6.704
_cell_length_b                   6.932
_cell_length_c                   13.252
_cell_volume                     596.979
_exptl_crystal_density_diffrn    6.535
_cod_original_formula_sum        'Pb U Si O7 H2'
_cod_database_code               9012787
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type helium-neon
_raman_measurement_device.excitation_laser_wavelength 780
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 12
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R060479.rod
_rod_data_source.block           3500000
_rod_database.code               1000061
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9012787 COD http://www.crystallography.net/cod/9012787.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
132.5834 0.0000000E+00
133.0656 1.845963
133.5477 2.838531
134.0298 1.698593
134.5119 3.6896002E-02
134.9940 0.5372310
135.4761 0.3335110
135.9583 4.8308998E-02
136.4404 0.3461610
136.9225 0.7090910
137.4046 0.7126620
137.8867 0.7195280
138.3688 1.296799
138.8510 2.768127
139.3331 4.849136
139.8152 6.608170
140.2973 7.907242
140.7794 9.177307
141.2615 10.46947
141.7437 11.82196
142.2258 13.46863
142.7079 15.56467
143.1900 18.03391
143.6721 20.63789
144.1542 23.37874
144.6364 26.23911
145.1185 29.30435
145.6006 32.63681
146.0827 35.77255
146.5648 38.46332
147.0469 40.84299
147.5291 42.95142
148.0112 44.68071
148.4933 46.27124
148.9754 48.28737
149.4575 50.97025
149.9396 53.71765
150.4218 56.47882
150.9039 59.15997
151.3860 61.60034
151.8681 63.68091
152.3502 65.46011
152.8323 67.33496
153.3145 69.30457
153.7966 71.38905
154.2787 73.65921
154.7608 76.05777
155.2429 78.47601
155.7250 80.82312
156.2072 83.06967
156.6893 85.61169
157.1714 88.66862
157.6535 91.76305
158.1356 94.83237
158.6177 97.80165
159.0999 100.5143
159.5820 102.7852
160.0641 104.5299
160.5462 106.3768
161.0283 108.2992
161.5104 110.3226
161.9926 112.6599
162.4747 115.3204
162.9568 117.7270
163.4389 119.2537
163.9210 119.9281
164.4031 119.9581
164.8853 119.3150
165.3674 118.0580
165.8495 116.2437
166.3316 113.8201
166.8137 110.9633
167.2958 107.7897
167.7780 104.3408
168.2601 100.6702
168.7422 96.64737
169.2243 92.37935
169.7064 88.38824
170.1885 84.85384
170.6707 81.46910
171.1528 77.98688
171.6349 74.44150
172.1170 70.96277
172.5991 67.55797
173.0812 64.21019
173.5634 61.30630
174.0455 59.27289
174.5276 57.38020
175.0097 55.28232
175.4918 53.00862
175.9739 50.84894
176.4561 49.21600
176.9382 48.34857
177.4203 47.14308
177.9024 45.22435
178.3845 43.29919
178.8666 41.67825
179.3488 40.44157
179.8309 39.52905
180.3130 38.89511
180.7951 38.62321
181.2772 38.49437
181.7593 38.70502
182.2415 38.91699
182.7236 38.90936
183.2057 38.62244
183.6878 38.09402
184.1699 37.33817
184.6520 35.99817
185.1342 35.20468
185.6163 35.35298
186.0984 35.90492
186.5805 36.31674
187.0626 36.42949
187.5447 36.37350
188.0269 36.39772
188.5090 36.60774
188.9911 36.50452
189.4732 35.51459
189.9553 34.20602
190.4374 33.50920
190.9196 34.05573
191.4017 35.10544
191.8838 35.55467
192.3659 35.36505
192.8480 35.22668
193.3301 35.54129
193.8123 36.17340
194.2944 36.67319
194.7765 36.88281
195.2586 36.96365
195.7407 37.13062
196.2228 37.41095
196.7050 37.61110
197.1871 37.56050
197.6692 37.27968
198.1513 37.10635
198.6334 37.20683
199.1155 37.38557
199.5977 37.44897
200.0798 37.40279
200.5619 37.50261
201.0440 37.96481
201.5261 38.78384
202.0082 39.81418
202.4904 41.46161
202.9725 43.02461
203.4546 44.11090
203.9367 44.68973
204.4188 45.02988
204.9009 45.40451
205.3831 45.74826
205.8652 46.38480
206.3473 47.46672
206.8294 48.63293
207.3115 49.72745
207.7936 50.73555
208.2758 51.71138
208.7579 52.63214
209.2400 53.37189
209.7221 54.30653
210.2042 55.82320
210.6863 57.25591
211.1685 57.96536
211.6506 57.90701
212.1327 57.71265
212.6148 58.33850
213.0969 60.43237
213.5790 62.00462
214.0612 62.66927
214.5433 63.08963
215.0254 63.64163
215.5075 64.45187
215.9896 65.69553
216.4717 67.70154
216.9539 71.08185
217.4360 73.75275
217.9181 75.23228
218.4002 76.21460
218.8823 77.34152
219.3644 78.76529
219.8466 80.33861
220.3287 81.82504
220.8108 83.15689
221.2929 84.82722
221.7750 87.18390
222.2571 89.81009
222.7393 92.23227
223.2214 94.35895
223.7035 96.22791
224.1856 97.76018
224.6677 98.98273
225.1498 100.2314
225.6320 101.6514
226.1141 103.1360
226.5962 104.5548
227.0783 105.9357
227.5604 107.1044
228.0425 107.8252
228.5247 108.1801
229.0068 108.4083
229.4889 108.6591
229.9710 108.8411
230.4531 108.7166
230.9352 108.1807
231.4174 107.4998
231.8995 107.1286
232.3816 106.8477
232.8637 105.9742
233.3458 104.0255
233.8279 101.2153
234.3101 98.16367
234.7922 94.85718
235.2743 91.37715
235.7564 87.77829
236.2385 84.07867
236.7206 80.27588
237.2028 76.38969
237.6849 72.42319
238.1670 68.25589
238.6491 63.56345
239.1312 59.18546
239.6133 55.47496
240.0955 52.24173
240.5776 49.09689
241.0597 45.80499
241.5418 42.43526
242.0239 39.43094
242.5060 37.08183
242.9882 34.70334
243.4703 31.85255
243.9524 28.88205
244.4345 26.32150
244.9166 24.52072
245.3987 23.31096
245.8809 21.94777
246.3630 20.36250
246.8451 18.68910
247.3272 16.67258
247.8093 14.66187
248.2914 13.24007
248.7736 12.77681
249.2557 12.90317
249.7378 12.09227
250.2199 8.970535
250.7020 6.591782
251.1841 6.032806
251.6663 6.201523
252.1484 5.687881
252.6305 3.788132
253.1126 1.084473
253.5947 0.6311040
254.0768 0.3498230
254.5590 0.1747440
255.0411 0.1814420
255.5232 0.3797150
256.0053 0.8103790
256.4874 1.486771
256.9695 2.318756
257.4517 3.086029
257.9338 3.975830
258.4159 4.548767
258.8980 4.642670
259.3801 4.490631
259.8622 4.321457
260.3444 4.216156
260.8265 4.139465
261.3086 4.023941
261.7907 3.841187
262.2728 3.665131
262.7549 3.680389
263.2371 3.615906
263.7192 3.078430
264.2013 1.982010
264.6834 0.7687680
265.1655 0.1225890
265.6476 0.3958740
266.1298 0.4117430
266.6119 0.2385100
267.0940 0.2508700
267.5761 1.381409
268.0582 3.182800
268.5403 4.993835
269.0225 5.965958
269.5046 5.807587
269.9867 6.134598
270.4688 7.254776
270.9509 8.706299
271.4330 10.12965
271.9152 11.47400
272.3973 12.83212
272.8794 14.27963
273.3615 15.83174
273.8436 17.45628
274.3257 19.32494
274.8079 21.18178
275.2900 22.65903
275.7721 23.76477
276.2542 24.99077
276.7363 26.82066
277.2184 29.16833
277.7006 31.15614
278.1827 32.50902
278.6648 33.70355
279.1469 35.03047
279.6290 36.48871
280.1111 37.98990
280.5933 39.47366
281.0754 40.96878
281.5575 42.58965
282.0396 44.74585
282.5217 46.53760
283.0038 47.24178
283.4860 47.01918
283.9681 46.74832
284.4502 46.91179
284.9323 47.17616
285.4144 46.85252
285.8965 45.75249
286.3787 44.56062
286.8608 43.75436
287.3429 43.19305
287.8250 42.32510
288.3071 40.90640
288.7892 39.17857
289.2714 37.48598
289.7535 35.83568
290.2356 34.19505
290.7177 32.58650
291.1998 30.97597
291.6819 29.20593
292.1641 27.14899
292.6462 25.10468
293.1283 23.39365
293.6104 21.98314
294.0925 20.71416
294.5746 19.63326
295.0568 18.64319
295.5389 17.48128
296.0210 16.01958
296.5031 14.68283
296.9852 13.97676
297.4673 13.70692
297.9495 13.36574
298.4316 12.80547
298.9137 12.08134
299.3958 11.18983
299.8779 10.06485
300.3600 9.097015
300.8422 8.751968
301.3243 8.723129
301.8064 8.479126
302.2885 7.624603
302.7706 6.738953
303.2527 6.688309
303.7349 7.555923
304.2170 8.173492
304.6991 7.695938
305.1812 6.784607
305.6633 6.338989
306.1454 6.553070
306.6276 7.065765
307.1097 7.679459
307.5918 8.379700
308.0739 8.896957
308.5560 9.088120
309.0381 9.056473
309.5203 8.917328
310.0024 8.672256
310.4845 8.510773
310.9666 8.483948
311.4487 8.543961
311.9308 8.812653
312.4130 9.408859
312.8951 10.13638
313.3772 10.85445
313.8593 11.52223
314.3414 11.99464
314.8235 12.14545
315.3057 12.14039
315.7878 12.23304
316.2699 12.38786
316.7520 12.70130
317.2341 13.55157
317.7162 14.62547
318.1984 15.19218
318.6805 14.67914
319.1626 13.68565
319.6447 13.21688
320.1268 13.40144
320.6089 13.44414
321.0911 12.81169
321.5732 11.80724
322.0553 10.78655
322.5374 9.740646
323.0195 8.795837
323.5016 8.142548
323.9838 7.789848
324.4659 7.368973
324.9480 6.685623
325.4301 5.910912
325.9122 5.246925
326.3943 4.700493
326.8765 4.255371
327.3586 3.951805
327.8407 3.754257
328.3228 3.478203
328.8049 3.031418
329.2870 2.565300
329.7692 2.299332
330.2513 2.210678
330.7334 1.988541
331.2155 1.286232
331.6976 0.3624190
332.1797 0.1714400
332.6619 0.2086720
333.1440 2.5169000E-02
333.6261 0.5474620
334.1082 1.217606
334.5903 1.675659
335.0724 1.595421
335.5546 1.353149
336.0367 1.482292
336.5188 2.021362
337.0009 2.554199
337.4830 2.832741
337.9651 2.947884
338.4473 3.078537
338.9294 3.262924
339.4115 3.435585
339.8936 3.454430
340.3757 3.362610
340.8578 3.538345
341.3400 4.288322
341.8221 5.202805
342.3042 5.658485
342.7863 5.608055
343.2684 5.422188
343.7505 5.142570
344.2327 4.865227
344.7148 4.878830
345.1969 5.327087
345.6790 5.853058
346.1611 6.026787
346.6432 5.903038
347.1254 5.727448
347.6075 5.493759
348.0896 5.276276
348.5717 5.231674
349.0538 5.380432
349.5359 5.445671
350.0181 5.096771
350.5002 4.482178
350.9823 4.259163
351.4644 4.760956
351.9465 5.412788
352.4286 6.035133
352.9108 6.548561
353.3929 6.491272
353.8750 5.430000
354.3571 3.864738
354.8392 3.066071
355.3214 3.277428
355.8035 3.565948
356.2856 3.601616
356.7677 3.492249
357.2498 3.477020
357.7319 3.650917
358.2141 3.770836
358.6962 3.366096
359.1783 2.269150
359.6604 1.716187
360.1425 2.422020
360.6246 3.375755
361.1068 3.569168
361.5889 2.935669
362.0710 2.141502
362.5531 1.749489
363.0352 1.750641
363.5173 1.534027
363.9995 0.8532710
364.4816 0.2162480
364.9637 0.1576080
365.4458 0.2942120
365.9279 0.2396160
366.4100 1.8723000E-02
366.8922 0.3679500
367.3743 0.4257660
367.8564 0.1709590
368.3385 0.5288090
368.8206 0.3056110
369.3027 0.1176830
369.7849 0.2636340
370.2670 8.8200001E-03
370.7491 0.3583680
371.2312 0.4073180
371.7133 9.6465997E-02
372.1954 0.1819310
372.6776 0.6281810
373.1597 1.424843
373.6418 1.650208
374.1239 1.322098
374.6060 0.7511670
375.0881 0.1492460
375.5703 0.4769740
376.0524 0.9290080
376.5345 1.034546
377.0166 1.169518
377.4987 1.438354
377.9808 1.784279
378.4630 2.132957
378.9451 2.450745
379.4272 2.723297
379.9093 2.907867
380.3914 2.905807
380.8735 2.979950
381.3557 3.056114
381.8378 3.259872
382.3199 3.788345
382.8020 4.607170
383.2841 5.401573
383.7662 5.773857
384.2484 5.631264
384.7305 5.712410
385.2126 6.212906
385.6947 6.760422
386.1768 7.215164
386.6589 7.631065
387.1411 8.147873
387.6232 8.872353
388.1053 9.725098
388.5874 10.41313
389.0695 10.83349
389.5516 11.24766
390.0338 11.70626
390.5159 12.20388
390.9980 12.71131
391.4801 13.23037
391.9622 13.82915
392.4443 14.62701
392.9265 15.63676
393.4086 16.58013
393.8907 17.39072
394.3728 18.16737
394.8549 19.04585
395.3370 19.96095
395.8192 20.66339
396.3013 20.69528
396.7834 20.41119
397.2655 21.11069
397.7476 23.16895
398.2297 25.29236
398.7119 26.93729
399.1940 28.20837
399.6761 29.09778
400.1582 29.42332
400.6403 29.72913
401.1224 30.66978
401.6046 32.21800
402.0867 33.61695
402.5688 34.52850
403.0509 35.35536
403.5330 36.58226
404.0151 38.17863
404.4973 39.74238
404.9794 41.24313
405.4615 42.65155
405.9436 43.88015
406.4257 44.92436
406.9078 45.90559
407.3900 46.90497
407.8721 47.96169
408.3542 49.14294
408.8363 50.66324
409.3184 52.13309
409.8005 53.21420
410.2827 53.99883
410.7648 54.86168
411.2469 56.02345
411.7290 57.24636
412.2111 57.92355
412.6932 57.84206
413.1754 57.86623
413.6575 58.29666
414.1396 58.81766
414.6217 59.10454
415.1038 59.10248
415.5859 58.95837
416.0681 58.84491
416.5502 58.79289
417.0323 58.29538
417.5144 57.17682
417.9965 55.90177
418.4786 54.53536
418.9608 53.14663
419.4429 51.86880
419.9250 50.78145
420.4071 49.76003
420.8892 48.45045
421.3713 46.72878
421.8535 44.86164
422.3356 42.73255
422.8177 40.54219
423.2998 38.46019
423.7819 36.51326
424.2640 34.65382
424.7462 32.80611
425.2283 30.93580
425.7104 29.20227
426.1925 27.80428
426.6746 26.39126
427.1567 24.76105
427.6389 23.05846
428.1210 21.54118
428.6031 20.34235
429.0852 19.35713
429.5673 18.40448
430.0494 17.47694
430.5316 16.42579
431.0137 15.02224
431.4958 13.67474
431.9779 12.74365
432.4600 12.23295
432.9421 11.77410
433.4243 11.08485
433.9064 10.19075
434.3885 9.134628
434.8706 7.617310
435.3527 6.645050
435.8348 7.681770
436.3170 9.568596
436.7991 10.26961
437.2812 8.792351
437.7633 6.669281
438.2454 5.205055
438.7275 4.336853
439.2097 3.686119
439.6918 3.174339
440.1739 2.763847
440.6560 2.385391
441.1381 2.021690
441.6202 1.772697
442.1024 1.816559
442.5845 1.906609
443.0666 1.706902
443.5487 1.206055
444.0308 0.7279430
444.5129 0.5382160
444.9951 0.5948490
445.4772 0.4836580
445.9593 1.9840000E-03
446.4414 0.3890910
446.9235 0.4972920
447.4056 0.4272540
447.8878 0.3113860
448.3699 0.1973040
448.8520 0.1013570
449.3341 5.2124001E-02
449.8162 7.2098002E-02
450.2983 7.6468997E-02
450.7805 9.4443999E-02
451.2626 7.2936997E-02
451.7447 0.1132660
452.2268 0.3683010
452.7089 0.4266360
453.1910 7.7904001E-02
453.6732 0.5380630
454.1553 0.8002780
454.6374 0.3902130
455.1195 0.1671070
455.6016 0.3698350
456.0837 0.7241900
456.5659 1.058716
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