#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-04-26 13:42:13 +0300 (Thu, 26 Apr 2018) $
#$Revision: 513 $
#$URL: svn://172.16.1.111/rod/cif/1/00/00/1000065.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000065
loop_
_publ_author_name
'Hill, R. J.'
_publ_section_title
;
 The crystal structure and infrared properties of adamite
;
_journal_name_full               'American Mineralogist'
_journal_page_first              979
_journal_page_last               986
_journal_volume                  61
_journal_year                    1976
_chemical_compound_source        R060593
_chemical_formula_sum            'As H O5 Zn2'
_chemical_name_mineral           Adamite
_space_group_IT_number           58
_symmetry_space_group_name_Hall  '-P 2 2n'
_symmetry_space_group_name_H-M   'P n n m'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_length_a                   8.306
_cell_length_b                   8.524
_cell_length_c                   6.043
_cell_volume                     427.846
_exptl_crystal_density_diffrn    4.451
_cod_original_formula_sum        'As Zn2 O5 H'
_cod_database_code               9000521
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type helium-neon
_raman_measurement_device.excitation_laser_wavelength 780
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 12
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R060593.rod
_rod_data_source.block           3500000
_rod_database.code               1000065
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9000521 COD http://www.crystallography.net/cod/9000521.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
164.8853 0.0000000E+00
165.3674 9.1599002E-02
165.8495 1.390686
166.3316 4.757355
166.8137 8.847992
167.2958 13.05312
167.7780 17.24849
168.2601 21.22409
168.7422 25.04451
169.2243 29.55615
169.7064 34.34982
170.1885 38.65688
170.6707 42.55664
171.1528 46.69083
171.6349 50.85645
172.1170 54.30750
172.5991 57.39445
173.0812 62.34895
173.5634 65.99113
174.0455 66.92111
174.5276 65.45018
175.0097 60.79924
175.4918 55.17619
175.9739 48.89537
176.4561 41.82683
176.9382 33.37985
177.4203 26.03418
177.9024 19.94025
178.3845 14.68259
178.8666 10.24086
179.3488 6.540802
179.8309 3.332138
180.3130 0.2623140
180.7951 3.101807
181.2772 5.150696
181.7593 5.325775
182.2415 4.742401
182.7236 4.213379
183.2057 3.930313
183.6878 3.542984
184.1699 2.523438
184.6520 0.6606290
185.1342 1.565857
185.6163 4.000137
186.0984 6.854248
186.5805 10.68132
187.0626 15.71768
187.5447 20.91490
188.0269 24.11115
188.5090 24.58331
188.9911 26.31319
189.4732 31.17885
189.9553 37.72121
190.4374 43.26245
190.9196 46.88559
191.4017 49.73053
191.8838 53.53413
192.3659 58.30064
192.8480 63.12756
193.3301 67.37698
193.8123 71.29008
194.2944 75.86734
194.7765 81.69057
195.2586 87.86108
195.7407 93.29727
196.2228 97.96893
196.7050 102.7885
197.1871 108.4866
197.6692 115.0275
198.1513 121.6147
198.6334 128.0323
199.1155 134.5206
199.5977 141.1407
200.0798 147.9346
200.5619 155.0416
201.0440 162.5047
201.5261 170.2993
202.0082 178.9386
202.4904 189.3555
202.9725 200.0940
203.4546 210.6114
203.9367 220.7969
204.4188 230.7568
204.9009 240.6077
205.3831 250.4327
205.8652 259.8126
206.3473 269.1441
206.8294 277.7777
207.3115 285.5647
207.7936 292.3281
208.2758 297.6807
208.7579 301.0723
209.2400 302.5019
209.7221 301.5440
210.2042 297.9185
210.6863 292.6093
211.1685 285.6426
211.6506 277.2997
212.1327 268.6732
212.6148 261.3099
213.0969 256.0515
213.5790 250.5329
214.0612 243.5425
214.5433 237.0504
215.0254 232.5122
215.5075 230.3107
215.9896 229.8568
216.4717 230.4181
216.9539 232.3217
217.4360 234.7200
217.9181 236.9520
218.4002 239.9938
218.8823 244.6985
219.3644 251.2610
219.8466 259.6745
220.3287 270.2688
220.8108 283.3825
221.2929 296.9913
221.7750 310.5860
222.2571 324.6427
222.7393 339.4067
223.2214 354.7960
223.7035 371.7906
224.1856 392.2758
224.6677 415.8598
225.1498 439.8892
225.6320 463.9445
226.1141 487.9658
226.5962 512.1920
227.0783 537.1184
227.5604 560.9395
228.0425 583.0470
228.5247 603.2167
229.0068 619.1499
229.4889 630.2755
229.9710 636.3784
230.4531 637.0433
230.9352 632.2882
231.4174 621.3881
231.8995 602.4687
232.3816 577.4320
232.8637 550.8909
233.3458 523.6409
233.8279 496.4471
234.3101 471.3081
234.7922 448.5977
235.2743 428.0161
235.7564 408.4203
236.2385 390.4622
236.7206 375.4736
237.2028 364.6024
237.6849 357.3854
238.1670 351.5996
238.6491 346.5249
239.1312 344.2607
239.6133 345.9132
240.0955 350.5420
240.5776 356.5146
241.0597 362.8145
241.5418 369.6904
242.0239 378.1973
242.5060 388.6847
242.9882 400.6647
243.4703 414.1428
243.9524 428.8096
244.4345 444.3464
244.9166 460.6039
245.3987 477.5438
245.8809 494.7022
246.3630 512.7397
246.8451 530.0791
247.3272 546.1753
247.8093 561.5122
248.2914 576.7266
248.7736 592.2335
249.2557 607.6998
249.7378 621.6580
250.2199 634.6069
250.7020 645.1278
251.1841 653.0094
251.6663 658.4246
252.1484 661.4982
252.6305 662.3105
253.1126 660.9065
253.5947 657.3756
254.0768 651.1978
254.5590 643.1672
255.0411 632.9258
255.5232 621.0601
256.0053 607.6890
256.4874 592.9235
256.9695 577.5596
257.4517 563.5497
257.9338 552.8604
258.4159 541.1567
258.8980 528.2920
259.3801 514.4247
259.8622 499.2039
260.3444 482.5639
260.8265 465.4963
261.3086 449.8887
261.7907 436.0939
262.2728 423.3046
262.7549 412.3221
263.2371 401.8801
263.7192 390.4543
264.2013 377.6541
264.6834 364.8714
265.1655 354.1727
265.6476 346.3625
266.1298 339.1484
266.6119 332.5023
267.0940 326.3908
267.5761 320.7935
268.0582 315.6847
268.5403 311.1602
269.0225 307.3328
269.5046 304.3183
269.9867 301.8651
270.4688 299.7234
270.9509 298.3107
271.4330 298.2039
271.9152 299.4178
272.3973 301.1898
272.8794 303.0551
273.3615 304.9938
273.8436 305.8454
274.3257 305.2900
274.8079 303.8582
275.2900 302.3088
275.7721 300.5829
276.2542 297.5266
276.7363 292.4039
277.2184 284.9383
277.7006 275.4955
278.1827 263.1122
278.6648 249.4486
279.1469 235.4181
279.6290 221.0928
280.1111 206.5236
280.5933 191.6193
281.0754 176.5739
281.5575 161.8371
282.0396 146.7103
282.5217 132.6221
283.0038 120.3258
283.4860 109.7809
283.9681 100.6727
284.4502 93.21199
284.9323 86.94574
285.4144 80.65767
285.8965 74.05197
286.3787 67.97614
286.8608 62.90536
287.3429 58.78036
287.8250 55.39406
288.3071 53.07587
288.7892 50.97734
289.2714 47.73999
289.7535 43.21223
290.2356 38.68811
290.7177 34.65508
291.1998 31.12282
291.6819 28.02637
292.1641 25.39136
292.6462 22.98790
293.1283 20.59795
293.6104 18.27788
294.0925 16.19089
294.5746 14.62479
295.0568 13.30547
295.5389 11.58583
296.0210 9.231812
296.5031 6.963562
296.9852 5.384689
297.4673 4.361694
297.9495 3.662308
298.4316 3.640976
298.9137 3.740997
299.3958 2.941223
299.8779 1.008484
300.3600 0.7998200
300.8422 1.707214
301.3243 1.898209
301.8064 1.550491
302.2885 0.5213470
302.7706 0.8560330
303.2527 2.317444
303.7349 3.887619
304.2170 5.229477
304.6991 5.940720
305.1812 6.445526
305.6633 7.393143
306.1454 9.061340
306.6276 10.67598
307.1097 11.21716
307.5918 10.78316
308.0739 11.20819
308.5560 13.73997
309.0381 16.82976
309.5203 18.59033
310.0024 18.85968
310.4845 19.07191
310.9666 20.27696
311.4487 22.28419
311.9308 24.13455
312.4130 25.53244
312.8951 26.88219
313.3772 28.69672
313.8593 30.88077
314.3414 32.73267
314.8235 33.55211
315.3057 33.79701
315.7878 34.77086
316.2699 36.86488
316.7520 38.99370
317.2341 40.66835
317.7162 41.80466
318.1984 42.03185
318.6805 40.58360
319.1626 38.43918
319.6447 37.18013
320.1268 36.94656
320.6089 36.90614
321.0911 36.83615
321.5732 36.59271
322.0553 35.90692
322.5374 34.56619
323.0195 33.02139
323.5016 31.93283
323.9838 31.30080
324.4659 30.04541
324.9480 27.34755
325.4301 24.08134
325.9122 21.38237
326.3943 19.36281
326.8765 17.48280
327.3586 15.37781
327.8407 13.07108
328.3228 10.70811
328.8049 8.181854
329.2870 5.820816
329.7692 3.890396
330.2513 2.376968
330.7334 1.251724
331.2155 0.6690670
331.6976 0.4578400
332.1797 0.2789760
332.6619 0.1530760
333.1440 0.1333770
333.6261 0.7492980
334.1082 1.647903
334.5903 2.801895
335.0724 4.921326
335.5546 6.954681
336.0367 7.122322
336.5188 5.215492
337.0009 3.471115
337.4830 3.257584
337.9651 4.084808
338.4473 5.046684
338.9294 6.330292
339.4115 7.214897
339.8936 6.843307
340.3757 5.427223
340.8578 4.352058
341.3400 4.157791
341.8221 4.500793
342.3042 4.941284
342.7863 5.573853
343.2684 5.842567
343.7505 5.165146
344.2327 3.933670
344.7148 3.101341
345.1969 2.908844
345.6790 3.040573
346.1611 3.407791
346.6432 3.949867
347.1254 3.925720
347.6075 2.643967
348.0896 0.9339750
348.5717 8.3999999E-05
349.0538 2.5536001E-02
349.5359 0.2786940
350.0181 1.778374
350.5002 4.250465
350.9823 6.301765
351.4644 7.719421
351.9465 8.806770
352.4286 9.718468
352.9108 10.46029
353.3929 10.93382
353.8750 10.77631
354.3571 10.65588
354.8392 12.35179
355.3214 16.69867
355.8035 20.68434
356.2856 22.96321
356.7677 24.19909
357.2498 25.45433
357.7319 26.98174
358.2141 28.86240
358.6962 31.38937
359.1783 34.72252
359.6604 37.73407
360.1425 39.86620
360.6246 41.90742
361.1068 44.72678
361.5889 48.37138
362.0710 51.99208
362.5531 54.84432
363.0352 56.94411
363.5173 59.33447
363.9995 61.83797
364.4816 64.77915
364.9637 68.46436
365.4458 72.71535
365.9279 77.07124
366.4100 81.27336
366.8922 85.45224
367.3743 89.98983
367.8564 95.06129
368.3385 100.2176
368.8206 104.9290
369.3027 109.9025
369.7849 116.3725
370.2670 124.5635
370.7491 132.9556
371.2312 139.4240
371.7133 143.3110
372.1954 146.8984
372.6776 150.1462
373.1597 153.1444
373.6418 156.5276
374.1239 159.8879
374.6060 161.8701
375.0881 161.3594
375.5703 158.3976
376.0524 154.5564
376.5345 150.2049
377.0166 144.6193
377.4987 137.1607
377.9808 128.4670
378.4630 119.2237
378.9451 109.7313
379.4272 100.2429
379.9093 91.39050
380.3914 83.35936
380.8735 75.70522
381.3557 68.12634
381.8378 61.09173
382.3199 54.90930
382.8020 49.56458
383.2841 44.83614
383.7662 40.51287
384.2484 36.60104
384.7305 33.11064
385.2126 30.37334
385.6947 27.75222
386.1768 24.97430
386.6589 22.16025
387.1411 19.56046
387.6232 17.31594
388.1053 15.38107
388.5874 13.52509
389.0695 11.30939
389.5516 10.08093
390.0338 11.11508
390.5159 12.58087
390.9980 12.60350
391.4801 10.66261
391.9622 8.127342
392.4443 6.704453
392.9265 6.457436
393.4086 6.069572
393.8907 5.358704
394.3728 4.869873
394.8549 4.982162
395.3370 5.461601
395.8192 5.696869
396.3013 5.111176
396.7834 3.991714
397.2655 3.410507
397.7476 3.598106
398.2297 4.077835
398.7119 4.420387
399.1940 4.844643
399.6761 5.794685
400.1582 7.621170
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404.0151 17.29743
404.4973 19.08289
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405.4615 23.63167
405.9436 25.45021
406.4257 26.57350
406.9078 27.32034
407.3900 27.56241
407.8721 27.68234
408.3542 29.18510
408.8363 33.59154
409.3184 38.01007
409.8005 40.05820
410.2827 40.43137
410.7648 41.66292
411.2469 45.04877
411.7290 49.55571
412.2111 52.74341
412.6932 53.97762
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413.6575 58.56175
414.1396 61.95457
414.6217 65.27032
415.1038 68.37961
415.5859 71.37527
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417.0323 80.17844
417.5144 83.54752
417.9965 86.35815
418.4786 88.04111
418.9608 88.87242
419.4429 89.46481
419.9250 90.14220
420.4071 90.69041
420.8892 90.51331
421.3713 89.40494
421.8535 87.79241
422.3356 86.13633
422.8177 83.72541
423.2998 79.68289
423.7819 74.09807
424.2640 68.12364
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425.2283 58.71214
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430.0494 14.98006
430.5316 13.20958
431.0137 10.34223
431.4958 7.392731
431.9779 4.962379
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432.9421 1.626541
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434.3885 1.194901
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441.6202 0.8768920
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442.5845 0.2497180
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455.1195 31.76303
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457.0480 36.22952
457.5301 38.94882
458.0122 40.93350
458.4943 42.20341
458.9764 43.39330
459.4586 44.40649
459.9407 45.51538
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461.3870 49.94215
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462.3513 53.15862
462.8334 55.71999
463.3155 59.07437
463.7976 61.77005
464.2797 62.90697
464.7618 63.73667
465.2440 65.78826
465.7261 69.04044
466.2082 72.82872
466.6903 77.67115
467.1724 82.54859
467.6545 85.75999
468.1367 87.30241
468.6188 89.42400
469.1009 93.79542
469.5830 99.89778
470.0651 105.2016
470.5472 108.9426
471.0294 112.9240
471.5115 117.9150
471.9936 123.2580
472.4757 128.1878
472.9578 132.4867
473.4399 136.3422
473.9221 139.8863
474.4042 142.9465
474.8863 146.7140
475.3684 151.7585
475.8505 156.8472
476.3326 161.8904
476.8148 166.5803
477.2969 170.3808
477.7790 172.9903
478.2611 174.9040
478.7432 177.1037
479.2253 179.6427
479.7075 182.2981
480.1896 185.8897
480.6717 188.8796
481.1538 190.1116
481.6359 189.8326
482.1180 189.2933
482.6002 189.0621
483.0823 189.2661
483.5644 190.5104
484.0465 193.1627
484.5286 195.4809
485.0107 196.4227
485.4929 196.7430
485.9750 197.1844
486.4571 197.7232
486.9392 198.8706
487.4213 201.1615
487.9034 204.2571
488.3856 207.3964
488.8677 210.4712
489.3498 213.6921
489.8319 217.4322
490.3140 221.5758
490.7961 224.8257
491.2783 227.0703
491.7604 228.5690
492.2425 229.7694
492.7246 230.2329
493.2067 229.2669
493.6888 226.6486
494.1710 222.3328
494.6531 216.1888
495.1352 207.7300
495.6173 199.0086
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