#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-04-26 13:42:21 +0300 (Thu, 26 Apr 2018) $
#$Revision: 515 $
#$URL: svn://172.16.1.111/rod/cif/1/00/00/1000067.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000067
loop_
_publ_author_name
'Olmi, F.'
'Sabelli, C.'
_publ_section_title
;
 Brizzite, NaSbO3, a new mineral from the Cetine mine (Tuscany, Italy):
 description and crystal structure Locality: Cetine mine, Tuscany, Italy
;
_journal_name_full               'European Journal of Mineralogy'
_journal_page_first              667
_journal_page_last               672
_journal_volume                  6
_journal_year                    1994
_chemical_compound_source        R060611
_chemical_formula_sum            'Na O3 Sb'
_chemical_name_mineral           Brizziite
_space_group_IT_number           148
_symmetry_space_group_name_Hall  '-R 3'
_symmetry_space_group_name_H-M   'R -3 :H'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                120
_cell_length_a                   5.301
_cell_length_b                   5.301
_cell_length_c                   15.932
_cell_volume                     387.719
_exptl_crystal_density_diffrn    4.953
_cod_original_sg_symbol_H-M      'R -3'
_cod_original_formula_sum        'Na Sb O3'
_cod_database_code               9005220
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type helium-neon
_raman_measurement_device.excitation_laser_wavelength 780
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 12
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R060611.rod
_rod_data_source.block           3500000
_rod_database.code               1000067
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9005220 COD http://www.crystallography.net/cod/9005220.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
93.97052 0.0000000E+00
94.45264 1.889160
94.93475 5.346680
95.41687 6.275879
95.89898 6.847656
96.38110 9.833496
96.86321 12.16113
97.34533 13.54053
97.82745 3.467285
98.30956 2.147949
98.79168 1.443848
99.27380 6.352051
99.75591 7.761719
100.2380 7.239746
100.7201 10.96484
101.2023 23.44727
101.6844 42.89355
102.1665 59.92920
102.6486 72.25049
103.1307 83.09375
103.6128 94.82227
104.0950 106.9453
104.5771 120.6924
105.0592 135.9717
105.5413 152.1157
106.0234 168.7068
106.5055 184.8613
106.9877 201.1711
107.4698 220.3394
107.9519 246.8022
108.4340 270.2725
108.9161 285.4753
109.3982 293.8411
109.8804 299.5010
110.3625 306.6919
110.8446 315.8643
111.3267 324.2886
111.8088 331.5303
112.2909 338.1550
112.7731 344.2546
113.2552 349.9141
113.7373 354.9905
114.2194 359.9783
114.7015 365.6562
115.1836 370.3528
115.6658 374.9368
116.1479 377.8933
116.6300 377.3835
117.1121 372.8372
117.5942 365.8164
118.0763 360.2803
118.5584 357.4465
119.0406 354.6750
119.5227 351.2803
120.0048 346.8584
120.4869 341.9036
120.9690 339.2490
121.4511 340.0085
121.9333 342.0903
122.4154 343.6616
122.8975 346.0425
123.3796 348.8330
123.8617 352.3584
124.3438 351.6836
124.8260 339.0686
125.3081 321.4060
125.7902 305.1248
126.2723 292.6882
126.7544 282.5989
127.2365 272.1909
127.7187 260.8469
128.2008 250.2222
128.6829 241.3652
129.1650 233.3408
129.6471 224.9153
130.1292 215.1577
130.6114 204.1753
131.0935 192.8127
131.5756 178.6924
132.0577 166.2869
132.5398 158.0149
133.0219 152.8511
133.5041 148.2502
133.9862 141.9922
134.4683 133.8369
134.9504 125.8921
135.4325 117.8420
135.9146 110.0193
136.3968 102.4504
136.8789 95.17676
137.3610 88.53613
137.8431 83.32764
138.3252 79.91113
138.8073 75.98267
139.2895 70.97656
139.7716 65.49146
140.2537 60.30518
140.7358 55.60791
141.2179 51.09399
141.7000 47.10449
142.1821 43.66797
142.6643 39.23584
143.1464 32.51245
143.6285 24.03418
144.1106 15.91821
144.5927 7.858643
145.0748 1.357422
145.5570 1.883301
146.0391 1.818848
146.5212 1.549316
147.0033 3.810547
147.4854 8.827148
147.9675 14.14697
148.4497 21.16626
148.9318 27.23828
149.4139 30.18066
149.8960 29.66309
150.3781 28.01099
150.8602 28.70557
151.3424 32.98096
151.8245 31.73389
152.3066 30.08081
152.7887 28.07422
153.2708 26.10083
153.7529 24.22241
154.2351 21.82422
154.7172 17.26270
155.1993 7.695313
155.6814 0.8073730
156.1635 7.856201
156.6456 13.80469
157.1278 18.80371
157.6099 22.89062
158.0920 26.23999
158.5741 29.64258
159.0562 34.76782
159.5383 38.19751
160.0205 37.63135
160.5026 34.54565
160.9847 32.28345
161.4668 32.78149
161.9489 35.69482
162.4310 38.93286
162.9131 43.28418
163.3953 47.21167
163.8774 49.37598
164.3595 49.97241
164.8416 50.98291
165.3237 53.96191
165.8058 58.18750
166.2880 61.89600
166.7701 64.94116
167.2522 67.36450
167.7343 68.80249
168.2164 68.90845
168.6985 69.72534
169.1807 73.47046
169.6628 78.42163
170.1449 82.43286
170.6270 84.25586
171.1091 84.91650
171.5912 86.79443
172.0734 90.28979
172.5555 94.45044
173.0376 99.79834
173.5197 105.2893
174.0018 109.1899
174.4839 109.8914
174.9661 108.2490
175.4482 109.5869
175.9303 117.1189
176.4124 124.2815
176.8945 129.2405
177.3766 132.5823
177.8588 135.4473
178.3409 138.6084
178.8230 142.0613
179.3051 145.8430
179.7872 150.8352
180.2693 155.2864
180.7515 158.4878
181.2336 160.6509
181.7157 162.3611
182.1978 164.0598
182.6799 165.7214
183.1620 167.8032
183.6441 170.2957
184.1263 173.0105
184.6084 176.6702
185.0905 180.8472
185.5726 183.6062
186.0547 182.6643
186.5368 177.2903
187.0190 175.2720
187.5011 179.5708
187.9832 185.0059
188.4653 187.8582
188.9474 187.7334
189.4296 186.3701
189.9117 185.2505
190.3938 184.3992
190.8759 183.4246
191.3580 181.2449
191.8401 179.4172
192.3223 180.4863
192.8044 185.3120
193.2865 189.8962
193.7686 188.7622
194.2507 183.7637
194.7328 180.7449
195.2150 182.7075
195.6971 187.6543
196.1792 191.8879
196.6613 195.3313
197.1434 197.4519
197.6255 197.3811
198.1077 195.7390
198.5898 194.0464
199.0719 193.0427
199.5540 192.6172
200.0361 192.3076
200.5182 192.1599
201.0004 191.9871
201.4825 191.6868
201.9646 191.1917
202.4467 190.3669
202.9288 189.2417
203.4109 187.9478
203.8930 186.3523
204.3752 184.4565
204.8573 182.0967
205.3394 179.1313
205.8215 175.5447
206.3036 171.1626
206.7857 165.7583
207.2679 159.4355
207.7500 154.4133
208.2321 152.8123
208.7142 150.6179
209.1963 146.0127
209.6784 139.7253
210.1606 133.2031
210.6427 127.6985
211.1248 123.3110
211.6069 119.1089
212.0890 114.7375
212.5711 111.0503
213.0533 108.9468
213.5354 108.1194
214.0175 107.6311
214.4996 106.7053
214.9817 105.3201
215.4638 103.0237
215.9460 98.64575
216.4281 94.56519
216.9102 92.25562
217.3923 91.50830
217.8744 90.96680
218.3565 89.46338
218.8387 86.90332
219.3208 83.94775
219.8029 79.63525
220.2850 75.78857
220.7671 73.77051
221.2492 73.48584
221.7314 73.56030
222.2135 72.70679
222.6956 70.88330
223.1777 70.21802
223.6598 72.36572
224.1419 74.47021
224.6240 74.01245
225.1062 70.96387
225.5883 67.72852
226.0704 66.79004
226.5525 67.58667
227.0346 65.90601
227.5167 57.54614
227.9989 49.07275
228.4810 47.79834
228.9631 54.26611
229.4452 60.93188
229.9273 61.72729
230.4094 58.44409
230.8916 56.14258
231.3737 56.73096
231.8558 58.03833
232.3379 57.40845
232.8200 54.57397
233.3021 51.59644
233.7843 50.24194
234.2664 49.50952
234.7485 47.77515
235.2306 44.06567
235.7127 39.64062
236.1948 36.02466
236.6770 33.17578
237.1591 31.28247
237.6412 31.28345
238.1233 32.04712
238.6054 32.29590
239.0875 31.39380
239.5697 30.15869
240.0518 29.99756
240.5339 31.25244
241.0160 32.50879
241.4981 32.48120
241.9802 32.49365
242.4624 34.10889
242.9445 38.11743
243.4266 43.08105
243.9087 46.45825
244.3908 47.68188
244.8729 48.73511
245.3550 50.62207
245.8372 52.39355
246.3193 52.57764
246.8014 50.52051
247.2835 48.46484
247.7656 51.05518
248.2477 61.37866
248.7299 68.86279
249.2120 70.30493
249.6941 69.36987
250.1762 68.50537
250.6583 68.51855
251.1404 69.09863
251.6226 69.84912
252.1047 71.17676
252.5868 71.66528
253.0689 69.87158
253.5510 68.24048
254.0331 69.05469
254.5153 72.67358
254.9974 77.02734
255.4795 78.86890
255.9616 76.92212
256.4437 75.08325
256.9258 71.90210
257.4080 69.90674
257.8901 71.46069
258.3722 76.63037
258.8543 83.00488
259.3364 87.32886
259.8185 88.79199
260.3007 90.11401
260.7828 91.04883
261.2649 92.06616
261.7470 93.63989
262.2291 95.70703
262.7112 97.62524
263.1934 98.51172
263.6755 97.65894
264.1576 98.44702
264.6397 102.7249
265.1218 106.7693
265.6039 108.1436
266.0861 107.0449
266.5682 105.4670
267.0503 105.3811
267.5324 107.0850
268.0145 108.4226
268.4966 109.2000
268.9788 109.8735
269.4609 110.7178
269.9430 111.6768
270.4251 112.4036
270.9072 112.4705
271.3893 111.8120
271.8715 112.6597
272.3536 116.6255
272.8357 120.1768
273.3178 121.7383
273.7999 121.6157
274.2820 120.6792
274.7642 119.2656
275.2463 117.5542
275.7284 118.0269
276.2105 122.9392
276.6926 127.0503
277.1747 127.9028
277.6568 126.6057
278.1389 125.6758
278.6211 126.4661
279.1032 128.6704
279.5853 131.0669
280.0674 133.9126
280.5495 136.6277
281.0316 138.9866
281.5138 141.1372
281.9959 143.5452
282.4780 146.5420
282.9601 149.4946
283.4422 150.4414
283.9243 147.8098
284.4065 146.4658
284.8886 148.4172
285.3707 151.9929
285.8528 154.7305
286.3349 155.8179
286.8170 156.0544
287.2992 156.8262
287.7813 158.5237
288.2634 159.4092
288.7455 157.9749
289.2276 156.0735
289.7097 156.3320
290.1919 159.4204
290.6740 163.2122
291.1561 164.7522
291.6382 163.5129
292.1203 164.3123
292.6024 169.7412
293.0846 176.2598
293.5667 179.8772
294.0488 180.1267
294.5309 180.3044
295.0130 183.9128
295.4951 191.0352
295.9773 196.2646
296.4594 197.2593
296.9415 197.5938
297.4236 200.1821
297.9057 204.9666
298.3878 210.0051
298.8700 213.9216
299.3521 217.0249
299.8342 221.0830
300.3163 226.3059
300.7984 232.1362
301.2805 238.4189
301.7627 244.8762
302.2448 251.0464
302.7269 256.9553
303.2090 262.5837
303.6911 267.5393
304.1732 271.0295
304.6554 274.8914
305.1375 280.4006
305.6196 286.8809
306.1017 292.5813
306.5838 296.7000
307.0659 300.2742
307.5481 305.2378
308.0302 311.6426
308.5123 317.8159
308.9944 323.9795
309.4765 329.8872
309.9586 334.2119
310.4408 336.0378
310.9229 336.9233
311.4050 339.9436
311.8871 345.6479
312.3692 350.1538
312.8513 351.5786
313.3335 351.9016
313.8156 354.0095
314.2977 358.3967
314.7798 362.1621
315.2619 362.5315
315.7440 359.5432
316.2262 355.7043
316.7083 350.2896
317.1904 344.7283
317.6725 339.8430
318.1546 335.7192
318.6367 332.9893
319.1188 332.4568
319.6010 333.7244
320.0831 334.4126
320.5652 334.2029
321.0473 333.7969
321.5294 333.9241
322.0115 334.2883
322.4937 334.5356
322.9758 334.5298
323.4579 334.7090
323.9400 336.0354
324.4221 339.1689
324.9042 341.1384
325.3864 340.7644
325.8685 338.7920
326.3506 336.5000
326.8327 334.3157
327.3148 331.3940
327.7969 325.7329
328.2791 316.5974
328.7612 309.6204
329.2433 309.0200
329.7254 309.5874
330.2075 304.7039
330.6896 293.2561
331.1718 279.6504
331.6539 267.7114
332.1360 257.8303
332.6181 249.1340
333.1002 243.5574
333.5823 237.7275
334.0645 228.3062
334.5466 215.7415
335.0287 203.8015
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335.9929 190.1431
336.4750 182.4775
336.9572 169.9084
337.4393 157.9316
337.9214 149.1643
338.4035 142.7212
338.8856 136.6750
339.3677 130.2207
339.8499 123.4060
340.3320 116.2886
340.8141 108.2600
341.2962 101.0486
341.7783 95.92773
342.2604 91.45850
342.7426 85.56030
343.2247 77.66211
343.7068 69.18506
344.1889 62.01733
344.6710 56.39502
345.1531 51.93164
345.6353 49.88696
346.1174 48.18799
346.5995 45.38354
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347.5637 36.40381
348.0458 30.76465
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349.0101 18.95239
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351.4207 5.978760
351.9028 5.535156
352.3849 5.313965
352.8670 3.722656
353.3491 1.270020
353.8312 5.097656
354.3134 6.760986
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355.2776 6.954346
355.7597 6.477783
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356.7239 7.588135
357.2061 11.37817
357.6882 14.41406
358.1703 17.33008
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365.4020 20.85449
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376.9728 34.18091
377.4549 26.87622
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382.2761 19.66260
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388.5436 5.516113
389.0257 6.7139000E-02
389.5078 10.24463
389.9900 20.30151
390.4721 25.54370
390.9542 26.54224
391.4363 27.58276
391.9184 29.92969
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392.8827 36.77612
393.3648 41.23120
393.8469 44.18384
394.3290 43.33423
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395.2932 40.66113
395.7754 43.33276
396.2575 46.47217
396.7396 47.99194
397.2217 47.99561
397.7038 48.18188
398.1859 49.05591
398.6681 49.78540
399.1501 49.27100
399.6323 48.01538
400.1144 47.89111
400.5965 49.94312
401.0786 53.53882
401.5607 56.95166
402.0428 60.66821
402.5250 63.39600
403.0071 64.06445
403.4892 63.99731
403.9713 64.66943
404.4534 66.40820
404.9355 68.73608
405.4177 71.21094
405.8998 73.99072
406.3819 75.79248
406.8640 75.95142
407.3461 75.85767
407.8282 75.51270
408.3104 75.46265
408.7925 77.18018
409.2746 81.90503
409.7567 88.51294
410.2388 91.76392
410.7209 87.87695
411.2031 84.99463
411.6852 84.99878
412.1673 85.86328
412.6494 85.45288
413.1315 83.29395
413.6136 80.64648
414.0958 79.16455
414.5779 79.06348
415.0600 78.69678
415.5421 78.73730
416.0242 77.97144
416.5063 75.66748
416.9885 72.39624
417.4706 69.15137
417.9527 66.24146
418.4348 63.71362
418.9169 62.51416
419.3990 63.84937
419.8812 64.25000
420.3633 61.94727
420.8454 58.75977
421.3275 56.56299
421.8096 55.79443
422.2917 54.56152
422.7739 49.71753
423.2560 41.72217
423.7381 38.07227
424.2202 42.49463
424.7023 47.31152
425.1844 46.38696
425.6666 41.25830
426.1487 36.87231
426.6308 34.74512
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