#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-04-26 13:42:33 +0300 (Thu, 26 Apr 2018) $
#$Revision: 518 $
#$URL: svn://172.16.1.111/rod/cif/1/00/00/1000070.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000070
loop_
_publ_author_name
'Ercit, T. S.'
_publ_section_title
;
 Caryinite revisited Locality: Langban, Sweden
;
_journal_name_full               'Mineralogical Magazine'
_journal_page_first              721
_journal_page_last               727
_journal_paper_doi               10.1180/minmag.1993.057.389.16
_journal_volume                  57
_journal_year                    1993
_chemical_compound_source        R060663
_chemical_formula_sum
'As2.892 Ca1.91 Mg0.56 Mn1.77 Na1.376 O12 P0.09 Pb0.384 V0.018'
_chemical_name_mineral           Caryinite
_space_group_IT_number           15
_symmetry_space_group_name_Hall  '-I 2ya'
_symmetry_space_group_name_H-M   'I 1 2/a 1'
_cell_angle_alpha                90
_cell_angle_beta                 98.97
_cell_angle_gamma                90
_cell_length_a                   6.855
_cell_length_b                   13.147
_cell_length_c                   11.479
_cell_volume                     1021.866
_exptl_crystal_density_diffrn    4.621
_cod_original_formula_sum
'Ca1.91 Na1.376 Pb.384 Mn1.77 Mg.56 (As2.892 P.09 V.018) O12'
_cod_database_code               9009485
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type helium-neon
_raman_measurement_device.excitation_laser_wavelength 780
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 12
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R060663.rod
_rod_data_source.block           3500000
_rod_database.code               1000070
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9009485 COD http://www.crystallography.net/cod/9009485.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
95.89898 0.0000000E+00
96.38110 1.297638
96.86321 2.678101
97.34533 3.177551
97.82745 1.675201
98.30956 0.4133000
98.79168 1.6357001E-02
99.27380 0.1039430
99.75591 0.5639340
100.2380 1.364838
100.7201 1.993835
101.2023 1.904358
101.6844 1.210327
102.1665 0.9544370
102.6486 1.695343
103.1307 2.862030
103.6128 3.910126
104.0950 4.826294
104.5771 5.619965
105.0592 5.914795
105.5413 6.128876
106.0234 6.511597
106.5055 7.390381
106.9877 8.757904
107.4698 10.09735
107.9519 11.69122
108.4340 13.38635
108.9161 14.59079
109.3982 14.23862
109.8804 13.02731
110.3625 11.82718
110.8446 10.64899
111.3267 9.610199
111.8088 8.393524
112.2909 7.358734
112.7731 6.881165
113.2552 7.067078
113.7373 7.493591
114.2194 7.443817
114.7015 6.322449
115.1836 5.723022
115.6658 6.102417
116.1479 6.746826
116.6300 7.109711
117.1121 6.945679
117.5942 6.312347
118.0763 5.312256
118.5584 3.783386
119.0406 2.348145
119.5227 1.161072
120.0048 0.1701970
120.4869 0.6960750
120.9690 1.561646
121.4511 2.198853
121.9333 2.243195
122.4154 1.471649
122.8975 0.5294490
123.3796 3.0425999E-02
123.8617 0.1597290
124.3438 0.2883000
124.8260 0.6941220
125.3081 1.099213
125.7902 1.271179
126.2723 1.029358
126.7544 0.5920720
127.2365 0.4585880
127.7187 0.6145020
128.2008 1.088562
128.6829 2.072906
129.1650 3.252014
129.6471 4.263580
130.1292 4.846298
130.6114 5.026306
131.0935 5.233658
131.5756 5.284851
132.0577 5.514832
132.5398 6.216965
133.0219 7.193619
133.5041 7.995880
133.9862 8.178482
134.4683 7.581223
134.9504 7.362549
135.4325 7.799332
135.9146 8.325363
136.3968 8.531815
136.8789 8.414627
137.3610 8.327179
137.8431 8.694992
138.3252 9.619614
138.8073 10.59676
139.2895 11.73096
139.7716 12.89943
140.2537 13.98985
140.7358 15.02791
141.2179 15.83792
141.7000 15.96432
142.1821 15.44661
142.6643 15.12761
143.1464 15.49796
143.6285 16.38403
144.1106 17.14217
144.5927 17.53664
145.0748 17.87517
145.5570 18.52032
146.0391 19.46962
146.5212 20.30396
147.0033 20.56691
147.4854 20.18558
147.9675 19.94716
148.4497 20.12343
148.9318 20.41002
149.4139 20.66666
149.8960 20.86078
150.3781 21.02486
150.8602 21.31567
151.3424 22.15532
151.8245 22.11568
152.3066 20.39949
152.7887 18.31198
153.2708 16.92305
153.7529 17.27986
154.2351 18.25005
154.7172 18.70233
155.1993 17.99615
155.6814 17.50677
156.1635 17.58449
156.6456 17.83043
157.1278 17.71884
157.6099 16.96974
158.0920 15.77840
158.5741 14.97691
159.0562 14.87415
159.5383 14.73691
160.0205 14.24100
160.5026 13.57816
160.9847 13.22617
161.4668 13.54314
161.9489 14.33505
162.4310 14.70827
162.9131 14.33087
163.3953 13.88945
163.8774 13.89206
164.3595 14.28421
164.8416 14.48743
165.3237 13.99243
165.8058 13.08194
166.2880 12.42532
166.7701 12.16222
167.2522 12.11047
167.7343 12.08141
168.2164 12.06909
168.6985 12.12062
169.1807 12.34375
169.6628 12.62825
170.1449 12.83014
170.6270 12.83620
171.1091 12.77908
171.5912 12.98161
172.0734 13.59222
172.5555 14.18094
173.0376 14.65236
173.5197 15.00305
174.0018 15.19853
174.4839 15.17270
174.9661 14.97349
175.4482 14.91836
175.9303 15.15067
176.4124 15.37009
176.8945 15.41231
177.3766 15.38449
177.8588 15.48154
178.3409 15.83531
178.8230 16.44362
179.3051 16.98323
179.7872 17.36069
180.2693 17.88091
180.7515 18.87849
181.2336 20.10698
181.7157 20.96191
182.1978 20.87134
182.6799 19.67146
183.1620 19.21846
183.6441 19.90199
184.1263 20.77908
184.6084 21.47072
185.0905 21.94089
185.5726 22.25298
186.0547 22.39038
186.5368 22.30669
187.0190 22.76691
187.5011 24.14754
187.9832 25.76729
188.4653 27.23404
188.9474 28.48486
189.4296 29.47144
189.9117 30.10826
190.3938 30.39252
190.8759 30.51707
191.3580 30.10303
191.8401 29.72307
192.3223 30.20462
192.8044 31.79115
193.2865 33.44116
193.7686 33.93982
194.2507 33.62781
194.7328 33.48097
195.2150 33.85307
195.6971 34.58337
196.1792 35.38818
196.6613 36.28987
197.1434 37.16034
197.6255 37.85291
198.1077 38.43471
198.5898 39.07298
199.0719 40.00713
199.5540 41.11116
200.0361 41.77977
200.5182 41.65216
201.0004 41.54121
201.4825 41.83954
201.9646 42.50229
202.4467 43.41411
202.9288 44.61386
203.4109 46.02481
203.8930 46.96175
204.3752 47.02724
204.8573 47.05457
205.3394 47.35167
205.8215 47.86009
206.3036 48.39618
206.7857 48.83658
207.2679 49.18747
207.7500 49.58618
208.2321 50.06921
208.7142 50.58360
209.1963 51.06705
209.6784 51.52744
210.1606 52.03168
210.6427 52.71571
211.1248 53.64328
211.6069 54.22607
212.0890 54.13670
212.5711 54.07956
213.0533 54.37489
213.5354 54.98964
214.0175 55.71037
214.4996 56.29994
214.9817 56.68948
215.4638 56.79706
215.9460 56.35835
216.4281 56.00420
216.9102 56.13417
217.3923 56.67879
217.8744 57.25177
218.3565 57.50510
218.8387 57.35564
219.3208 56.97624
219.8029 56.28957
220.2850 55.58722
220.7671 54.97318
221.2492 54.42097
221.7314 53.92873
222.2135 53.60320
222.6956 53.51794
223.1777 53.21925
223.6598 52.39906
224.1419 51.48129
224.6240 50.85637
225.1062 50.54004
225.5883 50.20206
226.0704 49.53027
226.5525 48.61763
227.0346 47.94481
227.5167 47.78697
227.9989 47.67624
228.4810 47.12576
228.9631 46.11862
229.4452 45.18576
229.9273 44.90317
230.4094 44.91235
230.8916 44.36308
231.3737 42.65675
231.8558 40.66472
232.3379 39.35591
232.8200 38.77458
233.3021 38.38551
233.7843 38.08888
234.2664 37.77948
234.7485 37.19666
235.2306 36.12334
235.7127 34.80452
236.1948 33.51929
236.6770 32.22978
237.1591 31.21890
237.6412 30.88165
238.1233 30.78458
238.6054 30.48474
239.0875 29.82216
239.5697 28.96083
240.0518 28.10489
240.5339 27.19504
241.0160 26.45911
241.4981 26.22293
241.9802 26.11217
242.4624 25.72134
242.9445 24.87051
243.4266 23.86586
243.9087 23.26457
244.3908 23.23958
244.8729 23.08353
245.3550 22.46394
245.8372 21.73697
246.3193 21.22649
246.8014 21.04701
247.2835 21.00084
247.7656 20.77834
248.2477 20.39893
248.7299 19.76796
249.2120 18.46791
249.6941 17.15987
250.1762 16.45990
250.6583 16.54207
251.1404 16.94215
251.6226 16.86621
252.1047 16.07632
252.5868 15.32887
253.0689 14.72951
253.5510 14.17818
254.0331 13.58958
254.5153 12.94266
254.9974 12.28734
255.4795 11.70503
255.9616 11.23358
256.4437 10.76500
256.9258 10.14406
257.4080 9.618423
257.8901 9.483704
258.3722 9.724213
258.8543 9.948715
259.3364 9.542938
259.8185 7.964035
260.3007 7.168228
260.7828 7.828384
261.2649 8.579880
261.7470 8.501648
262.2291 7.553192
262.7112 6.370560
263.1934 5.701645
263.6755 5.761276
264.1576 5.556793
264.6397 4.975662
265.1218 4.279007
265.6039 3.467422
266.0861 2.629044
266.5682 2.006561
267.0503 1.873520
267.5324 2.332397
268.0145 2.635864
268.4966 2.872635
268.9788 2.913345
269.4609 2.654327
269.9430 2.126724
270.4251 1.403198
270.9072 0.4758300
271.3893 0.6789700
271.8715 1.193039
272.3536 0.5696260
272.8357 5.7510000E-02
273.3178 0.1802520
273.7999 0.1003420
274.2820 0.4597470
274.7642 0.7149510
275.2463 0.8505400
275.7284 0.6532140
276.2105 0.3998570
276.6926 1.147247
277.1747 0.9443050
277.6568 0.1382290
278.1389 0.4443660
278.6211 0.3038790
279.1032 0.3266140
279.5853 0.4293370
280.0674 0.5648500
280.5495 1.307465
281.0316 1.311783
281.5138 0.8557280
281.9959 0.3836820
282.4780 6.1843999E-02
282.9601 9.2666999E-02
283.4422 3.4637000E-02
283.9243 0.6464080
284.4065 1.108032
284.8886 1.168442
285.3707 1.032883
285.8528 1.066422
286.3349 1.417206
286.8170 1.777237
287.2992 1.511612
287.7813 0.3375550
288.2634 0.4364010
288.7455 0.2850190
289.2276 0.2518310
289.7097 0.4769900
290.1919 0.2214360
290.6740 9.0469003E-02
291.1561 0.1385190
291.6382 1.024170
292.1203 1.531952
292.6024 1.220337
293.0846 0.6779630
293.5667 0.5389560
294.0488 0.8742980
294.5309 1.225189
295.0130 1.121246
295.4951 0.5496220
295.9773 0.1716920
296.4594 0.1421200
296.9415 0.2224120
297.4236 0.2047420
297.9057 9.7900003E-02
298.3878 6.1691001E-02
298.8700 0.1980130
299.3521 0.5157470
299.8342 0.9432370
300.3163 1.790039
300.7984 2.475449
301.2805 2.521759
301.7627 2.053802
302.2448 1.638214
302.7269 1.551117
303.2090 1.737335
303.6911 1.983765
304.1732 2.289001
304.6554 2.636414
305.1375 3.095795
305.6196 3.596069
306.1017 3.937286
306.5838 4.021606
307.0659 3.964478
307.5481 3.994934
308.0302 4.150482
308.5123 4.209869
308.9944 4.018768
309.4765 3.705048
309.9586 3.522736
310.4408 3.562439
310.9229 3.650818
311.4050 3.531616
311.8871 3.193085
312.3692 2.964539
312.8513 3.040405
313.3335 3.201904
313.8156 3.227814
314.2977 3.095245
314.7798 2.746033
315.2619 2.045044
315.7440 0.9965210
316.2262 2.6245000E-02
316.7083 1.088165
317.1904 2.031494
317.6725 2.582275
318.1546 2.795288
318.6367 3.155579
319.1188 3.975830
319.6010 5.178864
320.0831 6.373444
320.5652 7.608124
321.0473 8.790588
321.5294 9.860260
322.0115 10.83463
322.4937 11.83917
322.9758 12.93448
323.4579 14.06693
323.9400 15.05121
324.4221 15.84818
324.9042 16.66788
325.3864 17.68594
325.8685 18.78619
326.3506 19.78342
326.8327 20.61603
327.3148 21.30701
327.7969 21.89267
328.2791 22.37460
328.7612 22.70300
329.2433 22.95007
329.7254 23.00769
330.2075 22.70978
330.6896 22.01611
331.1718 21.18994
331.6539 20.51169
332.1360 19.98987
332.6181 19.29898
333.1002 18.17651
333.5823 17.10376
334.0645 16.45474
334.5466 16.20761
335.0287 16.24777
335.5108 16.67041
335.9929 17.30188
336.4750 16.96783
336.9572 14.91605
337.4393 12.84705
337.9214 11.45242
338.4035 10.54358
338.8856 9.663544
339.3677 8.599731
339.8499 7.469116
340.3320 6.583313
340.8141 5.969513
341.2962 5.458557
341.7783 4.949554
342.2604 4.522156
342.7426 4.330109
343.2247 4.419708
343.7068 4.624573
344.1889 4.679291
344.6710 4.426056
345.1531 4.586151
345.6353 5.596893
346.1174 6.768402
346.5995 7.445709
347.0816 7.616272
347.5637 7.841736
348.0458 8.620880
348.5280 9.991089
349.0101 11.40775
349.4922 12.75491
349.9743 14.21231
350.4564 16.00027
350.9385 17.98514
351.4207 19.76086
351.9028 21.00934
352.3849 21.98224
352.8670 23.83939
353.3491 27.41473
353.8312 30.85568
354.3134 33.76117
354.7955 36.46408
355.2776 39.37769
355.7597 42.64334
356.2418 46.12854
356.7239 49.63394
357.2061 53.04910
357.6882 56.72153
358.1703 61.02472
358.6524 65.26624
359.1345 68.97244
359.6166 72.14188
360.0987 74.99908
360.5808 77.77426
361.0630 80.47165
361.5451 82.93387
362.0272 85.20929
362.5093 87.20654
362.9914 89.04645
363.4735 90.57294
363.9557 91.44568
364.4378 91.44806
364.9199 90.72546
365.4020 89.87402
365.8841 89.04007
366.3662 87.83023
366.8484 86.13605
367.3305 84.12296
367.8126 81.80591
368.2947 79.23056
368.7768 76.70010
369.2589 74.75598
369.7411 73.71069
370.2232 72.42572
370.7053 70.34650
371.1874 68.44440
371.6695 67.20660
372.1516 66.65134
372.6338 66.53229
373.1159 66.69370
373.5980 67.12946
374.0801 67.61807
374.5622 67.83655
375.0443 68.53574
375.5265 70.13522
376.0086 72.30276
376.4907 74.52063
376.9728 76.55408
377.4549 78.49673
377.9370 80.40240
378.4192 81.91989
378.9013 84.42746
379.3834 89.38123
379.8655 94.81067
380.3476 99.00671
380.8297 101.6479
381.3119 104.1728
381.7940 108.2752
382.2761 113.9199
382.7582 118.7757
383.2403 121.8221
383.7224 124.8837
384.2046 129.2426
384.6867 134.6485
385.1688 140.2876
385.6509 145.7040
386.1330 151.0027
386.6151 156.4515
387.0973 162.0338
387.5794 167.7612
388.0615 173.6741
388.5436 179.7544
389.0257 185.9874
389.5078 192.3092
389.9900 198.8882
390.4721 205.7922
390.9542 213.0635
391.4363 220.8853
391.9184 229.5272
392.4005 238.5012
392.8827 247.0450
393.3648 255.0981
393.8469 263.4811
394.3290 272.4631
394.8111 281.9774
395.2932 291.8435
395.7754 302.1311
396.2575 312.7148
396.7396 323.6936
397.2217 335.0165
397.7038 346.1029
398.1859 356.6768
398.6681 367.3509
399.1501 378.7457
399.6323 390.6547
400.1144 402.2831
400.5965 413.1616
401.0786 423.6021
401.5607 434.3716
402.0428 445.7180
402.5250 456.9136
403.0071 468.4756
403.4892 479.5349
403.9713 488.6648
404.4534 495.6127
404.9355 501.9131
405.4177 509.3772
405.8998 518.2791
406.3819 526.7927
406.8640 535.5309
407.3461 543.3404
407.8282 549.6259
408.3104 554.5345
408.7925 558.4634
409.2746 561.6418
409.7567 564.1925
410.2388 566.7488
410.7209 569.7412
411.2031 572.1313
411.6852 573.9749
412.1673 575.1229
412.6494 575.3878
413.1315 574.7462
413.6136 573.4097
414.0958 571.6808
414.5779 569.6284
415.0600 566.8535
415.5421 563.5184
416.0242 559.2873
416.5063 553.3607
416.9885 546.3663
417.4706 539.8958
417.9527 535.1324
418.4348 531.4241
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