#\#CIF_2.0 #------------------------------------------------------------------------------ #$Date: 2018-04-26 13:42:41 +0300 (Thu, 26 Apr 2018) $ #$Revision: 520 $ #$URL: svn://172.16.1.111/rod/cif/1/00/00/1000072.rod $ #------------------------------------------------------------------------------ # # This file is available in the Raman Open Database (ROD), # http://solsa.crystallography.net/rod/ # # All data on this site have been placed in the public domain by the # contributors. # data_1000072 loop_ _publ_author_name 'Karpenko, V. Y.' 'Pautov, L. A.' 'Sokolova, E. V.' 'Hawthorne, F. C.' 'Agakhanov, A. A.' 'Dikaya, T. V.' _publ_section_title ; Ankinovichite - the nickel analogue of alvanite - a new mineral from Kurumsak (Kazakhstan) and Kara-Chagyr (Kyrgystan) Locality: Kara-Chagyr, Kyrgystan Note: isostructural with alvanite ; _journal_name_full 'Zapiski Vserossijskogo Mineralogicheskogo Obshchestva' _journal_page_first 59 _journal_page_last 70 _journal_volume 133 _journal_year 2004 _chemical_compound_source R060671 _chemical_formula_sum 'Al4 H16 Ni0.72 O20 V1.88 Zn0.28' _chemical_name_mineral Ankinovichite _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90 _cell_angle_beta 92.141 _cell_angle_gamma 90 _cell_length_a 17.8098 _cell_length_b 5.1228 _cell_length_c 8.8665 _cell_volume 808.380 _exptl_crystal_density_diffrn 2.467 _cod_original_formula_sum '(Ni.72 Zn.28) Al4 V1.88 O20 H16' _cod_database_code 9012777 _raman_determination_method experimental _raman_measurement_device.location 'Arizona University' _raman_measurement_device.company 'Thermo Scientific' _raman_measurement_device.model 'Nicolet Almega XR' _raman_measurement_device.optics_type microscope _raman_measurement_device.microscope_system dispersive _raman_measurement_device.microscope_objective_magnification 50 _raman_measurement_device.microscope_numerical_aperture 0.5 _raman_measurement_device.excitation_laser_type helium-neon _raman_measurement_device.excitation_laser_wavelength 780 _raman_measurement_device.configuration simple _raman_measurement_device.resolution 4 _raman_measurement_device.power_on_sample 12 _raman_measurement_device.direction_polarization unoriented _raman_measurement_device.spot_size 1 _raman_measurement_device.diffraction_grating 400 _raman_measurement.environment Air _raman_measurement.environment_details ; The sample was measured in air. ; _raman_measurement.temperature 300 _raman_measurement.pressure 100 _raman_measurement.background_subtraction no _raman_measurement.background_subtraction_details ; No background subtraction method was applied. ; _raman_measurement.baseline_correction no _raman_measurement.baseline_correction_details ; No baseline correction method was applied. ; _raman_measurement.integration_time 10 _rod_data_source.file R060671.rod _rod_data_source.block 3500000 _rod_database.code 1000072 loop_ _raman_complementary.id _raman_complementary.method 1 XRD loop_ _raman_measurement_device_calibration.id _raman_measurement_device_calibration.standard 1 neon_lamp loop_ _rod_related_entry.id _rod_related_entry.code _rod_related_entry.database _rod_related_entry.uri _rod_related_entry.description 1 9012777 COD http://www.crystallography.net/cod/9012777.html ; XRD analysis data was done. ; loop_ _raman_spectrum.raman_shift _raman_spectrum.intensity 94.93475 0.0000000E+00 95.41687 4.2479999E-02 95.89898 2.332520 96.38110 5.966797 96.86321 10.10046 97.34533 11.91858 97.82745 9.713867 98.30956 9.063721 98.79168 11.26440 99.27380 14.65833 99.75591 18.63660 100.2380 23.44897 100.7201 29.81689 101.2023 38.00281 101.6844 47.16821 102.1665 54.87415 102.6486 61.10059 103.1307 67.44226 103.6128 74.60498 104.0950 83.01575 104.5771 92.24060 105.0592 100.8218 105.5413 109.1012 106.0234 116.4576 106.5055 121.4832 106.9877 123.4412 107.4698 124.0630 107.9519 123.9662 108.4340 120.6476 108.9161 114.3092 109.3982 105.1369 109.8804 93.82745 110.3625 80.88965 110.8446 65.98010 111.3267 52.96881 111.8088 42.50012 112.2909 33.24585 112.7731 24.62378 113.2552 16.61237 113.7373 9.698181 114.2194 4.731262 114.7015 2.815674 115.1836 1.061462 115.6658 0.6869510 116.1479 2.239685 116.6300 3.432861 117.1121 4.221069 117.5942 4.623413 118.0763 4.554810 118.5584 3.823303 119.0406 3.149048 119.5227 2.973755 120.0048 3.055786 120.4869 2.751221 120.9690 1.806763 121.4511 0.2071530 121.9333 1.691101 122.4154 3.533325 122.8975 6.237793 123.3796 10.92535 123.8617 17.81952 124.3438 24.93390 124.8260 31.67419 125.3081 37.96344 125.7902 43.56158 126.2723 48.13885 126.7544 52.21069 127.2365 56.95428 127.7187 62.88116 128.2008 68.65662 128.6829 73.98694 129.1650 78.94763 129.6471 83.72119 130.1292 88.54541 130.6114 93.32867 131.0935 96.63629 131.5756 96.72009 132.0577 96.93988 132.5398 97.98419 133.0219 99.84192 133.5041 102.2525 133.9862 104.9790 134.4683 108.0082 134.9504 111.5513 135.4325 114.8233 135.9146 119.0560 136.3968 124.8399 136.8789 132.2181 137.3610 141.1326 137.8431 151.6736 138.3252 164.2146 138.8073 176.9532 139.2895 189.2593 139.7716 202.0084 140.2537 216.6257 140.7358 233.6746 141.2179 251.3033 141.7000 266.2654 142.1821 278.7355 142.6643 292.9374 143.1464 311.5256 143.6285 333.4385 144.1106 355.0228 144.5927 375.7097 145.0748 395.5108 145.5570 415.2618 146.0391 434.8839 146.5212 452.6122 147.0033 467.6702 147.4854 480.2739 147.9675 487.8694 148.4497 489.9550 148.9318 486.4712 149.4139 476.5954 149.8960 460.2573 150.3781 438.3457 150.8602 411.8676 151.3424 378.7817 151.8245 344.6526 152.3066 308.3059 152.7887 273.5635 153.2708 240.1206 153.7529 208.6747 154.2351 179.7175 154.7172 154.6382 155.1993 134.8290 155.6814 118.1701 156.1635 104.8996 156.6456 94.52271 157.1278 86.84406 157.6099 81.82123 158.0920 79.05890 158.5741 77.06000 159.0562 75.95142 159.5383 75.30377 160.0205 75.23657 160.5026 75.58746 160.9847 76.03265 161.4668 76.46332 161.9489 76.79767 162.4310 76.78790 162.9131 76.07104 163.3953 75.37891 163.8774 75.23157 164.3595 75.57697 164.8416 75.93970 165.3237 76.24438 165.8058 76.28534 166.2880 75.66125 166.7701 74.10095 167.2522 72.03857 167.7343 69.87079 168.2164 67.55719 168.6985 65.21826 169.1807 62.99243 169.6628 60.80731 170.1449 58.52515 170.6270 56.12793 171.1091 53.59869 171.5912 50.92371 172.0734 48.05719 172.5555 45.17371 173.0376 41.93317 173.5197 38.69513 174.0018 36.04608 174.4839 34.47900 174.9661 33.82471 175.4482 32.95673 175.9303 31.86652 176.4124 30.64215 176.8945 28.89911 177.3766 27.02167 177.8588 25.76996 178.3409 25.83734 178.8230 27.27808 179.3051 28.09369 179.7872 27.29938 180.2693 26.74518 180.7515 27.13049 181.2336 28.28131 181.7157 29.65326 182.1978 30.82855 182.6799 31.82355 183.1620 32.12280 183.6441 31.56116 184.1263 30.62506 184.6084 29.33752 185.0905 27.81781 185.5726 26.43774 186.0547 25.60675 186.5368 25.42865 187.0190 24.83685 187.5011 23.77106 187.9832 22.35809 188.4653 20.58569 188.9474 18.48492 189.4296 16.29382 189.9117 14.21667 190.3938 12.26935 190.8759 10.38989 191.3580 8.318542 191.8401 6.447815 192.3223 5.397583 192.8044 5.373474 193.2865 5.430908 193.7686 4.416870 194.2507 2.666626 194.7328 1.214111 195.2150 0.4094240 195.6971 9.6923999E-02 196.1792 6.8787001E-02 196.6613 0.1981200 197.1434 2.9175000E-02 197.6255 0.7122190 198.1077 1.852478 198.5898 3.587341 199.0719 6.154236 199.5540 9.417236 200.0361 12.76666 200.5182 16.07990 201.0004 19.68231 201.4825 23.43353 201.9646 27.51245 202.4467 32.31567 202.9288 38.08887 203.4109 44.83051 203.8930 52.42059 204.3752 61.06671 204.8573 70.46710 205.3394 80.74884 205.8215 91.65570 206.3036 102.7125 206.7857 113.4262 207.2679 123.7556 207.7500 134.5751 208.2321 146.2075 208.7142 158.0826 209.1963 169.9086 209.6784 181.8052 210.1606 194.0309 210.6427 206.7438 211.1248 219.7769 211.6069 234.1691 212.0890 250.0323 212.5711 266.9392 213.0533 284.9798 213.5354 303.9813 214.0175 323.7068 214.4996 343.8773 214.9817 364.3948 215.4638 386.7727 215.9460 411.8285 216.4281 437.5734 216.9102 463.0873 217.3923 488.3480 217.8744 514.1829 218.3565 541.2147 218.8387 569.5623 219.3208 598.3193 219.8029 627.9075 220.2850 657.6306 220.7671 687.5339 221.2492 717.3958 221.7314 746.3293 222.2135 773.7547 222.6956 799.4446 223.1777 823.1279 223.6598 845.8488 224.1419 865.8291 224.6240 882.2557 225.1062 895.0824 225.5883 903.4918 226.0704 906.9071 226.5525 904.5790 227.0346 896.0731 227.5167 878.5114 227.9989 856.4687 228.4810 833.7274 228.9631 810.5145 229.4452 786.6490 229.9273 761.1110 230.4094 735.0548 230.8916 711.4225 231.3737 691.5151 231.8558 673.8973 232.3379 656.6299 232.8200 639.4408 233.3021 624.5501 233.7843 613.8071 234.2664 606.2580 234.7485 600.9578 235.2306 598.2479 235.7127 597.2149 236.1948 596.3666 236.6770 595.3306 237.1591 596.0557 237.6412 600.7099 238.1233 607.3306 238.6054 614.0248 239.0875 620.2585 239.5697 626.2631 240.0518 632.2323 240.5339 638.0042 241.0160 644.3482 241.4981 652.8351 241.9802 661.4884 242.4624 668.4431 242.9445 673.0532 243.4266 675.6844 243.9087 676.9365 244.3908 676.8485 244.8729 675.1413 245.3550 672.6323 245.8372 668.2205 246.3193 660.5948 246.8014 649.2254 247.2835 635.2954 247.7656 620.5910 248.2477 605.3618 248.7299 588.6861 249.2120 570.2510 249.6941 550.6945 250.1762 530.2250 250.6583 508.9114 251.1404 487.3575 251.6226 466.2366 252.1047 445.4517 252.5868 425.6793 253.0689 406.9042 253.5510 389.0128 254.0331 371.9644 254.5153 355.7462 254.9974 340.0699 255.4795 324.3859 255.9616 308.6353 256.4437 293.1469 256.9258 278.0146 257.4080 263.0558 257.8901 248.1617 258.3722 233.3066 258.8543 218.3324 259.3364 202.9610 259.8185 186.8026 260.3007 171.2548 260.7828 155.8024 261.2649 141.0154 261.7470 127.2609 262.2291 114.5325 262.7112 102.7938 263.1934 91.92896 263.6755 81.98969 264.1576 72.88184 264.6397 64.66699 265.1218 57.06927 265.6039 50.05908 266.0861 43.59790 266.5682 37.54309 267.0503 31.72131 267.5324 26.06287 268.0145 21.36096 268.4966 18.10413 268.9788 15.14264 269.4609 11.80646 269.9430 8.224365 270.4251 5.030334 270.9072 2.770203 271.3893 1.497070 271.8715 0.2617190 272.3536 1.049805 272.8357 2.223755 273.3178 3.105286 273.7999 3.761536 274.2820 4.375183 274.7642 5.075928 275.2463 5.849976 275.7284 6.471680 276.2105 6.905762 276.6926 7.278503 277.1747 7.719635 277.6568 8.141541 278.1389 8.306549 278.6211 8.049133 279.1032 7.490387 279.5853 7.160461 280.0674 7.375977 280.5495 7.406586 281.0316 6.754883 281.5138 5.829926 281.9959 5.477692 282.4780 6.145447 282.9601 7.314636 283.4422 7.597382 283.9243 6.774628 284.4065 5.676697 284.8886 4.316437 285.3707 2.815277 285.8528 1.402649 286.3349 0.1743470 286.8170 1.089081 287.2992 2.791046 287.7813 4.982819 288.2634 7.360382 288.7455 10.07428 289.2276 12.86581 289.7097 15.29001 290.1919 17.22784 290.6740 19.18622 291.1561 21.84103 291.6382 25.26743 292.1203 28.80997 292.6024 32.45059 293.0846 36.15546 293.5667 39.92078 294.0488 43.75513 294.5309 47.51675 295.0130 50.87473 295.4951 53.87979 295.9773 57.90497 296.4594 63.76620 296.9415 70.10730 297.4236 75.86652 297.9057 81.01810 298.3878 86.16714 298.8700 91.62823 299.3521 97.47076 299.8342 103.7915 300.3163 110.9702 300.7984 118.2177 301.2805 124.9554 301.7627 131.3255 302.2448 138.2070 302.7269 146.3982 303.2090 155.1909 303.6911 162.5717 304.1732 168.2960 304.6554 173.2781 305.1375 178.1423 305.6196 182.6003 306.1017 185.8486 306.5838 187.5017 307.0659 187.9505 307.5481 187.8324 308.0302 187.1765 308.5123 186.1385 308.9944 184.4076 309.4765 182.4018 309.9586 180.8386 310.4408 179.9048 310.9229 179.4429 311.4050 179.3009 311.8871 179.4421 312.3692 179.9669 312.8513 180.7554 313.3335 182.0009 313.8156 183.7957 314.2977 186.1321 314.7798 189.4422 315.2619 194.4359 315.7440 201.0519 316.2262 207.5707 316.7083 213.5487 317.1904 219.5965 317.6725 226.3227 318.1546 233.7210 318.6367 241.1882 319.1188 248.5105 319.6010 255.5128 320.0831 261.8097 320.5652 267.3774 321.0473 272.3296 321.5294 277.1195 322.0115 281.4428 322.4937 284.2655 322.9758 285.0489 323.4579 284.0343 323.9400 281.7871 324.4221 277.9342 324.9042 273.8860 325.3864 270.2854 325.8685 266.8152 326.3506 262.7163 326.8327 257.6431 327.3148 252.2528 327.7969 247.4798 328.2791 243.2707 328.7612 239.7088 329.2433 237.0050 329.7254 234.8451 330.2075 232.9085 330.6896 231.1466 331.1718 229.6230 331.6539 228.3388 332.1360 227.3328 332.6181 226.9226 333.1002 227.0164 333.5823 227.7876 334.0645 229.5265 334.5466 232.1588 335.0287 235.2320 335.5108 238.4767 335.9929 241.9197 336.4750 245.4920 336.9572 249.1627 337.4393 253.0340 337.9214 257.0919 338.4035 261.3736 338.8856 265.9546 339.3677 270.8773 339.8499 276.0483 340.3320 281.2444 340.8141 286.3387 341.2962 291.6082 341.7783 297.3457 342.2604 303.3114 342.7426 309.4456 343.2247 315.7155 343.7068 321.3884 344.1889 325.3858 344.6710 327.1349 345.1531 328.4122 345.6353 329.0600 346.1174 329.2892 346.5995 329.5615 347.0816 329.7603 347.5637 329.0258 348.0458 326.6225 348.5280 322.4741 349.0101 317.0565 349.4922 309.5054 349.9743 301.8099 350.4564 294.6658 350.9385 288.0999 351.4207 281.9360 351.9028 276.1031 352.3849 270.6602 352.8670 265.8159 353.3491 261.2753 353.8312 257.6919 354.3134 255.3445 354.7955 253.9287 355.2776 253.0637 355.7597 252.6288 356.2418 252.7988 356.7239 253.9100 357.2061 256.5325 357.6882 259.0086 358.1703 260.4661 358.6524 262.4509 359.1345 266.0140 359.6166 271.2231 360.0987 277.4969 360.5808 284.3734 361.0630 291.9521 361.5451 299.3651 362.0272 306.6707 362.5093 313.8801 362.9914 320.9640 363.4735 327.8874 363.9557 334.6277 364.4378 341.2489 364.9199 347.5306 365.4020 352.5189 365.8841 355.6875 366.3662 358.0923 366.8484 360.0606 367.3305 361.2266 367.8126 361.5072 368.2947 360.8477 368.7768 358.7866 369.2589 354.3463 369.7411 346.8305 370.2232 338.7429 370.7053 330.2659 371.1874 321.3492 371.6695 311.5602 372.1516 301.0026 372.6338 290.1260 373.1159 279.3872 373.5980 268.8175 374.0801 258.0594 374.5622 245.9926 375.0443 235.1566 375.5265 226.8936 376.0086 220.1321 376.4907 213.3894 376.9728 205.9329 377.4549 198.0502 377.9370 190.2937 378.4192 182.6027 378.9013 175.2023 379.3834 168.0463 379.8655 161.2554 380.3476 155.0541 380.8297 149.4815 381.3119 144.1127 381.7940 138.5405 382.2761 132.7643 382.7582 127.1356 383.2403 121.8250 383.7224 116.5278 384.2046 111.0717 384.6867 105.4809 385.1688 99.68387 385.6509 93.48544 386.1330 87.14230 386.6151 81.11093 387.0973 75.33679 387.5794 70.12637 388.0615 66.15704 388.5436 62.71429 389.0257 58.72058 389.5078 53.65787 389.9900 48.58099 390.4721 44.36761 390.9542 40.95300 391.4363 38.04355 391.9184 35.74496 392.4005 33.67224 392.8827 31.27405 393.3648 28.53699 393.8469 25.78781 394.3290 22.96515 394.8111 20.27887 395.2932 18.18042 395.7754 16.75089 396.2575 15.51700 396.7396 13.98819 397.2217 12.23523 397.7038 10.92764 398.1859 10.43567 398.6681 10.08249 399.1501 9.412537 399.6323 8.494354 400.1144 7.609863 400.5965 6.896393 401.0786 6.310730 401.5607 5.748688 402.0428 5.143829 402.5250 4.661713 403.0071 4.327728 403.4892 4.128754 403.9713 4.118378 404.4534 4.292419 404.9355 4.469635 405.4177 4.440613 405.8998 4.177460 406.3819 3.825958 406.8640 3.213806 407.3461 2.691772 407.8282 2.574585 408.3104 2.695984 408.7925 2.567810 409.2746 1.832703 409.7567 0.7181700 410.2388 0.2598270 410.7209 1.092499 411.2031 1.800964 411.6852 2.450897 412.1673 2.830170 412.6494 2.627533 413.1315 1.813477 413.6136 0.7898250 414.0958 9.7382002E-02 414.5779 0.1775510 415.0600 0.4848330 415.5421 0.9215390 416.0242 1.295380 416.5063 1.646362 416.9885 1.876129 417.4706 1.694183 417.9527 0.7287600 418.4348 0.6094970 418.9169 0.7786870 419.3990 0.8396610 419.8812 2.257751 420.3633 2.768646 420.8454 2.863098 421.3275 2.947632 421.8096 3.119354 422.2917 3.269135 422.7739 3.345886 423.2560 3.341125 423.7381 3.001617 424.2202 1.925354 424.7023 1.025299 425.1844 1.296417 425.6666 2.383728 426.1487 2.981323 426.6308 1.875732 427.1129 0.2685550 427.5950 0.2729490 428.0771 2.017029 428.5593 3.266754 429.0414 2.513916 429.5235 0.6422420 430.0056 0.3029790 430.4877 5.4382000E-02 430.9698 0.5160830 431.4520 1.254761 431.9341 1.966949 432.4162 2.175537 432.8983 1.711884 433.3804 1.074188 433.8625 0.8479920 434.3447 1.102478 434.8268 1.253723 435.3089 1.258209 435.7910 1.177795 436.2731 1.012634 436.7552 0.7911070 437.2374 0.6026610 437.7195 0.5126650 438.2016 0.4695430 438.6837 0.2702030 439.1658 0.1953430 439.6479 0.6815190 440.1301 1.075500 440.6122 1.539429 441.0943 2.211700 441.5764 3.125549 442.0585 4.297180 442.5406 5.883789 443.0227 8.106873 443.5049 9.153473 443.9870 7.441284 444.4691 6.184265 444.9512 6.681122 445.4333 8.244263 445.9154 9.614197 446.3976 10.10663 446.8797 10.24475 447.3618 11.33081 447.8439 13.86276 448.3260 15.84872 448.8081 16.18771 449.2903 16.40768 449.7724 17.58472 450.2545 19.71075 450.7366 21.88950 451.2187 23.28333 451.7008 24.13058 452.1830 25.48340 452.6651 27.54480 453.1472 29.63187 453.6293 31.35812 454.1114 32.84866 454.5935 34.21716 455.0757 35.35519 455.5578 36.62146 456.0399 38.61218 456.5220 41.07114 457.0041 42.76828 457.4862 43.08835 457.9684 43.09787 458.4505 44.32648 458.9326 46.74973 459.4147 49.01236 459.8968 50.72778 460.3789 52.28955 460.8611 54.17468 461.3432 56.29761 461.8253 58.05042 462.3074 59.00558 462.7895 59.37402 463.2716 60.04800 463.7538 61.57074 464.2359 62.66806 464.7180 62.82831 465.2001 62.69952 465.6822 63.14902 466.1643 64.23965 466.6465 65.08432 467.1286 64.64249 467.6107 62.74289 468.0928 61.11377 468.5749 60.01358 469.0570 58.91702 469.5392 57.77640 470.0213 56.52509 470.5034 55.07574 470.9855 53.38306 471.4676 51.53970 471.9497 49.62976 472.4319 47.55597 472.9140 45.85504 473.3961 44.88776 473.8782 44.08185 474.3603 43.15469 474.8424 42.11948 475.3246 41.07993 475.8067 39.94330 476.2888 38.93695 476.7709 38.74838 477.2530 39.51099 477.7351 39.83105 478.2173 38.67746 478.6994 37.03128 479.1815 36.44403 479.6636 37.20993 480.1457 38.14935 480.6278 38.84091 481.1100 39.28098 481.5920 39.25311 482.0742 38.72113 482.5563 38.61960 483.0384 39.90265 483.5205 42.49289 484.0026 44.36966 484.4847 44.98138 484.9669 45.75906 485.4490 47.12152 485.9311 48.83142 486.4132 50.72455 486.8953 52.85748 487.3774 55.14340 487.8596 57.22015 488.3417 58.84665 488.8238 60.70453 489.3059 62.89636 489.7880 65.12436 490.2701 67.23334 490.7523 69.31070 491.2344 71.45956 491.7165 73.65958 492.1986 76.00909 492.6807 79.02579 493.1628 83.14764 493.6450 86.72559 494.1271 88.75464 494.6092 90.63593 495.0913 93.28183 495.5734 96.71646 496.0555 100.4102 496.5377 104.1473 497.0198 107.8587 497.5019 111.1558 497.9840 113.8823 498.4661 116.8579 498.9482 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