#\#CIF_2.0 #------------------------------------------------------------------------------ #$Date: 2018-04-26 13:42:54 +0300 (Thu, 26 Apr 2018) $ #$Revision: 523 $ #$URL: svn://172.16.1.111/rod/cif/1/00/00/1000075.rod $ #------------------------------------------------------------------------------ # # This file is available in the Raman Open Database (ROD), # http://solsa.crystallography.net/rod/ # # All data on this site have been placed in the public domain by the # contributors. # data_1000075 loop_ _publ_author_name 'Atencio, D.' 'Matioli, P. A.' 'Smith, J. B.' 'Chukanov, N. V.' 'Coutinho, J. M. V.' 'Rastsvetaeva, R. K.' 'Mockel, S.' _publ_section_title ; Footemineite, the Mn-analog of atencioite, from the Foote mine, Kings Mountain, Cleveland County, North Carolina, U.S.A., and its relationship with other roscherite-group minerals Locality: Foote mine, Kings Mountain, Cleveland County, North Carolina, USA ; _journal_name_full 'American Mineralogist' _journal_page_first 1 _journal_page_last 6 _journal_paper_doi 10.2138/am.2008.2469 _journal_volume 93 _journal_year 2008 _chemical_compound_source R060893 _chemical_formula_sum 'Be4 Ca2 Fe0.52 H16 Li0.17 Mg0.05 Mn4.14 O34 P6' _chemical_name_mineral Footemineite _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 73.84 _cell_angle_beta 85.34 _cell_angle_gamma 87.44 _cell_length_a 6.788 _cell_length_b 9.972 _cell_length_c 10.014 _cell_volume 648.740 _exptl_crystal_density_diffrn 2.869 _cod_original_formula_sum 'Ca2 Mn4.14 Li.17 Mg.05 Fe.52 P6 Be4 O34 H16' _cod_database_code 9010368 _raman_determination_method experimental _raman_measurement_device.location 'Arizona University' _raman_measurement_device.company 'Thermo Scientific' _raman_measurement_device.model 'Nicolet Almega XR' _raman_measurement_device.optics_type microscope _raman_measurement_device.microscope_system dispersive _raman_measurement_device.microscope_objective_magnification 50 _raman_measurement_device.microscope_numerical_aperture 0.5 _raman_measurement_device.excitation_laser_type helium-neon _raman_measurement_device.excitation_laser_wavelength 780 _raman_measurement_device.configuration simple _raman_measurement_device.resolution 4 _raman_measurement_device.power_on_sample 12 _raman_measurement_device.direction_polarization unoriented _raman_measurement_device.spot_size 1 _raman_measurement_device.diffraction_grating 400 _raman_measurement.environment Air _raman_measurement.environment_details ; The sample was measured in air. ; _raman_measurement.temperature 300 _raman_measurement.pressure 100 _raman_measurement.background_subtraction no _raman_measurement.background_subtraction_details ; No background subtraction method was applied. ; _raman_measurement.baseline_correction no _raman_measurement.baseline_correction_details ; No baseline correction method was applied. ; _raman_measurement.integration_time 10 _rod_data_source.file R060893.rod _rod_data_source.block 3500000 _rod_database.code 1000075 loop_ _raman_complementary.id _raman_complementary.method 1 XRD loop_ _raman_measurement_device_calibration.id _raman_measurement_device_calibration.standard 1 neon_lamp loop_ _rod_related_entry.id _rod_related_entry.code _rod_related_entry.database _rod_related_entry.uri _rod_related_entry.description 1 9010368 COD http://www.crystallography.net/cod/9010368.html ; XRD analysis data was done. ; loop_ _raman_spectrum.raman_shift _raman_spectrum.intensity 95.41687 0.0000000E+00 95.89898 0.2329410 96.38110 0.2901000 96.86321 1.232788 97.34533 3.110596 97.82745 4.607513 98.30956 5.682678 98.79168 5.956207 99.27380 5.462433 99.75591 4.135773 100.2380 2.387360 100.7201 1.080231 101.2023 0.2440190 101.6844 5.2979000E-02 102.1665 4.5380000E-02 102.6486 0.3875430 103.1307 0.8840940 103.6128 1.148071 104.0950 1.309601 104.5771 1.414948 105.0592 1.173157 105.5413 0.8010860 106.0234 0.7206120 106.5055 1.289215 106.9877 2.329529 107.4698 3.093872 107.9519 3.176788 108.4340 3.243378 108.9161 3.467926 109.3982 3.941010 109.8804 4.846405 110.3625 6.631805 110.8446 9.119720 111.3267 10.81360 111.8088 12.57980 112.2909 14.41891 112.7731 15.80228 113.2552 16.25946 113.7373 16.53305 114.2194 17.18216 114.7015 18.17093 115.1836 18.78229 115.6658 19.42633 116.1479 19.78549 116.6300 19.43835 117.1121 18.18866 117.5942 16.31622 118.0763 14.41434 118.5584 12.37677 119.0406 10.65350 119.5227 9.433014 120.0048 8.637817 120.4869 8.090027 120.9690 7.857727 121.4511 7.721741 121.9333 7.311523 122.4154 6.593994 122.8975 5.668396 123.3796 4.541321 123.8617 3.158752 124.3438 1.816315 124.8260 0.4284670 125.3081 0.6905520 125.7902 1.098450 126.2723 0.3212590 126.7544 0.9756470 127.2365 1.501404 127.7187 0.9084170 128.2008 0.5015260 128.6829 4.7851998E-02 129.1650 0.6174320 129.6471 0.7493590 130.1292 0.2990720 130.6114 0.4956970 131.0935 0.8823550 131.5756 0.5463260 132.0577 0.1780700 132.5398 0.1745300 133.0219 0.4461980 133.5041 0.5360720 133.9862 0.3479000 134.4683 0.1307070 134.9504 0.8199160 135.4325 1.888672 135.9146 2.979919 136.3968 3.857574 136.8789 4.518585 137.3610 5.180542 137.8431 6.093231 138.3252 7.304199 138.8073 8.624481 139.2895 9.893738 139.7716 11.32443 140.2537 13.37646 140.7358 16.30435 141.2179 19.21896 141.7000 20.82245 142.1821 21.25580 142.6643 21.48550 143.1464 22.02185 143.6285 22.69693 144.1106 22.91769 144.5927 22.55453 145.0748 21.61990 145.5570 20.09412 146.0391 17.99075 146.5212 15.80386 147.0033 13.94040 147.4854 12.42068 147.9675 10.99750 148.4497 9.676117 148.9318 8.394653 149.4139 7.085022 149.8960 5.747284 150.3781 4.471497 150.8602 3.381226 151.3424 2.400269 151.8245 1.796692 152.3066 1.899658 152.7887 2.135254 153.2708 2.306885 153.7529 1.905151 154.2351 1.201752 154.7172 0.8892520 155.1993 1.691681 155.6814 2.020935 156.1635 1.342010 156.6456 0.2870790 157.1278 0.3348690 157.6099 0.1018680 158.0920 0.7444150 158.5741 1.207794 159.0562 1.295532 159.5383 1.067230 160.0205 0.1490480 160.5026 1.102844 160.9847 1.828125 161.4668 1.399017 161.9489 0.1275020 162.4310 0.5162050 162.9131 0.1218870 163.3953 0.4528500 163.8774 0.8241580 164.3595 0.9819030 164.8416 0.8729250 165.3237 0.3932190 165.8058 0.3781130 166.2880 1.239838 166.7701 2.336761 167.2522 3.391937 167.7343 4.022125 168.2164 4.139771 168.6985 4.248413 169.1807 4.680695 169.6628 5.265503 170.1449 5.827362 170.6270 6.357483 171.1091 6.792694 171.5912 6.925995 172.0734 6.518768 172.5555 6.250397 173.0376 6.399414 173.5197 6.823822 174.0018 7.328003 174.4839 7.800201 174.9661 8.259064 175.4482 8.825867 175.9303 9.776550 176.4124 10.50864 176.8945 10.61328 177.3766 10.40491 177.8588 10.42328 178.3409 11.07205 178.8230 12.35883 179.3051 13.74005 179.7872 15.45465 180.2693 17.02655 180.7515 18.28644 181.2336 19.26917 181.7157 20.06512 182.1978 20.72119 182.6799 21.18414 183.1620 21.88553 183.6441 23.44717 184.1263 24.78012 184.6084 25.30737 185.0905 24.99210 185.5726 24.11996 186.0547 22.86099 186.5368 21.11975 187.0190 19.82950 187.5011 19.54309 187.9832 19.38611 188.4653 18.66788 188.9474 17.29584 189.4296 15.69974 189.9117 14.18472 190.3938 12.77316 190.8759 11.74591 191.3580 11.36685 191.8401 11.32242 192.3223 11.24939 192.8044 11.07532 193.2865 10.96841 193.7686 11.03882 194.2507 11.27917 194.7328 11.80441 195.2150 12.80609 195.6971 14.09079 196.1792 15.26437 196.6613 16.23639 197.1434 17.22882 197.6255 18.34500 198.1077 19.59885 198.5898 21.02911 199.0719 22.79553 199.5540 24.79871 200.0361 26.54675 200.5182 27.72556 201.0004 29.09747 201.4825 31.30496 201.9646 34.02856 202.4467 36.45667 202.9288 37.95612 203.4109 38.58157 203.8930 39.18240 204.3752 39.62299 204.8573 40.19354 205.3394 41.23044 205.8215 42.50519 206.3036 43.49261 206.7857 43.66748 207.2679 42.97348 207.7500 42.57172 208.2321 42.80283 208.7142 43.03287 209.1963 42.91882 209.6784 42.60413 210.1606 42.49432 210.6427 42.96182 211.1248 44.05609 211.6069 45.25049 212.0890 46.87939 212.5711 48.28857 213.0533 49.17749 213.5354 49.59525 214.0175 49.81839 214.4996 50.13507 214.9817 50.63809 215.4638 50.47861 215.9460 49.24719 216.4281 47.87820 216.9102 46.92053 217.3923 46.31100 217.8744 45.54892 218.3565 44.12308 218.8387 41.95975 219.3208 39.85251 219.8029 37.73666 220.2850 35.73083 220.7671 33.85114 221.2492 32.11911 221.7314 30.70218 222.2135 29.89551 222.6956 29.74948 223.1777 29.00812 223.6598 26.93381 224.1419 24.78043 224.6240 23.61588 225.1062 23.45636 225.5883 23.42084 226.0704 22.66821 226.5525 21.36185 227.0346 20.71980 227.5167 21.50380 227.9989 22.55618 228.4810 22.76678 228.9631 22.06639 229.4452 21.13788 229.9273 20.26303 230.4094 19.55127 230.8916 19.30083 231.3737 20.09235 231.8558 21.09212 232.3379 21.24376 232.8200 20.41164 233.3021 19.55353 233.7843 19.18097 234.2664 19.18272 234.7485 19.51457 235.2306 20.47806 235.7127 21.57028 236.1948 22.01387 236.6770 21.64183 237.1591 21.12274 237.6412 20.81764 238.1233 20.63226 238.6054 20.39426 239.0875 19.98474 239.5697 19.56285 240.0518 19.47849 240.5339 19.89691 241.0160 20.08255 241.4981 19.50055 241.9802 18.60611 242.4624 17.83408 242.9445 17.35269 243.4266 17.11794 243.9087 17.12183 244.3908 17.52823 244.8729 17.71460 245.3550 17.30107 245.8372 16.71654 246.3193 16.31386 246.8014 16.21126 247.2835 16.30443 247.7656 16.47601 248.2477 16.89484 248.7299 16.96725 249.2120 16.17462 249.6941 15.27809 250.1762 14.92157 250.6583 15.29041 251.1404 15.99976 251.6226 16.41560 252.1047 16.42770 252.5868 16.38527 253.0689 16.16547 253.5510 16.01198 254.0331 16.16592 254.5153 16.66225 254.9974 17.26343 255.4795 17.60231 255.9616 17.55780 256.4437 17.49710 256.9258 17.34819 257.4080 17.24615 257.8901 17.36734 258.3722 17.69960 258.8543 18.00148 259.3364 17.95456 259.8185 17.50900 260.3007 16.79097 260.7828 15.40462 261.2649 14.09528 261.7470 13.45422 262.2291 13.46056 262.7112 13.56689 263.1934 13.09550 263.6755 11.74715 264.1576 10.92754 264.6397 10.95779 265.1218 11.13753 265.6039 11.13530 266.0861 10.91475 266.5682 10.52469 267.0503 9.903427 267.5324 8.843323 268.0145 9.074127 268.4966 12.04872 268.9788 14.72859 269.4609 15.45305 269.9430 14.44395 270.4251 12.92635 270.9072 11.82838 271.3893 11.16209 271.8715 10.84624 272.3536 11.13274 272.8357 11.43954 273.3178 11.54822 273.7999 11.47519 274.2820 11.33125 274.7642 11.20729 275.2463 11.08250 275.7284 10.66029 276.2105 9.699020 276.6926 8.775803 277.1747 8.045151 277.6568 7.490616 278.1389 7.065735 278.6211 6.747574 279.1032 6.535812 279.5853 6.444138 280.0674 6.713531 280.5495 6.800415 281.0316 6.495117 281.5138 5.925735 281.9959 5.315018 282.4780 4.759933 282.9601 4.215469 283.4422 3.563477 283.9243 2.691711 284.4065 1.933273 284.8886 1.346405 285.3707 0.9161990 285.8528 0.6369170 286.3349 0.5126340 286.8170 0.5028690 287.2992 0.5814820 287.7813 0.8343960 288.2634 0.8860320 288.7455 0.5000150 289.2276 4.8232999E-02 289.7097 0.4375000 290.1919 0.5958250 290.6740 0.5958250 291.1561 0.4587860 291.6382 0.1417540 292.1203 5.9586000E-02 292.6024 0.5530550 293.0846 1.131287 293.5667 1.213135 294.0488 0.7357030 294.5309 0.2568970 295.0130 0.3272090 295.4951 0.9637600 295.9773 1.459320 296.4594 1.761765 296.9415 1.934830 297.4236 2.057571 297.9057 2.109589 298.3878 1.953598 298.8700 1.382217 299.3521 0.4706570 299.8342 0.1398620 300.3163 0.2194370 300.7984 0.2148590 301.2805 0.3239590 301.7627 0.5364690 302.2448 0.8560330 302.7269 1.323883 303.2090 1.906815 303.6911 2.533600 304.1732 3.461395 304.6554 4.013519 305.1375 3.612000 305.6196 2.614548 306.1017 1.941589 306.5838 1.954193 307.0659 2.439941 307.5481 3.030289 308.0302 3.719604 308.5123 4.379074 308.9944 5.045776 309.4765 5.689621 309.9586 6.182968 310.4408 6.446793 310.9229 6.750412 311.4050 7.530289 311.8871 8.798462 312.3692 9.971695 312.8513 11.17525 313.3335 12.11168 313.8156 12.24998 314.2977 11.48322 314.7798 10.63121 315.2619 10.51042 315.7440 11.06932 316.2262 11.38290 316.7083 11.21381 317.1904 10.88721 317.6725 10.63048 318.1546 10.45540 318.6367 10.36732 319.1188 10.43456 319.6010 10.58231 320.0831 10.48996 320.5652 10.02243 321.0473 9.458923 321.5294 8.907745 322.0115 8.378479 322.4937 7.909241 322.9758 7.552826 323.4579 7.231125 323.9400 6.733170 324.4221 5.929718 324.9042 5.252731 325.3864 4.961456 325.8685 4.885117 326.3506 4.708710 326.8327 4.337036 327.3148 3.822403 327.7969 3.159607 328.2791 2.268524 328.7612 1.679337 329.2433 1.631226 329.7254 1.874084 330.2075 2.151810 330.6896 2.420532 331.1718 2.698654 331.6539 3.075394 332.1360 3.557068 332.6181 3.636368 333.1002 2.832031 333.5823 1.973251 334.0645 1.691727 334.5466 1.970901 335.0287 2.406372 335.5108 2.750366 335.9929 3.008881 336.4750 3.245331 336.9572 3.329117 337.4393 3.526993 337.9214 4.125275 338.4035 4.929840 338.8856 5.445953 339.3677 5.412323 339.8499 5.025482 340.3320 4.807144 340.8141 4.782120 341.2962 4.843597 341.7783 5.035324 342.2604 5.279282 342.7426 5.504013 343.2247 5.689560 343.7068 5.778152 344.1889 5.655838 344.6710 5.169632 345.1531 4.950867 345.6353 5.243637 346.1174 5.642242 346.5995 5.944519 347.0816 6.073441 347.5637 5.853256 348.0458 5.073532 348.5280 3.697632 349.0101 2.835159 349.4922 2.748016 349.9743 2.823822 350.4564 2.817337 350.9385 2.735458 351.4207 2.712234 351.9028 2.862961 352.3849 3.108612 352.8670 3.063049 353.3491 2.563431 353.8312 1.908386 354.3134 0.8552090 354.7955 0.2013400 355.2776 0.7285920 355.7597 0.5514370 356.2418 4.7851998E-02 356.7239 0.1441500 357.2061 0.1755220 357.6882 0.3772130 358.1703 0.5545200 358.6524 0.6201630 359.1345 0.3945310 359.6166 6.4438000E-02 360.0987 0.4308930 360.5808 0.3446040 361.0630 0.2799070 361.5451 0.5221100 362.0272 2.6505001E-02 362.5093 0.5067290 362.9914 0.6394650 363.4735 0.4851530 363.9557 0.1514280 364.4378 0.3238980 364.9199 0.8344120 365.4020 0.9174650 365.8841 0.1625980 366.3662 0.4796600 366.8484 0.8168790 367.3305 1.032501 367.8126 1.267273 368.2947 1.577347 368.7768 2.008453 369.2589 2.673309 369.7411 3.706879 370.2232 4.603668 370.7053 5.350479 371.1874 5.965836 371.6695 6.433640 372.1516 6.769592 372.6338 7.016510 373.1159 7.115372 373.5980 7.082886 374.0801 7.538177 374.5622 8.701736 375.0443 10.13637 375.5265 12.04584 376.0086 14.03792 376.4907 15.42255 376.9728 15.74466 377.4549 15.58026 377.9370 16.24533 378.4192 17.98148 378.9013 19.87483 379.3834 21.89566 379.8655 23.84267 380.3476 25.51128 380.8297 26.86470 381.3119 28.13150 381.7940 29.62970 382.2761 31.35139 382.7582 32.66441 383.2403 33.19112 383.7224 33.63432 384.2046 34.68246 384.6867 36.11009 385.1688 37.11874 385.6509 37.06853 386.1330 36.32571 386.6151 35.76041 387.0973 35.47815 387.5794 35.00641 388.0615 33.98167 388.5436 32.60822 389.0257 31.14107 389.5078 29.62434 389.9900 28.02634 390.4721 26.20808 390.9542 24.21059 391.4363 22.45668 391.9184 21.14255 392.4005 20.07574 392.8827 19.01483 393.3648 17.97012 393.8469 16.84396 394.3290 15.41177 394.8111 13.93755 395.2932 12.90959 395.7754 12.41588 396.2575 12.08615 396.7396 11.61746 397.2217 11.02037 397.7038 10.44722 398.1859 9.603165 398.6681 9.043610 399.1501 9.240158 399.6323 10.05756 400.1144 11.02419 400.5965 11.93996 401.0786 12.79382 401.5607 13.52342 402.0428 14.00951 402.5250 14.59738 403.0071 15.16484 403.4892 15.97556 403.9713 17.37469 404.4534 19.45096 404.9355 21.88416 405.4177 24.38931 405.8998 27.11307 406.3819 28.96690 406.8640 29.24522 407.3461 29.43803 407.8282 30.29500 408.3104 31.68266 408.7925 33.13370 409.2746 34.38121 409.7567 35.43887 410.2388 36.40347 410.7209 37.66103 411.2031 38.26842 411.6852 37.58302 412.1673 36.53455 412.6494 36.06541 413.1315 36.38133 413.6136 36.94235 414.0958 36.89659 414.5779 35.91167 415.0600 35.54254 415.5421 36.44669 416.0242 37.36963 416.5063 37.87163 416.9885 38.01868 417.4706 38.04369 417.9527 38.09727 418.4348 38.16405 418.9169 38.07185 419.3990 37.81422 419.8812 37.15634 420.3633 35.86296 420.8454 34.31859 421.3275 32.94121 421.8096 31.84624 422.2917 30.48990 422.7739 28.12772 423.2560 24.80614 423.7381 21.64798 424.2202 18.57855 424.7023 16.04350 425.1844 14.50345 425.6666 13.74927 426.1487 13.02448 426.6308 11.96481 427.1129 10.77258 427.5950 9.649063 428.0771 8.498108 428.5593 7.897858 429.0414 8.466721 429.5235 9.678009 430.0056 10.27309 430.4877 9.943710 430.9698 9.697617 431.4520 10.05565 431.9341 10.84402 432.4162 11.72800 432.8983 12.62181 433.3804 13.60934 433.8625 14.84438 434.3447 16.37854 434.8268 17.68271 435.3089 18.31960 435.7910 19.07812 436.2731 20.55603 436.7552 22.62839 437.2374 24.83505 437.7195 26.94354 438.2016 28.91325 438.6837 30.55016 439.1658 31.51578 439.6479 32.58113 440.1301 34.04738 440.6122 35.49094 441.0943 36.59865 441.5764 37.26016 442.0585 37.40569 442.5406 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