#\#CIF_2.0 #------------------------------------------------------------------------------ #$Date: 2018-04-26 13:43:31 +0300 (Thu, 26 Apr 2018) $ #$Revision: 532 $ #$URL: svn://172.16.1.111/rod/cif/1/00/00/1000084.rod $ #------------------------------------------------------------------------------ # # This file is available in the Raman Open Database (ROD), # http://solsa.crystallography.net/rod/ # # All data on this site have been placed in the public domain by the # contributors. # data_1000084 loop_ _publ_author_name 'Rastsvetaeva, R. K.' 'Tamazyan, R. A.' 'Pushcharovskii D Yu' 'Nadezhina, T. N.' 'Voloshin, A. V.' _publ_section_title ; K-nenadkevichite, a new representative of the nenadkevichite-labuntsovite series ; _journal_name_full 'Crystallography Reports' _journal_page_first 908 _journal_page_last 914 _journal_volume 39 _journal_year 1994 _chemical_compound_source 'Vuoriyarvi, Kola Peninsula' _chemical_formula_sum 'H10.3 K2.98 Na1.22 Nb2.2 O31.15 Si8 Ti1.8' _chemical_name_mineral Vuoriyarvite _space_group_IT_number 8 _symmetry_space_group_name_Hall 'C -2y' _symmetry_space_group_name_H-M 'C 1 m 1' _cell_angle_alpha 90 _cell_angle_beta 117.87 _cell_angle_gamma 90 _cell_length_a 14.692 _cell_length_b 14.164 _cell_length_c 7.859 _cell_volume 1445.745 _exptl_crystal_density_diffrn 2.684 _cod_original_formula_sum 'Si8 (Nb2.2 Ti1.8) K2.98 Na1.22 O31.15 H10.3' _cod_database_code 9014345 _raman_determination_method experimental _raman_measurement_device.location 'Arizona University' _raman_measurement_device.company 'Thermo Scientific' _raman_measurement_device.model 'Nicolet Almega XR' _raman_measurement_device.optics_type microscope _raman_measurement_device.microscope_system dispersive _raman_measurement_device.microscope_objective_magnification 50 _raman_measurement_device.microscope_numerical_aperture 0.5 _raman_measurement_device.excitation_laser_type helium-neon _raman_measurement_device.excitation_laser_wavelength 780 _raman_measurement_device.configuration simple _raman_measurement_device.resolution 4 _raman_measurement_device.power_on_sample 12 _raman_measurement_device.direction_polarization unoriented _raman_measurement_device.spot_size 1 _raman_measurement_device.diffraction_grating 400 _raman_measurement.environment Air _raman_measurement.environment_details ; The sample was measured in air. ; _raman_measurement.temperature 300 _raman_measurement.pressure 100 _raman_measurement.background_subtraction no _raman_measurement.background_subtraction_details ; No background subtraction method was applied. ; _raman_measurement.baseline_correction no _raman_measurement.baseline_correction_details ; No baseline correction method was applied. ; _raman_measurement.integration_time 10 _rod_data_source.file R070610.rod _rod_data_source.block 3500000 _rod_database.code 1000084 loop_ _raman_complementary.id _raman_complementary.method 1 XRD loop_ _raman_measurement_device_calibration.id _raman_measurement_device_calibration.standard 1 neon_lamp loop_ _rod_related_entry.id _rod_related_entry.code _rod_related_entry.database _rod_related_entry.uri _rod_related_entry.description 1 9014345 COD http://www.crystallography.net/cod/9014345.html ; XRD analysis data was done. ; loop_ _raman_spectrum.raman_shift _raman_spectrum.intensity 143.8380 0.0000000E+00 144.3201 70.58301 144.8022 77.13379 145.2844 125.2842 145.7665 142.8574 146.2486 58.87988 146.7307 14.23145 147.2128 51.02441 147.6949 48.53223 148.1771 17.74121 148.6592 37.87500 149.1413 114.2061 149.6234 194.9561 150.1055 264.6895 150.5877 332.1504 151.0698 429.4492 151.5519 570.0352 152.0340 731.7383 152.5161 888.8311 152.9982 1041.019 153.4804 1201.751 153.9625 1386.952 154.4446 1598.354 154.9267 1800.664 155.4088 1962.828 155.8909 2127.292 156.3731 2325.461 156.8552 2563.781 157.3373 2823.237 157.8194 3078.407 158.3015 3328.743 158.7836 3578.553 159.2658 3828.605 159.7479 4079.444 160.2300 4332.190 160.7121 4588.451 161.1942 4843.876 161.6763 5081.492 162.1585 5282.368 162.6406 5486.861 163.1227 5728.504 163.6048 5971.613 164.0869 6167.725 164.5690 6283.220 165.0512 6327.008 165.5333 6385.637 166.0154 6483.291 166.4975 6571.807 166.9796 6661.744 167.4617 6734.752 167.9439 6754.240 168.4260 6686.508 168.9081 6524.127 169.3902 6360.480 169.8723 6207.898 170.3544 6045.035 170.8366 5857.260 171.3187 5645.969 171.8008 5427.018 172.2829 5216.722 172.7650 5019.903 173.2471 4795.758 173.7293 4512.356 174.2114 4221.293 174.6935 3969.251 175.1756 3765.235 175.6577 3586.426 176.1398 3413.602 176.6220 3249.641 177.1041 3067.881 177.5862 2844.276 178.0683 2602.992 178.5504 2384.057 179.0325 2197.820 179.5147 2033.970 179.9968 1877.624 180.4789 1725.778 180.9610 1595.729 181.4431 1511.114 181.9252 1459.181 182.4074 1388.771 182.8895 1275.699 183.3716 1150.289 183.8537 1044.311 184.3358 959.1221 184.8179 888.3340 185.3001 830.0957 185.7822 784.5020 186.2643 742.8535 186.7464 707.0557 187.2285 671.9023 187.7106 632.1328 188.1928 586.3604 188.6749 540.9326 189.1570 498.5244 189.6391 453.3486 190.1212 435.0146 190.6033 467.3076 191.0855 520.0977 191.5676 572.6650 192.0497 617.5400 192.5318 661.3809 193.0139 716.0586 193.4960 781.0322 193.9782 859.7607 194.4603 950.5684 194.9424 1053.062 195.4245 1166.866 195.9066 1291.771 196.3887 1427.635 196.8709 1575.617 197.3530 1740.726 197.8351 1912.521 198.3172 2078.499 198.7993 2251.873 199.2814 2452.137 199.7636 2690.142 200.2457 2961.444 200.7278 3234.697 201.2099 3491.475 201.6920 3742.045 202.1741 4031.512 202.6563 4346.256 203.1384 4657.188 203.6205 4940.502 204.1026 5199.494 204.5847 5512.283 205.0668 5937.977 205.5490 6356.551 206.0311 6723.779 206.5132 7051.088 206.9953 7371.486 207.4774 7709.645 207.9595 8067.740 208.4417 8429.616 208.9238 8799.431 209.4059 9169.165 209.8880 9538.779 210.3701 9905.110 210.8522 10259.03 211.3344 10590.17 211.8165 10894.00 212.2986 11195.52 212.7807 11511.98 213.2628 11813.57 213.7449 12078.30 214.2271 12304.75 214.7092 12512.58 215.1913 12720.58 215.6734 12929.54 216.1555 13103.55 216.6376 13244.38 217.1198 13348.17 217.6019 13408.12 218.0840 13423.42 218.5661 13404.30 219.0482 13357.99 219.5303 13284.14 220.0125 13178.26 220.4946 13031.75 220.9767 12856.14 221.4588 12660.92 221.9409 12444.62 222.4230 12219.09 222.9052 11986.38 223.3873 11747.91 223.8694 11533.74 224.3515 11354.26 224.8336 11201.11 225.3158 11059.93 225.7979 10925.89 226.2800 10810.53 226.7621 10727.62 227.2442 10672.37 227.7263 10633.27 228.2085 10594.29 228.6906 10569.30 229.1727 10591.68 229.6548 10672.09 230.1369 10791.04 230.6190 10935.99 231.1012 11103.03 231.5833 11278.51 232.0654 11442.43 232.5475 11606.58 233.0296 11818.38 233.5117 12107.20 233.9939 12410.41 234.4760 12670.64 234.9581 12896.32 235.4402 13136.98 235.9223 13428.76 236.4044 13762.41 236.8866 14092.24 237.3687 14403.48 237.8508 14723.65 238.3329 15079.86 238.8150 15464.14 239.2971 15840.81 239.7793 16180.54 240.2614 16486.82 240.7435 16788.54 241.2256 17078.34 241.7077 17373.92 242.1898 17698.42 242.6720 18042.66 243.1541 18366.01 243.6362 18638.85 244.1183 18861.55 244.6004 19045.29 245.0825 19179.41 245.5647 19280.27 246.0468 19366.85 246.5289 19433.89 247.0110 19458.11 247.4931 19416.84 247.9752 19308.70 248.4574 19167.03 248.9395 18997.10 249.4216 18781.34 249.9037 18500.70 250.3858 18162.34 250.8679 17801.50 251.3501 17449.93 251.8322 17110.54 252.3143 16741.78 252.7964 16337.96 253.2785 15907.51 253.7606 15439.97 254.2428 14942.46 254.7249 14442.03 255.2070 13966.83 255.6891 13518.87 256.1712 13055.32 256.6534 12566.53 257.1355 12068.54 257.6176 11563.52 258.0997 11054.94 258.5818 10549.52 259.0639 10058.34 259.5461 9583.528 260.0282 9104.818 260.5103 8599.717 260.9924 8111.481 261.4745 7647.960 261.9566 7214.791 262.4388 6820.595 262.9209 6471.471 263.4030 6172.998 263.8851 5865.698 264.3672 5525.958 264.8493 5205.072 265.3315 4922.659 265.8136 4672.965 266.2957 4434.812 266.7778 4190.316 267.2599 3937.960 267.7420 3710.671 268.2242 3525.478 268.7063 3349.615 269.1884 3176.923 269.6705 3006.079 270.1526 2834.553 270.6347 2654.975 271.1169 2465.200 271.5990 2326.970 272.0811 2298.650 272.5632 2267.576 273.0453 2198.111 273.5274 2101.628 274.0096 2009.175 274.4917 1942.726 274.9738 1901.522 275.4559 1871.120 275.9380 1853.166 276.4201 1843.465 276.9023 1842.034 277.3844 1849.548 277.8665 1868.679 278.3486 1903.343 278.8307 1950.380 279.3128 1978.097 279.7950 1961.094 280.2771 1952.184 280.7592 1966.082 281.2413 1996.732 281.7234 2033.728 282.2055 2071.348 282.6877 2107.637 283.1698 2131.475 283.6519 2118.273 284.1340 2121.642 284.6161 2166.717 285.0982 2230.413 285.5804 2282.173 286.0625 2305.250 286.5446 2305.309 287.0267 2302.662 287.5088 2291.692 287.9909 2284.705 288.4731 2284.073 288.9552 2287.519 289.4373 2296.177 289.9194 2311.783 290.4015 2326.412 290.8836 2315.470 291.3658 2256.005 291.8479 2204.447 292.3300 2175.176 292.8121 2153.304 293.2942 2123.973 293.7763 2081.213 294.2585 2029.289 294.7406 1976.398 295.2227 1917.743 295.7048 1866.500 296.1869 1829.884 296.6690 1796.312 297.1512 1756.390 297.6333 1706.730 298.1154 1651.865 298.5975 1598.546 299.0796 1542.294 299.5617 1497.807 300.0439 1480.022 300.5260 1462.897 301.0081 1426.457 301.4902 1367.565 301.9723 1298.958 302.4544 1236.286 302.9366 1178.275 303.4187 1131.254 303.9008 1112.549 304.3829 1091.406 304.8650 1045.961 305.3471 976.9487 305.8293 905.7109 306.3114 857.0635 306.7935 837.4062 307.2756 810.8398 307.7577 779.3750 308.2398 739.1973 308.7220 682.6147 309.2041 613.1704 309.6862 544.0752 310.1683 486.4932 310.6504 440.6416 311.1325 396.6299 311.6147 354.1929 312.0968 313.1392 312.5789 274.3599 313.0610 236.8911 313.5431 197.1338 314.0252 150.6523 314.5074 99.24072 314.9895 59.70166 315.4716 40.38916 315.9537 23.29248 316.4358 1.648438 316.9179 22.41162 317.4001 43.56738 317.8822 56.22314 318.3643 65.91113 318.8464 94.36670 319.3285 159.9229 319.8106 208.7305 320.2928 208.6040 320.7749 188.3442 321.2570 184.1616 321.7391 214.4155 322.2212 260.1304 322.7033 284.5376 323.1855 282.0830 323.6676 275.8687 324.1497 272.1257 324.6318 268.9375 325.1139 264.2644 325.5960 257.1733 326.0782 250.0784 326.5603 245.5901 327.0424 243.4883 327.5245 245.2693 328.0066 260.7986 328.4887 273.6465 328.9709 268.0549 329.4530 241.4646 329.9351 210.8113 330.4172 188.9470 330.8993 175.7161 331.3814 169.0427 331.8636 175.8611 332.3457 180.9976 332.8278 170.6309 333.3099 145.4612 333.7920 119.5923 334.2741 104.7021 334.7563 96.45337 335.2384 78.04126 335.7205 43.17334 336.2026 6.116943 336.6847 24.89478 337.1668 49.51172 337.6490 63.62476 338.1311 55.43726 338.6132 38.69067 339.0953 37.72461 339.5774 55.64990 340.0595 80.24487 340.5417 103.0552 341.0238 125.9341 341.5059 154.1565 341.9880 201.8870 342.4701 246.7356 342.9522 262.0955 343.4344 248.7180 343.9165 233.4141 344.3986 227.3545 344.8807 232.9702 345.3628 251.7534 345.8449 296.5881 346.3271 339.2656 346.8092 358.7383 347.2913 361.0701 347.7734 368.2051 348.2555 389.4465 348.7376 420.9712 349.2198 454.5024 349.7019 491.1611 350.1840 526.8062 350.6661 562.8525 351.1482 596.5273 351.6303 620.6719 352.1125 632.1404 352.5946 640.8347 353.0767 662.2183 353.5588 700.0046 354.0409 738.7625 354.5230 775.5371 355.0052 813.8911 355.4873 859.8948 355.9694 913.5605 356.4515 965.1179 356.9336 1002.521 357.4157 1020.835 357.8979 1055.235 358.3800 1117.564 358.8621 1183.860 359.3442 1239.929 359.8263 1287.323 360.3084 1337.655 360.7906 1400.422 361.2727 1474.824 361.7548 1537.120 362.2369 1566.136 362.7190 1607.252 363.2011 1679.028 363.6833 1769.104 364.1654 1859.586 364.6475 1941.762 365.1296 2015.428 365.6117 2077.863 366.0938 2113.822 366.5760 2159.430 367.0581 2228.581 367.5402 2302.239 368.0223 2362.445 368.5044 2404.172 368.9865 2435.592 369.4687 2466.926 369.9508 2494.513 370.4329 2532.523 370.9150 2602.104 371.3971 2665.205 371.8792 2696.068 372.3614 2696.889 372.8435 2690.658 373.3256 2700.219 373.8077 2726.098 374.2898 2741.567 374.7719 2746.853 375.2541 2738.640 375.7362 2710.472 376.2183 2669.003 376.7004 2627.515 377.1825 2596.197 377.6646 2566.011 378.1468 2509.291 378.6289 2413.433 379.1110 2326.151 379.5931 2278.613 380.0752 2243.311 380.5573 2190.602 381.0395 2109.616 381.5216 2021.124 382.0037 1949.084 382.4858 1893.776 382.9679 1836.832 383.4500 1775.512 383.9322 1707.249 384.4143 1626.485 384.8964 1529.578 385.3785 1441.591 385.8606 1382.276 386.3427 1341.651 386.8249 1295.598 387.3070 1240.436 387.7891 1181.221 388.2712 1118.642 388.7533 1052.785 389.2354 995.0518 389.7176 947.5625 390.1997 908.3872 390.6818 882.5693 391.1639 869.7024 391.6460 850.2483 392.1281 806.0088 392.6103 739.6296 393.0924 688.0994 393.5745 662.6033 394.0566 641.4668 394.5387 616.2034 395.0208 587.3987 395.5030 556.2349 395.9851 521.9175 396.4672 486.2095 396.9493 456.3811 397.4314 445.7700 397.9135 426.2258 398.3957 386.7427 398.8778 342.7932 399.3599 309.3152 399.8420 290.2612 400.3241 279.3418 400.8062 268.1597 401.2884 255.8359 401.7705 242.0027 402.2526 228.1172 402.7347 212.4937 403.2168 191.7727 403.6989 169.2859 404.1811 151.8000 404.6632 144.7629 405.1453 146.2664 405.6274 143.3206 406.1095 130.9939 406.5916 122.1272 407.0738 122.1323 407.5559 126.3442 408.0380 129.7158 408.5201 130.4568 409.0022 127.7893 409.4843 118.4031 409.9665 100.0308 410.4486 85.80371 410.9307 84.32837 411.4128 84.85962 411.8949 79.24707 412.3770 66.77954 412.8592 52.53687 413.3413 38.87231 413.8234 26.34717 414.3055 17.74048 414.7876 14.93091 415.2697 12.50586 415.7519 3.662842 416.2340 8.911377 416.7161 15.98486 417.1982 10.28589 417.6803 1.385742 418.1624 1.698486 418.6446 10.62012 419.1267 14.99341 419.6088 6.002930 420.0909 12.46460 420.5730 27.07617 421.0551 43.20117 421.5373 48.62183 422.0194 28.00854 422.5015 3.759033 422.9836 19.87451 423.4657 11.33887 423.9478 8.147217 424.4300 17.78833 424.9121 13.73120 425.3942 7.857910 425.8763 3.804932 426.3584 14.09570 426.8405 20.70093 427.3227 21.90186 427.8048 12.61572 428.2869 14.08130 428.7690 57.12671 429.2511 79.93677 429.7332 56.52197 430.2154 39.37964 430.6975 44.94946 431.1796 60.27490 431.6617 67.15771 432.1438 57.50488 432.6259 39.03491 433.1081 24.61914 433.5902 12.65112 434.0723 10.06396 434.5544 23.79541 435.0365 43.34082 435.5186 67.23901 436.0008 93.44946 436.4829 111.7014 436.9650 105.5042 437.4471 82.06812 437.9292 80.90186 438.4113 115.4639 438.8935 148.2288 439.3756 148.1799 439.8577 128.6514 440.3398 115.9692 440.8219 121.8091 441.3040 133.1338 441.7862 136.6733 442.2683 133.5010 442.7504 132.1648 443.2325 135.5198 443.7146 143.7515 444.1967 158.6768 444.6789 184.1003 445.1610 205.0669 445.6431 210.9941 446.1252 212.9553 446.6073 227.4194 447.0894 256.7739 447.5716 286.8997 448.0537 302.0127 448.5358 299.1780 449.0179 301.8411 449.5000 310.5740 449.9821 323.1738 450.4643 340.0081 450.9464 359.8374 451.4285 382.1150 451.9106 407.0239 452.3927 430.8586 452.8748 441.2898 453.3570 427.8027 453.8391 419.0015 454.3212 415.8259 454.8033 419.1243 455.2854 432.6350 455.7675 455.6045 456.2497 479.0117 456.7318 492.4648 457.2139 496.3677 457.6960 504.7698 458.1782 522.0713 458.6603 538.2761 459.1424 548.4282 459.6245 553.6719 460.1066 555.8025 460.5887 551.8750 461.0709 548.7095 461.5530 557.6743 462.0351 578.3457 462.5172 594.3420 462.9993 595.3438 463.4814 591.5525 463.9636 601.4019 464.4457 627.4822 464.9278 655.9004 465.4099 682.7866 465.8920 709.2070 466.3741 738.5139 466.8563 770.8176 467.3384 797.9001 467.8205 810.4375 468.3026 807.1543 468.7847 810.0583 469.2668 824.7327 469.7490 838.7627 470.2311 843.5571 470.7132 845.1223 471.1953 855.9121 471.6774 882.1558 472.1595 915.1348 472.6417 933.0859 473.1238 920.9316 473.6059 925.9436 474.0880 969.6155 474.5701 1014.701 475.0522 1033.255 475.5344 1027.550 476.0165 1023.940 476.4986 1046.585 476.9807 1090.432 477.4628 1127.096 477.9449 1156.648 478.4271 1178.342 478.9092 1182.362 479.3913 1181.175 479.8734 1194.144 480.3555 1233.065 480.8376 1270.164 481.3198 1278.799 481.8019 1265.314 482.2840 1254.260 482.7661 1251.768 483.2482 1255.407 483.7303 1264.397 484.2125 1279.807 484.6946 1289.272 485.1767 1292.200 485.6588 1288.088 486.1409 1273.096 486.6230 1249.566 487.1052 1226.225 487.5873 1209.025 488.0694 1196.312 488.5515 1181.027 489.0336 1174.610 489.5157 1149.899 489.9979 1090.566 490.4800 1020.877 490.9621 960.0552 491.4442 913.2083 491.9263 876.8574 492.4084 851.9023 492.8906 840.3179 493.3727 808.6436 493.8548 734.4431 494.3369 669.4927 494.8190 645.3406 495.3011 642.7664 495.7833 625.9150 496.2654 574.8643 496.7475 516.3188 497.2296 483.2510 497.7117 474.5803 498.1938 472.7920 498.6760 477.4404 499.1581 480.3909 499.6402 466.0801 500.1223 432.8337 500.6044 412.3625 501.0865 419.1213 501.5687 438.0981 502.0508 455.8145 502.5329 471.2949 503.0150 488.6279 503.4971 511.4446 503.9792 537.9026 504.4614 557.2141 504.9435 557.6072 505.4256 565.8440 505.9077 590.0347 506.3898 620.7322 506.8719 648.9407 507.3541 672.5471 507.8362 694.7014 508.3183 719.9631 508.8004 748.9504 509.2825 772.3049 509.7646 790.5835 510.2468 801.6040 510.7289 799.4941 511.2110 791.3906 511.6931 789.1377 512.1752 798.2219 512.6573 812.1782 513.1395 825.4136 513.6216 837.6841 514.1037 844.2129 514.5858 842.6616 515.0679 836.6833 515.5500 827.8975 516.0322 816.0603 516.5143 812.2483 516.9964 834.6963 517.4785 854.2319 517.9606 840.1997 518.4427 797.8411 518.9249 754.1992 519.4070 724.3259 519.8891 706.9102 520.3712 697.5447 520.8533 712.1667 521.3354 712.7822 521.8176 687.7922 522.2997 655.6460 522.7818 630.4097 523.2639 613.8623 523.7460 600.5347 524.2281 583.9722 524.7103 565.6052 525.1924 561.7556 525.6745 586.4080 526.1566 599.4531 526.6387 573.3687 527.1208 532.8748 527.6030 507.0869 528.0851 503.7747 528.5672 509.3779 529.0493 517.5601 529.5314 526.1987 530.0135 526.4219 530.4957 514.6313 530.9778 503.4172 531.4599 507.7288 531.9420 527.3096 532.4241 531.5750 532.9063 508.0298 533.3884 481.3242 533.8705 457.4177 534.3526 440.2456 534.8347 439.4631 535.3168 458.8691 535.7990 483.5513 536.2811 486.1873 536.7632 453.0820 537.2453 432.9712 537.7274 434.2627 538.2095 440.3940 538.6917 448.0461 539.1738 454.5020 539.6559 454.5806 540.1380 442.9888 540.6201 428.9094 541.1022 431.2664 541.5844 451.6658 542.0665 470.9482 542.5486 484.2761 543.0307 493.1313 543.5128 500.1299 543.9949 506.0854 544.4771 509.7329 544.9592 506.3909 545.4413 500.6741 545.9234 496.7568 546.4055 495.7285 546.8876 500.6172 547.3698 514.2117 547.8519 533.8281 548.3340 549.1118 548.8161 562.1497 549.2982 566.8918 549.7803 551.1084 550.2625 536.2151 550.7446 539.9961 551.2267 562.4937 551.7088 592.8625 552.1909 626.7812 552.6730 660.8516 553.1552 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