#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-04-26 13:43:31 +0300 (Thu, 26 Apr 2018) $
#$Revision: 532 $
#$URL: svn://172.16.1.111/rod/cif/1/00/00/1000084.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000084
loop_
_publ_author_name
'Rastsvetaeva, R. K.'
'Tamazyan, R. A.'
'Pushcharovskii D Yu'
'Nadezhina, T. N.'
'Voloshin, A. V.'
_publ_section_title
;
 K-nenadkevichite, a new representative of the nenadkevichite-labuntsovite
 series
;
_journal_name_full               'Crystallography Reports'
_journal_page_first              908
_journal_page_last               914
_journal_volume                  39
_journal_year                    1994
_chemical_compound_source        'Vuoriyarvi, Kola Peninsula'
_chemical_formula_sum            'H10.3 K2.98 Na1.22 Nb2.2 O31.15 Si8 Ti1.8'
_chemical_name_mineral           Vuoriyarvite
_space_group_IT_number           8
_symmetry_space_group_name_Hall  'C -2y'
_symmetry_space_group_name_H-M   'C 1 m 1'
_cell_angle_alpha                90
_cell_angle_beta                 117.87
_cell_angle_gamma                90
_cell_length_a                   14.692
_cell_length_b                   14.164
_cell_length_c                   7.859
_cell_volume                     1445.745
_exptl_crystal_density_diffrn    2.684
_cod_original_formula_sum        'Si8 (Nb2.2 Ti1.8) K2.98 Na1.22 O31.15 H10.3'
_cod_database_code               9014345
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type helium-neon
_raman_measurement_device.excitation_laser_wavelength 780
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 12
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R070610.rod
_rod_data_source.block           3500000
_rod_database.code               1000084
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9014345 COD http://www.crystallography.net/cod/9014345.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
143.8380 0.0000000E+00
144.3201 70.58301
144.8022 77.13379
145.2844 125.2842
145.7665 142.8574
146.2486 58.87988
146.7307 14.23145
147.2128 51.02441
147.6949 48.53223
148.1771 17.74121
148.6592 37.87500
149.1413 114.2061
149.6234 194.9561
150.1055 264.6895
150.5877 332.1504
151.0698 429.4492
151.5519 570.0352
152.0340 731.7383
152.5161 888.8311
152.9982 1041.019
153.4804 1201.751
153.9625 1386.952
154.4446 1598.354
154.9267 1800.664
155.4088 1962.828
155.8909 2127.292
156.3731 2325.461
156.8552 2563.781
157.3373 2823.237
157.8194 3078.407
158.3015 3328.743
158.7836 3578.553
159.2658 3828.605
159.7479 4079.444
160.2300 4332.190
160.7121 4588.451
161.1942 4843.876
161.6763 5081.492
162.1585 5282.368
162.6406 5486.861
163.1227 5728.504
163.6048 5971.613
164.0869 6167.725
164.5690 6283.220
165.0512 6327.008
165.5333 6385.637
166.0154 6483.291
166.4975 6571.807
166.9796 6661.744
167.4617 6734.752
167.9439 6754.240
168.4260 6686.508
168.9081 6524.127
169.3902 6360.480
169.8723 6207.898
170.3544 6045.035
170.8366 5857.260
171.3187 5645.969
171.8008 5427.018
172.2829 5216.722
172.7650 5019.903
173.2471 4795.758
173.7293 4512.356
174.2114 4221.293
174.6935 3969.251
175.1756 3765.235
175.6577 3586.426
176.1398 3413.602
176.6220 3249.641
177.1041 3067.881
177.5862 2844.276
178.0683 2602.992
178.5504 2384.057
179.0325 2197.820
179.5147 2033.970
179.9968 1877.624
180.4789 1725.778
180.9610 1595.729
181.4431 1511.114
181.9252 1459.181
182.4074 1388.771
182.8895 1275.699
183.3716 1150.289
183.8537 1044.311
184.3358 959.1221
184.8179 888.3340
185.3001 830.0957
185.7822 784.5020
186.2643 742.8535
186.7464 707.0557
187.2285 671.9023
187.7106 632.1328
188.1928 586.3604
188.6749 540.9326
189.1570 498.5244
189.6391 453.3486
190.1212 435.0146
190.6033 467.3076
191.0855 520.0977
191.5676 572.6650
192.0497 617.5400
192.5318 661.3809
193.0139 716.0586
193.4960 781.0322
193.9782 859.7607
194.4603 950.5684
194.9424 1053.062
195.4245 1166.866
195.9066 1291.771
196.3887 1427.635
196.8709 1575.617
197.3530 1740.726
197.8351 1912.521
198.3172 2078.499
198.7993 2251.873
199.2814 2452.137
199.7636 2690.142
200.2457 2961.444
200.7278 3234.697
201.2099 3491.475
201.6920 3742.045
202.1741 4031.512
202.6563 4346.256
203.1384 4657.188
203.6205 4940.502
204.1026 5199.494
204.5847 5512.283
205.0668 5937.977
205.5490 6356.551
206.0311 6723.779
206.5132 7051.088
206.9953 7371.486
207.4774 7709.645
207.9595 8067.740
208.4417 8429.616
208.9238 8799.431
209.4059 9169.165
209.8880 9538.779
210.3701 9905.110
210.8522 10259.03
211.3344 10590.17
211.8165 10894.00
212.2986 11195.52
212.7807 11511.98
213.2628 11813.57
213.7449 12078.30
214.2271 12304.75
214.7092 12512.58
215.1913 12720.58
215.6734 12929.54
216.1555 13103.55
216.6376 13244.38
217.1198 13348.17
217.6019 13408.12
218.0840 13423.42
218.5661 13404.30
219.0482 13357.99
219.5303 13284.14
220.0125 13178.26
220.4946 13031.75
220.9767 12856.14
221.4588 12660.92
221.9409 12444.62
222.4230 12219.09
222.9052 11986.38
223.3873 11747.91
223.8694 11533.74
224.3515 11354.26
224.8336 11201.11
225.3158 11059.93
225.7979 10925.89
226.2800 10810.53
226.7621 10727.62
227.2442 10672.37
227.7263 10633.27
228.2085 10594.29
228.6906 10569.30
229.1727 10591.68
229.6548 10672.09
230.1369 10791.04
230.6190 10935.99
231.1012 11103.03
231.5833 11278.51
232.0654 11442.43
232.5475 11606.58
233.0296 11818.38
233.5117 12107.20
233.9939 12410.41
234.4760 12670.64
234.9581 12896.32
235.4402 13136.98
235.9223 13428.76
236.4044 13762.41
236.8866 14092.24
237.3687 14403.48
237.8508 14723.65
238.3329 15079.86
238.8150 15464.14
239.2971 15840.81
239.7793 16180.54
240.2614 16486.82
240.7435 16788.54
241.2256 17078.34
241.7077 17373.92
242.1898 17698.42
242.6720 18042.66
243.1541 18366.01
243.6362 18638.85
244.1183 18861.55
244.6004 19045.29
245.0825 19179.41
245.5647 19280.27
246.0468 19366.85
246.5289 19433.89
247.0110 19458.11
247.4931 19416.84
247.9752 19308.70
248.4574 19167.03
248.9395 18997.10
249.4216 18781.34
249.9037 18500.70
250.3858 18162.34
250.8679 17801.50
251.3501 17449.93
251.8322 17110.54
252.3143 16741.78
252.7964 16337.96
253.2785 15907.51
253.7606 15439.97
254.2428 14942.46
254.7249 14442.03
255.2070 13966.83
255.6891 13518.87
256.1712 13055.32
256.6534 12566.53
257.1355 12068.54
257.6176 11563.52
258.0997 11054.94
258.5818 10549.52
259.0639 10058.34
259.5461 9583.528
260.0282 9104.818
260.5103 8599.717
260.9924 8111.481
261.4745 7647.960
261.9566 7214.791
262.4388 6820.595
262.9209 6471.471
263.4030 6172.998
263.8851 5865.698
264.3672 5525.958
264.8493 5205.072
265.3315 4922.659
265.8136 4672.965
266.2957 4434.812
266.7778 4190.316
267.2599 3937.960
267.7420 3710.671
268.2242 3525.478
268.7063 3349.615
269.1884 3176.923
269.6705 3006.079
270.1526 2834.553
270.6347 2654.975
271.1169 2465.200
271.5990 2326.970
272.0811 2298.650
272.5632 2267.576
273.0453 2198.111
273.5274 2101.628
274.0096 2009.175
274.4917 1942.726
274.9738 1901.522
275.4559 1871.120
275.9380 1853.166
276.4201 1843.465
276.9023 1842.034
277.3844 1849.548
277.8665 1868.679
278.3486 1903.343
278.8307 1950.380
279.3128 1978.097
279.7950 1961.094
280.2771 1952.184
280.7592 1966.082
281.2413 1996.732
281.7234 2033.728
282.2055 2071.348
282.6877 2107.637
283.1698 2131.475
283.6519 2118.273
284.1340 2121.642
284.6161 2166.717
285.0982 2230.413
285.5804 2282.173
286.0625 2305.250
286.5446 2305.309
287.0267 2302.662
287.5088 2291.692
287.9909 2284.705
288.4731 2284.073
288.9552 2287.519
289.4373 2296.177
289.9194 2311.783
290.4015 2326.412
290.8836 2315.470
291.3658 2256.005
291.8479 2204.447
292.3300 2175.176
292.8121 2153.304
293.2942 2123.973
293.7763 2081.213
294.2585 2029.289
294.7406 1976.398
295.2227 1917.743
295.7048 1866.500
296.1869 1829.884
296.6690 1796.312
297.1512 1756.390
297.6333 1706.730
298.1154 1651.865
298.5975 1598.546
299.0796 1542.294
299.5617 1497.807
300.0439 1480.022
300.5260 1462.897
301.0081 1426.457
301.4902 1367.565
301.9723 1298.958
302.4544 1236.286
302.9366 1178.275
303.4187 1131.254
303.9008 1112.549
304.3829 1091.406
304.8650 1045.961
305.3471 976.9487
305.8293 905.7109
306.3114 857.0635
306.7935 837.4062
307.2756 810.8398
307.7577 779.3750
308.2398 739.1973
308.7220 682.6147
309.2041 613.1704
309.6862 544.0752
310.1683 486.4932
310.6504 440.6416
311.1325 396.6299
311.6147 354.1929
312.0968 313.1392
312.5789 274.3599
313.0610 236.8911
313.5431 197.1338
314.0252 150.6523
314.5074 99.24072
314.9895 59.70166
315.4716 40.38916
315.9537 23.29248
316.4358 1.648438
316.9179 22.41162
317.4001 43.56738
317.8822 56.22314
318.3643 65.91113
318.8464 94.36670
319.3285 159.9229
319.8106 208.7305
320.2928 208.6040
320.7749 188.3442
321.2570 184.1616
321.7391 214.4155
322.2212 260.1304
322.7033 284.5376
323.1855 282.0830
323.6676 275.8687
324.1497 272.1257
324.6318 268.9375
325.1139 264.2644
325.5960 257.1733
326.0782 250.0784
326.5603 245.5901
327.0424 243.4883
327.5245 245.2693
328.0066 260.7986
328.4887 273.6465
328.9709 268.0549
329.4530 241.4646
329.9351 210.8113
330.4172 188.9470
330.8993 175.7161
331.3814 169.0427
331.8636 175.8611
332.3457 180.9976
332.8278 170.6309
333.3099 145.4612
333.7920 119.5923
334.2741 104.7021
334.7563 96.45337
335.2384 78.04126
335.7205 43.17334
336.2026 6.116943
336.6847 24.89478
337.1668 49.51172
337.6490 63.62476
338.1311 55.43726
338.6132 38.69067
339.0953 37.72461
339.5774 55.64990
340.0595 80.24487
340.5417 103.0552
341.0238 125.9341
341.5059 154.1565
341.9880 201.8870
342.4701 246.7356
342.9522 262.0955
343.4344 248.7180
343.9165 233.4141
344.3986 227.3545
344.8807 232.9702
345.3628 251.7534
345.8449 296.5881
346.3271 339.2656
346.8092 358.7383
347.2913 361.0701
347.7734 368.2051
348.2555 389.4465
348.7376 420.9712
349.2198 454.5024
349.7019 491.1611
350.1840 526.8062
350.6661 562.8525
351.1482 596.5273
351.6303 620.6719
352.1125 632.1404
352.5946 640.8347
353.0767 662.2183
353.5588 700.0046
354.0409 738.7625
354.5230 775.5371
355.0052 813.8911
355.4873 859.8948
355.9694 913.5605
356.4515 965.1179
356.9336 1002.521
357.4157 1020.835
357.8979 1055.235
358.3800 1117.564
358.8621 1183.860
359.3442 1239.929
359.8263 1287.323
360.3084 1337.655
360.7906 1400.422
361.2727 1474.824
361.7548 1537.120
362.2369 1566.136
362.7190 1607.252
363.2011 1679.028
363.6833 1769.104
364.1654 1859.586
364.6475 1941.762
365.1296 2015.428
365.6117 2077.863
366.0938 2113.822
366.5760 2159.430
367.0581 2228.581
367.5402 2302.239
368.0223 2362.445
368.5044 2404.172
368.9865 2435.592
369.4687 2466.926
369.9508 2494.513
370.4329 2532.523
370.9150 2602.104
371.3971 2665.205
371.8792 2696.068
372.3614 2696.889
372.8435 2690.658
373.3256 2700.219
373.8077 2726.098
374.2898 2741.567
374.7719 2746.853
375.2541 2738.640
375.7362 2710.472
376.2183 2669.003
376.7004 2627.515
377.1825 2596.197
377.6646 2566.011
378.1468 2509.291
378.6289 2413.433
379.1110 2326.151
379.5931 2278.613
380.0752 2243.311
380.5573 2190.602
381.0395 2109.616
381.5216 2021.124
382.0037 1949.084
382.4858 1893.776
382.9679 1836.832
383.4500 1775.512
383.9322 1707.249
384.4143 1626.485
384.8964 1529.578
385.3785 1441.591
385.8606 1382.276
386.3427 1341.651
386.8249 1295.598
387.3070 1240.436
387.7891 1181.221
388.2712 1118.642
388.7533 1052.785
389.2354 995.0518
389.7176 947.5625
390.1997 908.3872
390.6818 882.5693
391.1639 869.7024
391.6460 850.2483
392.1281 806.0088
392.6103 739.6296
393.0924 688.0994
393.5745 662.6033
394.0566 641.4668
394.5387 616.2034
395.0208 587.3987
395.5030 556.2349
395.9851 521.9175
396.4672 486.2095
396.9493 456.3811
397.4314 445.7700
397.9135 426.2258
398.3957 386.7427
398.8778 342.7932
399.3599 309.3152
399.8420 290.2612
400.3241 279.3418
400.8062 268.1597
401.2884 255.8359
401.7705 242.0027
402.2526 228.1172
402.7347 212.4937
403.2168 191.7727
403.6989 169.2859
404.1811 151.8000
404.6632 144.7629
405.1453 146.2664
405.6274 143.3206
406.1095 130.9939
406.5916 122.1272
407.0738 122.1323
407.5559 126.3442
408.0380 129.7158
408.5201 130.4568
409.0022 127.7893
409.4843 118.4031
409.9665 100.0308
410.4486 85.80371
410.9307 84.32837
411.4128 84.85962
411.8949 79.24707
412.3770 66.77954
412.8592 52.53687
413.3413 38.87231
413.8234 26.34717
414.3055 17.74048
414.7876 14.93091
415.2697 12.50586
415.7519 3.662842
416.2340 8.911377
416.7161 15.98486
417.1982 10.28589
417.6803 1.385742
418.1624 1.698486
418.6446 10.62012
419.1267 14.99341
419.6088 6.002930
420.0909 12.46460
420.5730 27.07617
421.0551 43.20117
421.5373 48.62183
422.0194 28.00854
422.5015 3.759033
422.9836 19.87451
423.4657 11.33887
423.9478 8.147217
424.4300 17.78833
424.9121 13.73120
425.3942 7.857910
425.8763 3.804932
426.3584 14.09570
426.8405 20.70093
427.3227 21.90186
427.8048 12.61572
428.2869 14.08130
428.7690 57.12671
429.2511 79.93677
429.7332 56.52197
430.2154 39.37964
430.6975 44.94946
431.1796 60.27490
431.6617 67.15771
432.1438 57.50488
432.6259 39.03491
433.1081 24.61914
433.5902 12.65112
434.0723 10.06396
434.5544 23.79541
435.0365 43.34082
435.5186 67.23901
436.0008 93.44946
436.4829 111.7014
436.9650 105.5042
437.4471 82.06812
437.9292 80.90186
438.4113 115.4639
438.8935 148.2288
439.3756 148.1799
439.8577 128.6514
440.3398 115.9692
440.8219 121.8091
441.3040 133.1338
441.7862 136.6733
442.2683 133.5010
442.7504 132.1648
443.2325 135.5198
443.7146 143.7515
444.1967 158.6768
444.6789 184.1003
445.1610 205.0669
445.6431 210.9941
446.1252 212.9553
446.6073 227.4194
447.0894 256.7739
447.5716 286.8997
448.0537 302.0127
448.5358 299.1780
449.0179 301.8411
449.5000 310.5740
449.9821 323.1738
450.4643 340.0081
450.9464 359.8374
451.4285 382.1150
451.9106 407.0239
452.3927 430.8586
452.8748 441.2898
453.3570 427.8027
453.8391 419.0015
454.3212 415.8259
454.8033 419.1243
455.2854 432.6350
455.7675 455.6045
456.2497 479.0117
456.7318 492.4648
457.2139 496.3677
457.6960 504.7698
458.1782 522.0713
458.6603 538.2761
459.1424 548.4282
459.6245 553.6719
460.1066 555.8025
460.5887 551.8750
461.0709 548.7095
461.5530 557.6743
462.0351 578.3457
462.5172 594.3420
462.9993 595.3438
463.4814 591.5525
463.9636 601.4019
464.4457 627.4822
464.9278 655.9004
465.4099 682.7866
465.8920 709.2070
466.3741 738.5139
466.8563 770.8176
467.3384 797.9001
467.8205 810.4375
468.3026 807.1543
468.7847 810.0583
469.2668 824.7327
469.7490 838.7627
470.2311 843.5571
470.7132 845.1223
471.1953 855.9121
471.6774 882.1558
472.1595 915.1348
472.6417 933.0859
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1233.904 410.8340
1234.386 390.4761
1234.868 388.7412
1235.350 387.1357
1235.833 370.3064
1236.315 345.6304
1236.797 324.9373
1237.279 309.6001
1237.761 314.6113
1238.243 333.9253
1238.725 333.6323
1239.207 312.5366
1239.689 293.7498
1240.172 287.0234
1240.654 290.4150
1241.136 310.2097
1241.618 326.0247
1242.100 308.5254
1242.582 280.9128
1243.064 276.1013
1243.546 278.2539
1244.028 250.7061
1244.511 197.7615
1244.993 163.6409
1245.475 164.8398
1245.957 172.7988
1246.439 195.2610
1246.921 201.7698
1247.403 166.0151
1247.885 126.5002
1248.368 108.4104
1248.850 105.3958
1249.332 109.4153
1249.814 120.0696
1250.296 124.8755
1250.778 125.4895
1251.260 109.4841
1251.742 72.68188
1252.224 39.44287
1252.707 16.99902
1253.189 11.91479
1253.671 32.24219
1254.153 60.77930
1254.635 65.05054
1255.117 52.64941
1255.599 43.27222
1256.081 36.15820
1256.563 27.74829
1257.046 18.09888
1257.528 8.813232
1258.010 0.7431640
1258.492 3.185303
1258.974 1.525391
1259.456 8.104248
1259.938 6.131104
1260.420 0.0000000E+00
