#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-04-26 13:43:35 +0300 (Thu, 26 Apr 2018) $
#$Revision: 533 $
#$URL: svn://172.16.1.111/rod/cif/1/00/00/1000085.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000085
loop_
_publ_author_name
'Yakubovich, O. V.'
'Massa, W.'
'Chukanov, N. V.'
_publ_section_title
;
 Crystal structure of britvinite
 [Pb7(OH)3F(BO3)2(CO3)][Mg4.5(OH)3(Si5O14)]: A new layered silicate with
 an original type of silicon-oxygen networks Locality: Varmland, Sweden
;
_journal_name_full               'Crystallography Reports'
_journal_page_first              206
_journal_page_last               215
_journal_paper_doi               10.1134/S1063774508020077
_journal_volume                  53
_journal_year                    2008
_chemical_compound_source        R070639
_chemical_formula_sum            'C2 B3.468 F2 Mg9 O58 Pb14.144 Si10.532'
_chemical_name_mineral           Britvinite
_space_group_IT_number           2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                80.365
_cell_angle_beta                 75.816
_cell_angle_gamma                59.870
_cell_length_a                   9.3409
_cell_length_b                   9.3579
_cell_length_c                   18.8333
_cell_volume                     1378.475
_exptl_crystal_density_diffrn    5.388
_cod_original_formula_sum        'Si10.532 Mg9 Pb14.144 C2 B3.468 O58 F2'
_cod_database_code               9012668
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type helium-neon
_raman_measurement_device.excitation_laser_wavelength 780
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 12
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R070639.rod
_rod_data_source.block           3500000
_rod_database.code               1000085
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9012668 COD http://www.crystallography.net/cod/9012668.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
154.7179 0.0000000E+00
155.2001 91.79688
155.6822 122.2803
156.1643 67.97949
156.6464 43.85352
157.1285 96.41211
157.6106 158.6387
158.0928 209.9756
158.5749 198.8359
159.0570 156.7812
159.5391 106.5469
160.0212 41.22266
160.5033 0.9707030
160.9855 10.73633
161.4676 4.909180
161.9497 25.98828
162.4318 73.73145
162.9139 114.9668
163.3960 129.8184
163.8782 116.7471
164.3603 119.9180
164.8424 156.1426
165.3245 192.2549
165.8066 205.4824
166.2887 196.9551
166.7709 189.9951
167.2530 196.7051
167.7351 210.0176
168.2172 219.5254
168.6993 232.6611
169.1814 243.2129
169.6636 246.1465
170.1457 242.9219
170.6278 241.9902
171.1099 240.1025
171.5920 233.3594
172.0741 227.0869
172.5563 230.4619
173.0384 230.3711
173.5205 223.2754
174.0026 212.5918
174.4847 204.1104
174.9668 195.9951
175.4490 187.5625
175.9311 180.7207
176.4132 180.4258
176.8953 184.2236
177.3774 173.0635
177.8595 130.9668
178.3417 85.69238
178.8238 55.84668
179.3059 43.02441
179.7880 38.62500
180.2701 45.50977
180.7522 75.62109
181.2344 104.9248
181.7165 97.47559
182.1986 93.37695
182.6807 110.5020
183.1628 147.0625
183.6449 185.2173
184.1271 205.2598
184.6092 224.4849
185.0913 227.0430
185.5734 199.6567
186.0555 166.6416
186.5376 145.0752
187.0198 141.6523
187.5019 152.0806
187.9840 162.5732
188.4661 184.6445
188.9482 191.9541
189.4303 161.1567
189.9125 120.3071
190.3946 104.2300
190.8767 131.1870
191.3588 191.1772
191.8409 235.0156
192.3230 258.6797
192.8052 272.3315
193.2873 263.9053
193.7694 246.0391
194.2515 242.9771
194.7336 271.2358
195.2157 326.3535
195.6979 364.9951
196.1800 387.6191
196.6621 398.4429
197.1442 387.8618
197.6263 364.3101
198.1084 351.9521
198.5906 370.6343
199.0727 418.0117
199.5548 444.9463
200.0369 445.7681
200.5190 432.7178
201.0011 413.3169
201.4833 387.5088
201.9654 349.2920
202.4475 285.5815
202.9296 202.2290
203.4117 146.0596
203.8938 139.2964
204.3760 147.1719
204.8581 141.3159
205.3402 119.8350
205.8223 89.22168
206.3044 46.20459
206.7865 3.512695
207.2687 37.86230
207.7508 39.68311
208.2329 28.68506
208.7150 32.24902
209.1971 54.45264
209.6792 80.60645
210.1614 102.1558
210.6435 119.0933
211.1256 129.5239
211.6077 129.5181
212.0898 122.9463
212.5719 79.73242
213.0541 39.33398
213.5362 2.770996
214.0183 25.80078
214.5004 49.69531
214.9825 78.01562
215.4646 124.6392
215.9468 181.7734
216.4289 214.2563
216.9110 203.9146
217.3931 192.7412
217.8752 207.2168
218.3573 240.2017
218.8395 271.4268
219.3216 288.4224
219.8037 292.4565
220.2858 293.5435
220.7679 293.0288
221.2500 287.0557
221.7322 269.2964
222.2143 243.7271
222.6964 221.8784
223.1785 214.7749
223.6606 223.1572
224.1427 227.7295
224.6249 222.3950
225.1070 218.5596
225.5891 222.1841
226.0712 231.9043
226.5533 241.8491
227.0354 244.7612
227.5176 238.4038
227.9997 241.0752
228.4818 270.6284
228.9639 294.3135
229.4460 293.6191
229.9281 272.1675
230.4103 248.2695
230.8924 240.6265
231.3745 251.8403
231.8566 267.9043
232.3387 301.2588
232.8208 328.8242
233.3030 336.9707
233.7851 327.0566
234.2672 310.7622
234.7493 299.1016
235.2314 289.2832
235.7135 295.1587
236.1957 330.5962
236.6778 367.3647
237.1599 391.1006
237.6420 400.7729
238.1241 403.6646
238.6062 408.0703
239.0884 415.1030
239.5705 417.9189
240.0526 403.9219
240.5347 395.8213
241.0168 413.9634
241.4989 456.8848
241.9811 502.4102
242.4632 524.1987
242.9453 511.2417
243.4274 506.1343
243.9095 507.7266
244.3916 516.4180
244.8738 537.2681
245.3559 568.9399
245.8380 600.7427
246.3201 620.1006
246.8022 622.0566
247.2843 624.4287
247.7665 622.9507
248.2486 624.5278
248.7307 636.2744
249.2128 658.5908
249.6949 685.1040
250.1770 709.7095
250.6592 733.4771
251.1413 748.3364
251.6234 742.4058
252.1055 736.0762
252.5876 749.3569
253.0697 783.2480
253.5519 817.9043
254.0340 830.0859
254.5161 811.5098
254.9982 801.2773
255.4803 807.3604
255.9624 816.3525
256.4445 815.7983
256.9267 804.8345
257.4088 794.6533
257.8909 797.7520
258.3730 818.1338
258.8551 832.5020
259.3372 844.5449
259.8194 848.1240
260.3015 835.5347
260.7836 806.3018
261.2657 769.7686
261.7478 733.2148
262.2299 696.4897
262.7121 668.3960
263.1942 650.7817
263.6763 640.3823
264.1584 636.8208
264.6405 638.3667
265.1227 638.5508
265.6048 632.4976
266.0869 620.5596
266.5690 615.7090
267.0511 622.9043
267.5332 631.9380
268.0154 639.6104
268.4975 645.0244
268.9796 637.4854
269.4617 602.3477
269.9438 540.6069
270.4259 502.1958
270.9081 498.3350
271.3902 510.5654
271.8723 529.4546
272.3544 552.8057
272.8365 569.4521
273.3186 569.7729
273.8008 554.0986
274.2829 539.4570
274.7650 523.6577
275.2471 510.1670
275.7292 501.1685
276.2113 497.0229
276.6935 498.3931
277.1756 507.2402
277.6577 522.7036
278.1398 536.0112
278.6219 547.9912
279.1040 557.2207
279.5862 564.7881
280.0683 569.9536
280.5504 565.3569
281.0325 540.0059
281.5146 502.8853
281.9967 488.2358
282.4789 506.2793
282.9610 536.5122
283.4431 570.8286
283.9252 608.4009
284.4073 643.6494
284.8894 674.7422
285.3716 700.2397
285.8537 718.0278
286.3358 719.7168
286.8179 724.6914
287.3000 744.9614
287.7821 777.9487
288.2643 814.1123
288.7464 851.7573
289.2285 887.9604
289.7106 915.8525
290.1927 932.5083
290.6748 947.2905
291.1570 960.9419
291.6391 975.4482
292.1212 995.7153
292.6033 1021.358
293.0854 1057.550
293.5675 1121.910
294.0497 1237.506
294.5318 1320.457
295.0139 1299.789
295.4960 1222.263
295.9781 1203.515
296.4602 1294.833
296.9424 1430.285
297.4245 1490.187
297.9066 1465.971
298.3887 1438.144
298.8708 1429.227
299.3529 1433.737
299.8351 1440.692
300.3172 1446.039
300.7993 1457.816
301.2814 1497.770
301.7635 1571.542
302.2456 1617.916
302.7278 1604.389
303.2099 1561.880
303.6920 1530.262
304.1741 1517.264
304.6562 1514.163
305.1383 1515.168
305.6205 1521.061
306.1026 1516.620
306.5847 1491.940
307.0668 1460.349
307.5489 1436.959
308.0310 1424.034
308.5132 1409.911
308.9953 1382.166
309.4774 1340.582
309.9595 1306.854
310.4416 1291.159
310.9237 1277.222
311.4059 1251.021
311.8880 1212.699
312.3701 1171.450
312.8522 1131.170
313.3343 1093.791
313.8164 1071.062
314.2986 1083.190
314.7807 1091.383
315.2628 1070.674
315.7449 1025.134
316.2270 972.4814
316.7091 921.6250
317.1913 873.3452
317.6734 831.5264
318.1555 800.2964
318.6376 770.1597
319.1197 732.9937
319.6018 694.5513
320.0840 670.8174
320.5661 670.4165
321.0482 682.0972
321.5303 675.2046
322.0124 641.7012
322.4945 607.6006
322.9767 575.3359
323.4588 546.6162
323.9409 524.8203
324.4230 510.9185
324.9051 500.6157
325.3872 491.8540
325.8694 491.7344
326.3515 480.8843
326.8336 446.8398
327.3157 408.0200
327.7978 382.7153
328.2799 377.3311
328.7621 380.8125
329.2442 377.7744
329.7263 365.5586
330.2084 352.4448
330.6905 336.7080
331.1726 321.3677
331.6548 308.2217
332.1369 297.6230
332.6190 289.1885
333.1011 282.6143
333.5832 278.0713
334.0653 274.6914
334.5475 279.4722
335.0296 278.9453
335.5117 262.3657
335.9938 233.8433
336.4759 206.9351
336.9580 193.0479
337.4402 191.8408
337.9223 180.4004
338.4044 139.3193
338.8865 109.3867
339.3686 111.5430
339.8507 130.8257
340.3329 140.1768
340.8150 123.3047
341.2971 87.47314
341.7792 63.86328
342.2613 62.81592
342.7434 62.05957
343.2256 60.92920
343.7077 58.15674
344.1898 49.71533
344.6719 34.26172
345.1540 19.63574
345.6361 24.21240
346.1183 66.93994
346.6004 91.70654
347.0825 80.34863
347.5646 62.49023
348.0467 60.63086
348.5288 78.68799
349.0110 103.1313
349.4931 116.5649
349.9752 115.8730
350.4573 116.6758
350.9394 129.1338
351.4215 134.7769
351.9037 115.3159
352.3858 77.66406
352.8679 49.19629
353.3500 59.90625
353.8321 108.0977
354.3142 135.9629
354.7964 127.6948
355.2785 116.8818
355.7606 123.8921
356.2427 138.0850
356.7248 136.5786
357.2069 99.79688
357.6891 42.71436
358.1712 9.556152
358.6533 9.051270
359.1354 12.95654
359.6175 6.551758
360.0996 0.8037110
360.5818 4.277832
361.0639 30.24268
361.5460 59.46387
362.0281 65.35059
362.5102 44.99414
362.9923 27.83545
363.4745 28.57080
363.9566 33.20801
364.4387 25.41211
364.9208 1.421875
365.4029 18.47803
365.8850 14.93066
366.3672 7.618652
366.8493 24.99121
367.3314 31.80957
367.8135 32.09375
368.2956 28.55518
368.7777 21.56836
369.2599 16.11230
369.7420 19.93848
370.2241 25.07861
370.7062 13.50537
371.1883 20.13330
371.6704 50.80225
372.1526 53.98145
372.6347 34.26562
373.1168 18.62646
373.5989 12.20117
374.0810 9.670898
374.5631 6.232422
375.0453 2.223145
375.5274 0.8935550
376.0095 3.147461
376.4916 10.29541
376.9737 26.56201
377.4558 72.80322
377.9380 103.7368
378.4201 89.13623
378.9022 49.14893
379.3843 24.15625
379.8664 31.16748
380.3485 55.27051
380.8307 66.30664
381.3128 64.53320
381.7949 48.54150
382.2770 7.147949
382.7591 63.25635
383.2412 73.19092
383.7234 32.01416
384.2055 19.73438
384.6876 33.63818
385.1697 1.705078
385.6518 27.13721
386.1339 37.78027
386.6161 44.95703
387.0982 52.48828
387.5803 61.24463
388.0624 71.55420
388.5445 83.81543
389.0266 97.86914
389.5088 111.7358
389.9909 123.9468
390.4730 137.7412
390.9551 155.8862
391.4372 175.1216
391.9193 190.1133
392.4015 198.3398
392.8836 204.9663
393.3657 222.0972
393.8478 256.2715
394.3299 284.4883
394.8120 294.4761
395.2942 304.1616
395.7763 328.5352
396.2584 368.6987
396.7405 409.7573
397.2226 434.0615
397.7047 441.3838
398.1869 459.0068
398.6690 496.0186
399.1511 535.0894
399.6332 569.8887
400.1153 599.2080
400.5974 619.7524
401.0796 620.3867
401.5617 613.7720
402.0438 633.0205
402.5259 686.0112
403.0080 733.7036
403.4901 748.8188
403.9723 747.0146
404.4544 750.7363
404.9365 765.4536
405.4186 783.1514
405.9007 796.5239
406.3828 806.7739
406.8650 821.3701
407.3471 845.9458
407.8292 871.7046
408.3113 881.2266
408.7934 869.8823
409.2755 867.3950
409.7577 894.7363
410.2398 931.5615
410.7219 947.8286
411.2040 938.3203
411.6861 922.0273
412.1682 919.1221
412.6504 932.4526
413.1325 929.8726
413.6146 889.7988
414.0967 854.0996
414.5788 852.8955
415.0609 877.1387
415.5431 896.3979
416.0252 891.7322
416.5073 868.4248
416.9894 850.4636
417.4715 839.1731
417.9536 831.8103
418.4358 830.8213
418.9179 832.6892
419.4000 836.2578
419.8821 840.3105
420.3642 839.2761
420.8463 822.6775
421.3285 781.9338
421.8106 749.8047
422.2927 729.4719
422.7748 714.3340
423.2569 705.4304
423.7390 700.1445
424.2212 689.6455
424.7033 662.8828
425.1854 624.1450
425.6675 601.1052
426.1496 603.4575
426.6317 605.5728
427.1139 593.1621
427.5960 576.4258
428.0781 569.4236
428.5602 579.0920
429.0423 592.9880
429.5244 596.5508
430.0066 591.0598
430.4887 583.2729
430.9708 570.6108
431.4529 560.0557
431.9350 561.1736
432.4171 574.7722
432.8993 585.7432
433.3814 583.7383
433.8635 575.1992
434.3456 572.2227
434.8277 574.7861
435.3098 580.4473
435.7920 592.5039
436.2741 611.8101
436.7562 624.4397
437.2383 616.6316
437.7204 613.7075
438.2025 635.8865
438.6847 676.4268
439.1668 713.8691
439.6489 738.5215
440.1310 755.8950
440.6131 777.3281
441.0952 806.7446
441.5774 835.8608
442.0595 870.2727
442.5416 899.5037
443.0237 912.9326
443.5058 908.4880
443.9879 897.9072
444.4701 895.0193
444.9522 901.9646
445.4343 901.7437
445.9164 892.4846
446.3985 877.6787
446.8806 847.2700
447.3628 813.4473
447.8449 800.5771
448.3270 826.0049
448.8091 869.7832
449.2912 876.9946
449.7733 828.0842
450.2555 796.6235
450.7376 819.5022
451.2197 856.1323
451.7018 877.3879
452.1839 878.7791
452.6660 874.2959
453.1482 869.9927
453.6303 866.2419
454.1124 872.5732
454.5945 896.4834
455.0766 916.8730
455.5587 910.0273
456.0409 884.4810
456.5230 864.4954
457.0051 856.8926
457.4872 856.0806
457.9693 856.9604
458.4514 859.1162
458.9336 864.4443
459.4157 873.2954
459.8978 886.9756
460.3799 912.2178
460.8620 970.5918
461.3441 998.6304
461.8262 970.0872
462.3083 913.9946
462.7905 860.0010
463.2726 813.5718
463.7547 762.9004
464.2368 692.8267
464.7189 598.8687
465.2010 526.1064
465.6832 493.5234
466.1653 461.3083
466.6474 414.8225
467.1295 360.5776
467.6116 308.9729
468.0938 265.5061
468.5759 229.7146
469.0580 200.3625
469.5401 175.6162
470.0222 162.2625
470.5043 181.5618
470.9865 198.1536
471.4686 183.3992
471.9507 137.9956
472.4328 93.37598
472.9149 75.88037
473.3970 78.64575
473.8792 75.21362
474.3613 61.13599
474.8434 49.98267
475.3255 55.96094
475.8076 70.75146
476.2897 76.67334
476.7719 65.14282
477.2540 53.03760
477.7361 51.28735
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