#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-04-26 13:43:47 +0300 (Thu, 26 Apr 2018) $
#$Revision: 536 $
#$URL: svn://172.16.1.111/rod/cif/1/00/00/1000088.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000088
loop_
_publ_author_name
'Cooper, M. A.'
'Hawthorne, F. C.'
_publ_section_title
;
 The crystal structure of kombatite, Pb14(VO4)2O9Cl4, a complex
 heteropolyhedral sheet mineral
;
_journal_name_full               'American Mineralogist'
_journal_page_first              550
_journal_page_last               554
_journal_volume                  79
_journal_year                    1994
_chemical_compound_source        R070720
_chemical_formula_sum            'Cl4 O17 Pb14 V2'
_chemical_name_mineral           Kombatite
_space_group_IT_number           15
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_cell_angle_alpha                90
_cell_angle_beta                 118.11
_cell_angle_gamma                90
_cell_length_a                   12.682
_cell_length_b                   22.566
_cell_length_c                   11.279
_cell_volume                     2847.105
_exptl_crystal_density_diffrn    7.970
_cod_original_formula_sum        'Pb14 V2 Cl4 O17'
_cod_database_code               9001609
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type helium-neon
_raman_measurement_device.excitation_laser_wavelength 780
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 12
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R070720.rod
_rod_data_source.block           3500000
_rod_database.code               1000088
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9001609 COD http://www.crystallography.net/cod/9001609.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
178.8238 1.974609
179.3059 22.96973
179.7880 76.37207
180.2701 108.5566
180.7522 115.1387
181.2344 135.8730
181.7165 183.8604
182.1986 238.5352
182.6807 283.4902
183.1628 308.5615
183.6449 283.6328
184.1271 261.1328
184.6092 257.1992
185.0913 253.1182
185.5734 256.0098
186.0555 254.0439
186.5376 229.1865
187.0198 174.3535
187.5019 108.1816
187.9840 77.18066
188.4661 124.6074
188.9482 156.5664
189.4303 149.4248
189.9125 127.1143
190.3946 123.3027
190.8767 154.8721
191.3588 210.0371
191.8409 232.5977
192.3230 192.3057
192.8052 152.7070
193.2873 121.8242
193.7694 98.83398
194.2515 85.66406
194.7336 84.53564
195.2157 93.86328
195.6979 96.55127
196.1800 95.76562
196.6621 86.89307
197.1442 62.86914
197.6263 28.11377
198.1084 5.146973
198.5906 30.07617
199.0727 45.40771
199.5548 51.25000
200.0369 29.13672
200.5190 13.82764
201.0011 36.37402
201.4833 92.68115
201.9654 139.0117
202.4475 135.5015
202.9296 88.27100
203.4117 69.45020
203.8938 103.4175
204.3760 152.5444
204.8581 183.9521
205.3402 195.4683
205.8223 200.6201
206.3044 204.3628
206.7865 209.3320
207.2687 225.9878
207.7508 264.8350
208.2329 312.9922
208.7150 354.4702
209.1971 388.3447
209.6792 415.5127
210.1614 429.0093
210.6435 435.3647
211.1256 450.4932
211.6077 487.2163
212.0898 320.5093
212.5719 152.1030
213.0541 23.35352
213.5362 193.9160
214.0183 349.1733
214.5004 493.5762
214.9825 638.1318
215.4646 794.1846
215.9468 956.1372
216.4289 1099.179
216.9110 1210.737
217.3931 1318.928
217.8752 1439.823
218.3573 1569.909
218.8395 1699.003
219.3216 1821.449
219.8037 1937.480
220.2858 2048.066
220.7679 2151.721
221.2500 2250.154
221.7322 2345.005
222.2143 2435.939
222.6964 2521.196
223.1785 2597.209
223.6606 2663.501
224.1427 2732.280
224.6249 2815.489
225.1070 2891.924
225.5891 2949.901
226.0712 2992.039
226.5533 3031.489
227.0354 3081.548
227.5176 3144.705
227.9997 3203.031
228.4818 3248.223
228.9639 3296.344
229.4460 3359.732
229.9281 3434.567
230.4103 3504.834
230.8924 3549.778
231.3745 3559.653
231.8566 3592.063
232.3387 3676.149
232.8208 3756.251
233.3030 3805.202
233.7851 3823.174
234.2672 3827.636
234.7493 3836.227
235.2314 3846.946
235.7135 3865.767
236.1957 3903.991
236.6778 3938.836
237.1599 3958.404
237.6420 3963.929
238.1241 3966.006
238.6062 3977.918
239.0884 4007.247
239.5705 4022.730
240.0526 4013.345
240.5347 4000.769
241.0168 3995.387
241.4989 3999.331
241.9811 4010.774
242.4632 4028.833
242.9453 4056.364
243.4274 4082.654
243.9095 4103.756
244.3916 4125.230
244.8738 4153.788
245.3559 4187.667
245.8380 4218.209
246.3201 4236.426
246.8022 4233.076
247.2843 4241.085
247.7665 4273.553
248.2486 4307.115
248.7307 4326.637
249.2128 4330.347
249.6949 4324.078
250.1770 4315.158
250.6592 4305.994
251.1413 4280.706
251.6234 4236.010
252.1055 4179.297
252.5876 4114.265
253.0697 4042.683
253.5519 3966.491
254.0340 3888.616
254.5161 3809.437
254.9982 3722.613
255.4803 3616.112
255.9624 3508.621
256.4445 3416.131
256.9267 3341.106
257.4088 3274.646
257.8909 3209.698
258.3730 3145.629
258.8551 3079.230
259.3372 3006.309
259.8194 2931.048
260.3015 2857.361
260.7836 2788.231
261.2657 2726.895
261.7478 2676.355
262.2299 2637.930
262.7121 2600.915
263.1942 2564.021
263.6763 2531.416
264.1584 2504.199
264.6405 2482.767
265.1227 2471.152
265.6048 2472.416
266.0869 2488.007
266.5690 2511.691
267.0511 2547.523
267.5332 2590.078
268.0154 2635.120
268.4975 2682.790
268.9796 2735.263
269.4617 2793.111
269.9438 2867.550
270.4259 2953.060
270.9081 3056.292
271.3902 3158.068
271.8723 3239.230
272.3544 3301.016
272.8365 3368.226
273.3186 3463.412
273.8008 3584.486
274.2829 3694.033
274.7650 3798.681
275.2471 3886.307
275.7292 3949.466
276.2113 3987.642
276.6935 4001.190
277.1756 3985.999
277.6577 3942.669
278.1398 3894.503
278.6219 3858.821
279.1040 3804.424
279.5862 3704.440
280.0683 3562.223
280.5504 3404.669
281.0325 3242.371
281.5146 3078.814
281.9967 2926.125
282.4789 2790.513
282.9610 2659.226
283.4431 2521.355
283.9252 2379.087
284.4073 2247.913
284.8894 2139.153
285.3716 2045.966
285.8537 1942.698
286.3358 1809.474
286.8179 1691.356
287.3000 1616.458
287.7821 1579.027
288.2643 1557.546
288.7464 1543.978
289.2285 1539.359
289.7106 1545.137
290.1927 1564.717
290.6748 1587.860
291.1570 1603.459
291.6391 1617.498
292.1212 1649.648
292.6033 1710.599
293.0854 1790.376
293.5675 1865.963
294.0497 1930.285
294.5318 2010.283
295.0139 2124.267
295.4960 2261.872
295.9781 2400.050
296.4602 2531.434
296.9424 2660.438
297.4245 2793.354
297.9066 2931.934
298.3887 3067.239
298.8708 3186.567
299.3529 3302.593
299.8351 3440.286
300.3172 3609.372
300.7993 3790.637
301.2814 3958.814
301.7635 4112.251
302.2456 4266.669
302.7278 4418.904
303.2099 4575.436
303.6920 4747.237
304.1741 4937.720
304.6562 5130.907
305.1383 5309.579
305.6205 5472.149
306.1026 5638.877
306.5847 5818.777
307.0668 6000.658
307.5489 6167.460
308.0310 6317.916
308.5132 6474.968
308.9953 6665.669
309.4774 6891.606
309.9595 7096.469
310.4416 7262.925
310.9237 7418.382
311.4059 7583.978
311.8880 7759.819
312.3701 7936.276
312.8522 8106.391
313.3343 8269.764
313.8164 8439.757
314.2986 8630.256
314.7807 8813.742
315.2628 8972.168
315.7449 9108.068
316.2270 9239.115
316.7091 9378.670
317.1913 9520.219
317.6734 9628.551
318.1555 9679.903
318.6376 9729.560
319.1197 9827.829
319.6018 9941.582
320.0840 9991.541
320.5661 9935.634
321.0482 9796.846
321.5303 9646.417
322.0124 9475.377
322.4945 9306.924
322.9767 9137.976
323.4588 8976.430
323.9409 8837.281
324.4230 8727.011
324.9051 8634.336
325.3872 8534.658
325.8694 8423.589
326.3515 8312.639
326.8336 8197.559
327.3157 8087.325
327.7978 7996.715
328.2799 7927.447
328.7621 7859.854
329.2442 7763.682
329.7263 7616.463
330.2084 7496.687
330.6905 7433.061
331.1726 7374.941
331.6548 7277.860
332.1369 7140.880
332.6190 6999.392
333.1011 6892.701
333.5832 6829.394
334.0653 6767.218
334.5475 6715.499
335.0296 6653.736
335.5117 6563.025
335.9938 6452.110
336.4759 6345.394
336.9580 6260.972
337.4402 6198.029
337.9223 6140.288
338.4044 6122.571
338.8865 6073.467
339.3686 5953.773
339.8507 5793.595
340.3329 5646.279
340.8150 5542.837
341.2971 5470.315
341.7792 5371.713
342.2613 5228.952
342.7434 5080.319
343.2256 4929.881
343.7077 4776.562
344.1898 4617.683
344.6719 4452.317
345.1540 4284.273
345.6361 4120.834
346.1183 3969.755
346.6004 3808.367
347.0825 3630.572
347.5646 3448.228
348.0467 3264.683
348.5288 3083.684
349.0110 2910.648
349.4931 2754.187
349.9752 2615.129
350.4573 2487.256
350.9394 2381.741
351.4215 2276.443
351.9037 2161.334
352.3858 2036.521
352.8679 1906.994
353.3500 1769.268
353.8321 1624.811
354.3142 1517.475
354.7964 1471.039
355.2785 1436.568
355.7606 1397.577
356.2427 1354.890
356.7248 1310.487
357.2069 1262.812
357.6891 1216.170
358.1712 1183.439
358.6533 1166.276
359.1354 1159.450
359.6175 1154.453
360.0996 1159.968
360.5818 1190.633
361.0639 1256.850
361.5460 1335.272
362.0281 1384.518
362.5102 1397.745
362.9923 1446.027
363.4745 1578.613
363.9566 1740.925
364.4387 1879.950
364.9208 1989.089
365.4029 2086.667
365.8850 2188.180
366.3672 2290.820
366.8493 2382.012
367.3314 2461.361
367.8135 2523.551
368.2956 2567.397
368.7777 2593.812
369.2599 2595.381
369.7420 2559.212
370.2241 2499.070
370.7062 2438.928
371.1883 2382.375
371.6704 2319.183
372.1526 2235.983
372.6347 2135.920
373.1168 2038.511
373.5989 1954.081
374.0810 1866.853
374.5631 1759.010
375.0453 1632.479
375.5274 1508.873
376.0095 1402.552
376.4916 1307.690
376.9737 1197.972
377.4558 1052.266
377.9380 916.7764
378.4201 818.1099
378.9022 740.0811
379.3843 652.7388
379.8664 544.1782
380.3485 421.2822
380.8307 298.9312
381.3128 163.4966
381.7949 53.73828
382.2770 18.14258
382.7591 68.87354
383.2412 106.4097
383.7234 135.1328
384.2055 167.1074
384.6876 218.0273
385.1697 296.6401
385.6518 356.7671
386.1339 396.7329
386.6161 423.6562
387.0982 437.6855
387.5803 441.5083
388.0624 440.3872
388.5445 438.8750
389.0266 435.9883
389.5088 420.4736
389.9909 369.7109
390.4730 332.1685
390.9551 330.2104
391.4372 341.2705
391.9193 336.1670
392.4015 302.0112
392.8836 250.6133
393.3657 206.2969
393.8478 174.7910
394.3299 136.5220
394.8120 86.28613
395.2942 30.69824
395.7763 27.31494
396.2584 86.90332
396.7405 146.3931
397.2226 202.5166
397.7047 255.0684
398.1869 314.6138
398.6690 383.1533
399.1511 458.0508
399.6332 540.0859
400.1153 626.7319
400.5974 711.2124
401.0796 784.9673
401.5617 855.6182
402.0438 940.1387
402.5259 1039.491
403.0080 1149.041
403.4901 1268.453
403.9723 1396.556
404.4544 1532.739
404.9365 1682.736
405.4186 1831.511
405.9007 1957.424
406.3828 2066.814
406.8650 2196.393
407.3471 2363.544
407.8292 2551.288
408.3113 2731.625
408.7934 2900.030
409.2755 3079.125
409.7577 3292.215
410.2398 3513.198
410.7219 3706.045
411.2040 3864.217
411.6861 3998.107
412.1682 4112.108
412.6504 4201.942
413.1325 4307.872
413.6146 4447.686
414.0967 4587.636
414.5788 4722.253
415.0609 4843.239
415.5431 4930.299
416.0252 4968.360
416.5073 4966.244
416.9894 4966.887
417.4715 4990.324
417.9536 4991.901
418.4358 4950.931
418.9179 4893.883
419.4000 4851.580
419.8821 4832.378
420.3642 4816.974
420.8463 4774.676
421.3285 4694.821
421.8106 4620.114
422.2927 4552.592
422.7748 4488.161
423.2569 4432.001
423.7390 4378.797
424.2212 4311.049
424.7033 4206.455
425.1854 4075.013
425.6675 3980.492
426.1496 3947.828
426.6317 3911.941
427.1139 3851.026
427.5960 3772.292
428.0781 3680.869
428.5602 3575.858
429.0423 3469.424
429.5244 3376.593
430.0066 3297.533
430.4887 3225.240
430.9708 3160.706
431.4529 3099.672
431.9350 3038.214
432.4171 2976.174
432.8993 2912.503
433.3814 2846.648
433.8635 2779.566
434.3456 2710.509
434.8277 2638.865
435.3098 2569.978
435.7920 2508.694
436.2741 2454.807
436.7562 2402.085
437.2383 2344.554
437.7204 2292.847
438.2025 2258.329
438.6847 2235.558
439.1668 2207.146
439.6489 2163.642
440.1310 2110.482
440.6131 2064.264
441.0952 2037.169
441.5774 1999.660
442.0595 1940.482
442.5416 1874.844
443.0237 1819.810
443.5058 1777.326
443.9879 1731.962
444.4701 1663.640
444.9522 1568.175
445.4343 1483.660
445.9164 1426.542
446.3985 1364.720
446.8806 1283.735
447.3628 1192.567
447.8449 1109.010
448.3270 1040.506
448.8091 981.6714
449.2912 923.2554
449.7733 867.8687
450.2555 810.2859
450.7376 744.6306
451.2197 679.5437
451.7018 619.6548
452.1839 566.6550
452.6660 521.2515
453.1482 483.7351
453.6303 454.3999
454.1124 434.8479
454.5945 426.2585
455.0766 419.9719
455.5587 409.2104
456.0409 395.4805
456.5230 383.8247
457.0051 376.4580
457.4872 370.6819
457.9693 366.8469
458.4514 363.4316
458.9336 351.9521
459.4157 326.2996
459.8978 292.6521
460.3799 268.0969
460.8620 255.8879
461.3441 244.9197
461.8262 233.8296
462.3083 222.7312
462.7905 213.8154
463.2726 206.5728
463.7547 194.9189
464.2368 170.4902
464.7189 130.3279
465.2010 105.3801
465.6832 111.1111
466.1653 114.2388
466.6474 104.2478
467.1295 84.90503
467.6116 61.46582
468.0938 36.24756
468.5759 12.40356
469.0580 1.814697
469.5401 3.871094
470.0222 3.717285
470.5043 2.374512
470.9865 6.282227
471.4686 1.044189
471.9507 12.99146
472.4328 27.92383
472.9149 39.93567
473.3970 48.23572
473.8792 48.68823
474.3613 38.89771
474.8434 27.95764
475.3255 21.87756
475.8076 18.71411
476.2897 15.04895
476.7719 11.51440
477.2540 6.244507
477.7361 4.920532
478.2182 19.26025
478.7003 26.78625
479.1824 22.64514
479.6646 15.62451
480.1467 20.62463
480.6288 43.46826
481.1109 59.68359
481.5930 61.18677
482.0751 61.16614
482.5573 70.73987
483.0394 88.34033
483.5215 103.9808
484.0036 109.8969
484.4857 108.0594
484.9678 111.9044
485.4500 128.4597
485.9321 141.5591
486.4142 146.9651
486.8963 149.2017
487.3784 152.3243
487.8605 157.5034
488.3427 163.8306
488.8248 169.8123
489.3069 175.3348
489.7890 185.2062
490.2711 211.1919
490.7532 225.2219
491.2354 203.1171
491.7175 158.9730
492.1996 125.6726
492.6817 121.2751
493.1638 127.8455
493.6459 122.3127
494.1281 105.9241
494.6102 97.58142
495.0923 108.1006
495.5744 125.7737
496.0565 129.4414
496.5386 117.2034
497.0208 103.7939
497.5029 89.27515
497.9850 77.19495
498.4671 72.93311
498.9492 75.94055
499.4313 79.50293
499.9135 78.58838
500.3956 73.40125
500.8777 65.79846
501.3598 46.97571
501.8419 36.51306
502.3240 42.41345
502.8062 56.20984
503.2883 70.57556
503.7704 82.66638
504.2525 89.90283
504.7346 86.25916
505.2167 69.28394
505.6989 59.67468
506.1810 60.93555
506.6631 66.72107
507.1452 74.72217
507.6273 84.61194
508.1094 95.96741
508.5916 109.1252
509.0737 123.0742
509.5558 138.7538
510.0379 155.7999
510.5200 163.5549
511.0021 153.3810
511.4843 138.0115
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1273.711 16.94366
1274.193 18.27933
1274.675 23.64197
1275.157 32.21547
1275.639 34.17975
1276.121 22.83508
1276.603 12.83995
1277.085 11.73192
1277.568 13.81271
1278.050 13.82352
1278.532 13.17043
1279.014 13.38647
1279.496 13.69041
1279.978 11.41832
1280.460 7.081360
1280.942 9.123047
1281.425 20.51918
1281.907 26.85178
1282.389 26.86528
1282.871 23.07317
1283.353 16.04967
1283.835 8.525360
1284.317 2.275894
1284.799 0.8279270
1285.281 4.753113
1285.764 14.58603
1286.246 16.99025
1286.728 13.87393
1287.210 7.181122
1287.692 4.488800
1288.174 1.202271
1288.656 0.0000000E+00
