#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-04-26 13:44:36 +0300 (Thu, 26 Apr 2018) $
#$Revision: 549 $
#$URL: svn://172.16.1.111/rod/cif/1/00/00/1000097.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000097
loop_
_publ_author_name
'Rozhdestvenskaya, I. V.'
'Bannova, I. I.'
'Nikishova, L. V.'
'Soboleva, T. V.'
_publ_section_title
;
 The crystal structure of fenaksite K2Na2Fe2Si8O20 Locality: synthetic
;
_journal_name_full               'Doklady Earth Sciences'
_journal_page_first              1029
_journal_page_last               1033
_journal_volume                  398
_journal_year                    2004
_chemical_compound_source        R080135
_chemical_formula_sum            'Fe K Na O10 Si4'
_chemical_name_mineral           Fenaksite
_space_group_IT_number           2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                100.21
_cell_angle_beta                 114.13
_cell_angle_gamma                105.87
_cell_length_a                   8.142
_cell_length_b                   9.954
_cell_length_c                   6.983
_cell_volume                     469.098
_exptl_crystal_density_diffrn    2.763
_cod_original_formula_sum        'K Na Fe Si4 O10'
_cod_database_code               9012902
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type helium-neon
_raman_measurement_device.excitation_laser_wavelength 780
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 12
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R080135.rod
_rod_data_source.block           3500000
_rod_database.code               1000097
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9012902 COD http://www.crystallography.net/cod/9012902.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
114.9964 0.0000000E+00
115.4785 8.1329998E-03
115.9606 5.1727001E-02
116.4427 0.1500850
116.9248 1.159943
117.4069 3.554031
117.8891 6.735199
118.3712 9.591629
118.8533 11.88860
119.3354 13.87718
119.8175 15.53250
120.2996 16.87999
120.7818 18.67918
121.2639 21.95599
121.7460 26.95245
122.2281 31.26537
122.7102 33.73602
123.1923 35.67676
123.6745 37.57625
124.1566 39.57224
124.6387 41.63834
125.1208 43.87216
125.6029 46.73897
126.0850 48.78033
126.5672 50.08063
127.0493 50.81461
127.5314 51.46268
128.0135 52.66602
128.4956 53.35321
128.9777 52.37477
129.4599 48.59584
129.9420 45.86211
130.4241 44.35292
130.9062 43.36986
131.3883 42.09261
131.8704 40.47238
132.3526 38.77298
132.8347 36.75934
133.3168 34.28531
133.7989 31.70834
134.2810 29.21199
134.7632 26.80740
135.2453 24.25227
135.7274 21.23700
136.2095 17.95308
136.6916 15.07623
137.1737 12.77742
137.6559 10.80515
138.1380 8.936920
138.6201 7.191605
139.1022 5.447235
139.5843 3.346878
140.0664 1.205612
140.5486 0.4332730
141.0307 1.276779
141.5128 1.476669
141.9949 1.400665
142.4770 0.7617650
142.9591 0.2794650
143.4413 0.3602600
143.9234 0.7915950
144.4055 1.185837
144.8876 1.271011
145.3697 1.046524
145.8518 0.7504430
146.3340 0.3998870
146.8161 4.1533999E-02
147.2982 0.9539950
147.7803 2.072266
148.2624 3.049500
148.7445 3.628281
149.2267 2.695023
149.7088 2.291855
150.1909 2.819534
150.6730 3.683807
151.1551 4.625931
151.6372 5.582870
152.1194 6.563187
152.6015 7.627075
153.0836 8.944733
153.5657 9.740051
154.0478 9.608978
154.5299 9.150375
155.0121 8.754120
155.4942 8.474762
155.9763 8.703796
156.4584 10.45755
156.9405 13.88742
157.4226 16.80481
157.9048 18.69922
158.3869 19.67047
158.8690 19.63698
159.3511 17.91795
159.8332 16.27197
160.3153 16.93645
160.7975 19.92693
161.2796 23.26891
161.7617 26.11580
162.2438 28.44502
162.7259 29.68172
163.2081 28.71002
163.6902 27.34477
164.1723 27.04581
164.6544 27.94427
165.1365 29.06708
165.6186 29.38788
166.1008 28.77905
166.5829 27.92177
167.0650 26.63704
167.5471 25.33456
168.0292 24.21330
168.5113 23.33830
168.9935 22.74899
169.4756 22.65309
169.9577 23.81731
170.4398 23.92587
170.9219 22.38223
171.4040 20.14334
171.8862 17.93680
172.3683 16.04355
172.8504 14.48676
173.3325 12.77356
173.8146 10.37140
174.2967 8.505844
174.7789 7.715942
175.2610 7.307053
175.7431 6.339996
176.2252 4.344330
176.7073 1.807343
177.1894 0.3903350
177.6716 1.204697
178.1537 1.635574
178.6358 0.8065800
179.1179 0.7297360
179.6000 1.862183
180.0821 1.944061
180.5643 1.392059
181.0464 1.561279
181.5285 3.110489
182.0106 4.310776
182.4927 4.100220
182.9748 2.742508
183.4570 1.415802
183.9391 0.6535190
184.4212 0.3151090
184.9033 5.3249998E-03
185.3854 0.2772060
185.8675 0.5280300
186.3497 0.7391970
186.8318 0.9128270
187.3139 1.068314
187.7960 0.9764400
188.2781 0.9980320
188.7602 1.610443
189.2424 3.060715
189.7245 4.787521
190.2066 6.063385
190.6887 6.793457
191.1708 7.415131
191.6530 8.039337
192.1351 8.651260
192.6172 9.335617
193.0993 10.18161
193.5814 10.86626
194.0635 10.50174
194.5457 8.005508
195.0278 6.685364
195.5099 8.116959
195.9920 10.46201
196.4741 11.90263
196.9562 11.60419
197.4384 10.11092
197.9205 8.964783
198.4026 8.153488
198.8847 7.764648
199.3668 7.998291
199.8489 8.619492
200.3311 9.452255
200.8132 10.38820
201.2953 11.32939
201.7774 11.99335
202.2595 12.24239
202.7416 12.36736
203.2238 12.30420
203.7059 12.17992
204.1880 12.17728
204.6701 12.40331
205.1522 12.80873
205.6343 13.12352
206.1165 13.08049
206.5986 13.22717
207.0807 13.71794
207.5628 14.47414
208.0449 15.45880
208.5270 16.74724
209.0092 18.09343
209.4913 18.42857
209.9734 16.83047
210.4555 15.54611
210.9376 15.57732
211.4197 16.57011
211.9019 17.49292
212.3840 17.66776
212.8661 17.60532
213.3482 18.73080
213.8303 21.81841
214.3124 24.75563
214.7946 26.00133
215.2767 25.88980
215.7588 26.23869
216.2409 28.04707
216.7230 30.68661
217.2052 32.82208
217.6873 34.09933
218.1694 35.58084
218.6515 38.22925
219.1336 42.01212
219.6157 45.76865
220.0979 48.85927
220.5800 51.88257
221.0621 55.60165
221.5442 60.25200
222.0263 64.97029
222.5084 68.67586
222.9906 71.24113
223.4727 74.37135
223.9548 78.99312
224.4369 84.16681
224.9190 89.35117
225.4011 94.49377
225.8833 99.38512
226.3654 103.6686
226.8475 107.1241
227.3296 110.9562
227.8117 116.3170
228.2938 121.5476
228.7760 125.6527
229.2581 128.4259
229.7402 130.0855
230.2223 130.7664
230.7044 130.1735
231.1865 129.5203
231.6687 129.8651
232.1508 129.5645
232.6329 127.3453
233.1150 123.0616
233.5971 117.7673
234.0792 112.9526
234.5614 109.0661
235.0435 104.5087
235.5256 99.06870
236.0077 93.20435
236.4898 86.84700
236.9719 80.16864
237.4541 73.77254
237.9362 68.67148
238.4183 65.73264
238.9004 62.12437
239.3825 57.03789
239.8646 51.90553
240.3468 47.85182
240.8289 45.01091
241.3110 42.64868
241.7931 39.72273
242.2752 35.62056
242.7573 32.85645
243.2395 32.35399
243.7216 32.28030
244.2037 31.38608
244.6858 29.57921
245.1679 27.64980
245.6501 26.43820
246.1322 26.04294
246.6143 26.24110
247.0964 27.63663
247.5785 29.10674
248.0606 29.80087
248.5428 29.71396
249.0249 29.52350
249.5070 29.87111
249.9891 30.87303
250.4712 31.83672
250.9533 32.67824
251.4355 33.60947
251.9176 34.63350
252.3997 35.75920
252.8818 37.10828
253.3639 38.74902
253.8460 40.74168
254.3282 42.97076
254.8103 45.66786
255.2924 48.40344
255.7745 50.88673
256.2566 53.10780
256.7387 55.08991
257.2209 56.64120
257.7030 57.95734
258.1851 60.09225
258.6672 63.95485
259.1493 67.88838
259.6314 70.60181
260.1136 72.20725
260.5957 73.83755
261.0778 76.22167
261.5599 79.11403
262.0420 81.65430
262.5241 83.27100
263.0063 85.20180
263.4884 88.73929
263.9705 93.66812
264.4526 98.06409
264.9347 100.7351
265.4168 102.4672
265.8990 104.8632
266.3811 108.2430
266.8632 111.6858
267.3453 114.5194
267.8274 116.8043
268.3095 119.1150
268.7917 121.9582
269.2738 124.5887
269.7559 125.9843
270.2380 125.9332
270.7201 125.7296
271.2022 126.3739
271.6844 127.7205
272.1665 128.8979
272.6486 130.2673
273.1307 130.6207
273.6128 128.7037
274.0949 124.5258
274.5771 120.0820
275.0592 117.0941
275.5413 115.1367
276.0234 111.5343
276.5055 104.4854
276.9876 97.56716
277.4698 93.76471
277.9519 92.58729
278.4340 91.50189
278.9161 88.85821
279.3982 85.00763
279.8803 81.35564
280.3625 77.61436
280.8446 74.76844
281.3267 73.45958
281.8088 73.40824
282.2909 73.97224
282.7730 75.25474
283.2552 76.83257
283.7373 77.08171
284.2194 74.89314
284.7015 73.56890
285.1836 75.31741
285.6658 78.65466
286.1479 81.43226
286.6300 82.71243
287.1121 82.81877
287.5942 82.33771
288.0764 81.06028
288.5585 79.65112
289.0406 78.38703
289.5227 77.14292
290.0048 75.89949
290.4869 74.69846
290.9691 73.16646
291.4512 70.58332
291.9333 66.69725
292.4154 62.67848
292.8975 58.88902
293.3796 55.00491
293.8618 50.74073
294.3439 46.07521
294.8260 41.32994
295.3081 36.82295
295.7902 32.51948
296.2723 28.65944
296.7545 25.34790
297.2366 22.47273
297.7187 20.26178
298.2008 18.62568
298.6829 16.93870
299.1650 14.36926
299.6472 10.74228
300.1293 7.821884
300.6114 6.235840
301.0935 4.970230
301.5756 3.553902
302.0577 2.060799
302.5399 0.8250270
303.0220 0.1760640
303.5041 9.0813003E-02
303.9862 3.6858000E-02
304.4683 0.1038740
304.9504 9.2789002E-02
305.4326 0.2314380
305.9147 0.6679380
306.3968 0.7941210
306.8789 0.2152250
307.3610 0.7902680
307.8431 0.9052200
308.3253 0.7857740
308.8074 1.914330
309.2895 1.408363
309.7716 0.2024920
310.2537 0.5130460
310.7358 0.1643980
311.2180 0.6756520
311.7001 0.6268920
312.1822 0.9424900
312.6643 1.987450
313.1464 1.393005
313.6285 0.6025310
314.1107 0.8782270
314.5928 2.542976
315.0749 4.805283
315.5570 6.599113
316.0391 7.874275
316.5212 8.845764
317.0034 8.955856
317.4855 9.216347
317.9676 10.25302
318.4497 12.07248
318.9318 14.20541
319.4139 16.20539
319.8961 18.04662
320.3782 19.98041
320.8603 21.94534
321.3424 24.07518
321.8245 26.78755
322.3066 29.74135
322.7888 32.12865
323.2709 33.15866
323.7530 33.07005
324.2351 33.66627
324.7172 35.70984
325.1993 37.37170
325.6815 38.04275
326.1636 38.04643
326.6457 37.82281
327.1278 37.56274
327.6099 37.25670
328.0920 36.91701
328.5742 36.67876
329.0563 36.08306
329.5384 35.29008
330.0205 34.00493
330.5026 31.80559
330.9847 28.56756
331.4669 24.89344
331.9490 21.52982
332.4311 18.46812
332.9132 15.76128
333.3953 13.38964
333.8774 11.41290
334.3596 10.17121
334.8417 9.547012
335.3238 8.837265
335.8059 7.166687
336.2880 4.508156
336.7701 2.588318
337.2523 1.953377
337.7344 1.538971
338.2165 0.9001160
338.6986 8.7852001E-02
339.1807 0.7608720
339.6628 1.667557
340.1450 2.519836
340.6271 2.825500
341.1092 2.235603
341.5913 1.768982
342.0735 2.022446
342.5556 2.535881
343.0377 2.715370
343.5198 2.283295
344.0019 1.607811
344.4840 1.296547
344.9662 1.431145
345.4483 1.563683
345.9304 1.467911
346.4125 1.374870
346.8946 1.542519
347.3767 2.013382
347.8589 2.386253
348.3410 2.158180
348.8231 1.348610
349.3052 0.7918550
349.7873 0.9184880
350.2694 0.9525220
350.7516 0.2312930
351.2337 1.082108
351.7158 2.263741
352.1979 2.874641
352.6800 3.023239
353.1621 2.994675
353.6443 2.651070
354.1264 2.459930
354.6085 2.719727
355.0906 3.296577
355.5727 4.079697
356.0548 5.318825
356.5370 6.406326
357.0191 6.255417
357.5012 4.724892
357.9833 3.557907
358.4654 3.699135
358.9475 4.469803
359.4297 4.984932
359.9118 5.066750
360.3939 5.386482
360.8760 6.542374
361.3581 8.400993
361.8402 10.39260
362.3224 12.60783
362.8045 14.54359
363.2866 15.45435
363.7687 15.45376
364.2508 15.72639
364.7329 17.05682
365.2151 18.86741
365.6972 20.26131
366.1793 21.15143
366.6614 21.54321
367.1435 21.02190
367.6256 20.08463
368.1078 20.19859
368.5899 22.56108
369.0720 25.18669
369.5541 26.42244
370.0362 26.45110
370.5183 26.30178
371.0005 26.33801
371.4826 26.61265
371.9647 27.26541
372.4468 28.47890
372.9289 29.56091
373.4110 30.45705
373.8932 31.00200
374.3753 30.65060
374.8574 29.14291
375.3395 27.45855
375.8216 26.83312
376.3037 27.34642
376.7859 28.26385
377.2680 30.01311
377.7501 31.80789
378.2322 32.77381
378.7143 32.97237
379.1964 33.35666
379.6786 34.67686
380.1607 36.85241
380.6428 38.85258
381.1249 40.72231
381.6070 42.38564
382.0891 43.67794
382.5713 44.76679
383.0534 46.00215
383.5355 47.55697
384.0176 49.21735
384.4997 50.53204
384.9818 51.31709
385.4640 52.02641
385.9461 52.80066
386.4282 53.41934
386.9103 53.69830
387.3924 53.60991
387.8745 53.24895
388.3567 52.77168
388.8388 52.28374
389.3209 50.84924
389.8030 47.68913
390.2851 44.53005
390.7672 42.12684
391.2494 40.22068
391.7315 38.16338
392.2136 35.55953
392.6957 32.59966
393.1778 30.07005
393.6599 28.31701
394.1421 26.53091
394.6242 24.72371
395.1063 22.79379
395.5884 20.49146
396.0706 17.81737
396.5527 15.26808
397.0348 13.63812
397.5169 13.29201
397.9990 12.42834
398.4811 10.56472
398.9633 8.738892
399.4454 7.275826
399.9275 6.121063
400.4096 5.101593
400.8917 4.107628
401.3738 3.244873
401.8560 2.914680
402.3381 3.569237
402.8202 3.787964
403.3023 2.608025
403.7844 1.104637
404.2665 0.4024120
404.7487 0.8385240
405.2308 1.787880
405.7129 2.723808
406.1950 3.722641
406.6771 4.154640
407.1592 3.315453
407.6414 2.392113
408.1235 2.312660
408.6056 3.026688
409.0877 3.912460
409.5698 4.441986
410.0519 4.832001
410.5341 5.667152
411.0162 7.021210
411.4983 8.580101
411.9804 10.47740
412.4625 12.37392
412.9446 13.65224
413.4268 14.10126
413.9089 14.13825
414.3910 13.80450
414.8731 13.20519
415.3552 12.98979
415.8373 13.47016
416.3195 14.34035
416.8016 15.18381
417.2837 15.96957
417.7658 16.45256
418.2479 16.38255
418.7300 16.14696
419.2122 16.25851
419.6943 16.75116
420.1764 17.15173
420.6585 17.02162
421.1406 16.43096
421.6227 16.22371
422.1049 16.71143
422.5870 17.20027
423.0691 17.53459
423.5512 17.66281
424.0333 17.34444
424.5154 16.45337
424.9976 15.51712
425.4797 15.57905
425.9618 17.52557
426.4439 18.70177
426.9260 19.00591
427.4081 18.66204
427.8903 17.34248
428.3724 15.37438
428.8545 13.87279
429.3366 13.80125
429.8187 15.09472
430.3008 16.28034
430.7830 17.51395
431.2651 18.44979
431.7472 18.81612
432.2293 18.93549
432.7114 19.04430
433.1935 19.24909
433.6757 19.82197
434.1578 21.36644
434.6399 24.26675
435.1220 26.75634
435.6041 28.52150
436.0862 29.97630
436.5684 31.22089
437.0505 32.30062
437.5326 33.31578
438.0147 34.44894
438.4968 35.53135
438.9789 35.79350
439.4611 34.75121
439.9432 34.11694
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