#\#CIF_2.0 #------------------------------------------------------------------------------ #$Date: 2018-04-26 13:45:17 +0300 (Thu, 26 Apr 2018) $ #$Revision: 561 $ #$URL: svn://172.16.1.111/rod/cif/1/00/01/1000106.rod $ #------------------------------------------------------------------------------ # # This file is available in the Raman Open Database (ROD), # http://solsa.crystallography.net/rod/ # # All data on this site have been placed in the public domain by the # contributors. # data_1000106 loop_ _publ_author_name 'Kampf, A. R.' 'Foord, E. E.' _publ_section_title ; Artroeite, PbAlF3(OH)2, a new mineral from the Grand Reef mine, Graham County, Arizona: Description and crystal structure ; _journal_name_full 'American Mineralogist' _journal_page_first 179 _journal_page_last 183 _journal_volume 80 _journal_year 1995 _chemical_compound_source R100034 _chemical_formula_sum 'Al F3 H2 O2 Pb' _chemical_name_mineral Artroeite _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 90.68 _cell_angle_beta 107.69 _cell_angle_gamma 104.46 _cell_length_a 6.270 _cell_length_b 6.821 _cell_length_c 5.057 _cell_volume 198.618 _exptl_crystal_density_diffrn 5.438 _cod_original_formula_sum 'Pb Al F3 O2 H2' _cod_database_code 9001665 _raman_determination_method experimental _raman_measurement_device.location 'Arizona University' _raman_measurement_device.company 'Thermo Scientific' _raman_measurement_device.model 'Nicolet Almega XR' _raman_measurement_device.optics_type microscope _raman_measurement_device.microscope_system dispersive _raman_measurement_device.microscope_objective_magnification 50 _raman_measurement_device.microscope_numerical_aperture 0.5 _raman_measurement_device.excitation_laser_type helium-neon _raman_measurement_device.excitation_laser_wavelength 780 _raman_measurement_device.configuration simple _raman_measurement_device.resolution 4 _raman_measurement_device.power_on_sample 12 _raman_measurement_device.direction_polarization unoriented _raman_measurement_device.spot_size 1 _raman_measurement_device.diffraction_grating 400 _raman_measurement.environment Air _raman_measurement.environment_details ; The sample was measured in air. ; _raman_measurement.temperature 300 _raman_measurement.pressure 100 _raman_measurement.background_subtraction no _raman_measurement.background_subtraction_details ; No background subtraction method was applied. ; _raman_measurement.baseline_correction no _raman_measurement.baseline_correction_details ; No baseline correction method was applied. ; _raman_measurement.integration_time 10 _rod_data_source.file R100034.rod _rod_data_source.block 3500000 _rod_database.code 1000106 loop_ _raman_complementary.id _raman_complementary.method 1 XRD loop_ _raman_measurement_device_calibration.id _raman_measurement_device_calibration.standard 1 neon_lamp loop_ _rod_related_entry.id _rod_related_entry.code _rod_related_entry.database _rod_related_entry.uri _rod_related_entry.description 1 9001665 COD http://www.crystallography.net/cod/9001665.html ; XRD analysis data was done. ; loop_ _raman_spectrum.raman_shift _raman_spectrum.intensity 92.97955 0.0000000E+00 93.46167 20.91077 93.94379 39.55853 94.42590 57.58453 94.90802 72.29999 95.39014 78.73093 95.87225 75.85211 96.35437 71.26706 96.83649 63.30908 97.31860 53.88647 97.80072 44.47568 98.28284 35.66801 98.76495 28.89391 99.24707 25.95738 99.72919 24.14607 100.2113 20.40108 100.6934 15.61308 101.1755 11.11920 101.6577 7.572769 102.1398 5.430603 102.6219 5.262405 103.1040 4.187500 103.5861 2.463242 104.0682 0.7520750 104.5504 0.9762270 105.0325 2.642258 105.5146 3.878571 105.9967 4.117126 106.4788 2.997681 106.9609 1.782990 107.4431 0.6495510 107.9252 0.5587460 108.4073 2.033340 108.8894 3.821442 109.3715 5.939468 109.8536 8.242706 110.3358 10.50645 110.8179 13.57233 111.3000 17.99911 111.7821 23.71350 112.2642 30.03082 112.7463 36.69360 113.2285 43.95042 113.7106 52.22183 114.1927 61.79698 114.6748 71.76527 115.1569 80.79825 115.6390 88.72873 116.1212 96.16315 116.6033 103.7003 117.0854 110.8190 117.5675 116.8452 118.0496 121.3491 118.5317 124.6977 119.0139 128.5943 119.4960 132.9761 119.9781 138.0950 120.4602 144.4701 120.9423 151.6155 121.4244 158.6672 121.9066 164.9344 122.3887 170.3534 122.8708 176.4111 123.3529 183.1583 123.8350 190.3282 124.3171 197.7600 124.7993 205.4668 125.2814 213.4915 125.7635 221.8181 126.2456 230.4335 126.7277 240.2490 127.2098 252.2123 127.6920 264.9506 128.1741 276.9487 128.6562 287.7093 129.1383 298.4070 129.6204 310.5829 130.1025 324.0544 130.5847 337.9846 131.0668 352.6067 131.5489 367.6113 132.0310 381.9387 132.5131 396.2674 132.9952 408.8036 133.4774 419.5908 133.9595 428.6721 134.4416 433.6717 134.9237 431.9786 135.4058 423.1109 135.8879 409.1184 136.3701 387.3271 136.8522 362.3480 137.3343 335.6830 137.8164 307.5006 138.2985 278.8226 138.7806 250.6324 139.2628 221.8607 139.7449 196.0456 140.2270 172.9078 140.7091 152.4539 141.1912 134.9037 141.6733 120.3781 142.1555 108.3465 142.6376 97.42014 143.1197 87.70688 143.6018 79.26004 144.0839 72.29280 144.5660 66.59128 145.0482 61.89244 145.5303 58.11136 146.0124 55.16852 146.4945 52.37746 146.9766 49.37865 147.4587 46.83492 147.9409 45.11395 148.4230 44.13402 148.9051 43.54410 149.3872 43.26624 149.8693 43.19601 150.3514 42.76035 150.8336 42.44226 151.3157 42.03949 151.7978 42.43965 152.2799 43.76840 152.7620 45.02951 153.2441 44.94469 153.7263 44.28035 154.2084 44.41344 154.6905 46.44547 155.1726 49.50412 155.6547 51.66237 156.1368 52.65778 156.6190 53.12540 157.1011 53.25072 157.5832 53.19096 158.0653 53.24792 158.5474 53.66359 159.0295 54.41342 159.5117 55.04321 159.9938 55.93237 160.4759 56.32892 160.9580 55.75853 161.4401 54.40923 161.9222 52.79181 162.4044 51.29094 162.8865 49.90594 163.3686 48.59795 163.8507 48.12462 164.3328 47.27814 164.8149 45.17397 165.2971 41.94554 165.7792 38.57043 166.2613 36.17868 166.7434 35.27534 167.2255 33.94238 167.7076 32.27789 168.1898 30.19051 168.6719 27.37608 169.1540 23.83302 169.6361 20.23074 170.1182 17.56989 170.6003 16.46190 171.0825 14.75491 171.5646 11.55640 172.0467 7.987450 172.5288 5.459656 173.0109 4.447197 173.4930 4.084373 173.9752 2.880661 174.4573 2.757307 174.9394 1.190262 175.4215 2.541908 175.9036 3.385201 176.3857 3.706985 176.8679 3.283707 177.3500 2.681694 177.8321 2.664268 178.3142 3.254562 178.7963 3.987457 179.2784 4.744011 179.7606 5.491104 180.2427 5.884499 180.7248 5.789604 181.2069 5.290771 181.6890 4.379456 182.1711 3.034645 182.6533 1.684746 183.1354 0.8119890 183.6175 0.4935530 184.0996 3.4157000E-02 184.5817 0.9014890 185.0638 1.923653 185.5460 2.793640 186.0281 3.463203 186.5102 4.078499 186.9923 4.940559 187.4744 6.350449 187.9565 7.165405 188.4387 6.280731 188.9208 5.403839 189.4029 5.728966 189.8850 7.627861 190.3671 10.68363 190.8492 14.26168 191.3314 19.05676 191.8135 23.16739 192.2956 25.39615 192.7777 27.48358 193.2598 31.00948 193.7419 36.57581 194.2241 43.60757 194.7062 50.71144 195.1883 58.17305 195.6704 65.41116 196.1525 72.13285 196.6346 78.69486 197.1168 85.70059 197.5989 93.44895 198.0810 101.4118 198.5631 107.9796 199.0452 111.9909 199.5273 116.2582 200.0095 121.6204 200.4916 127.4604 200.9737 132.6790 201.4558 136.6887 201.9379 140.0359 202.4200 144.4965 202.9022 150.7674 203.3843 156.6634 203.8664 161.2959 204.3485 164.9514 204.8306 168.3206 205.3127 171.5625 205.7949 174.8440 206.2770 178.4396 206.7591 182.3514 207.2412 186.5430 207.7233 190.8196 208.2054 195.2811 208.6876 200.3970 209.1697 206.1912 209.6518 213.0187 210.1339 220.9894 210.6160 230.0506 211.0981 240.3310 211.5803 252.1143 212.0624 265.3757 212.5445 279.4533 213.0266 295.1403 213.5087 310.7654 213.9908 325.5848 214.4730 339.8287 214.9551 350.9386 215.4372 356.2372 215.9193 355.6912 216.4014 349.6463 216.8836 336.4093 217.3657 318.3388 217.8478 295.0897 218.3299 266.5829 218.8120 236.3712 219.2941 208.9879 219.7763 184.3343 220.2584 163.1250 220.7405 146.6123 221.2226 132.5085 221.7047 119.4184 222.1868 106.9533 222.6690 95.53971 223.1511 85.92567 223.6332 78.43543 224.1153 72.08543 224.5974 66.98766 225.0795 62.64721 225.5617 58.78267 226.0438 55.29398 226.5259 52.18603 227.0080 49.47244 227.4901 47.19793 227.9722 45.34396 228.4544 44.20366 228.9365 43.24385 229.4186 42.01266 229.9007 40.40388 230.3828 38.69225 230.8649 37.35321 231.3471 36.38509 231.8292 35.88019 232.3113 36.08562 232.7934 36.49789 233.2755 36.72621 233.7576 36.69247 234.2398 36.57804 234.7219 36.63782 235.2040 36.57120 235.6861 37.35136 236.1682 39.67657 236.6503 42.39073 237.1325 44.41766 237.6146 45.47054 238.0967 46.09042 238.5788 47.15524 239.0609 49.33203 239.5430 50.36848 240.0252 49.70737 240.5073 48.13589 240.9894 46.37160 241.4715 44.54279 241.9536 42.01637 242.4357 39.71634 242.9179 36.22183 243.4000 32.83943 243.8821 29.10162 244.3642 25.73742 244.8463 23.81197 245.3284 23.57345 245.8106 23.77630 246.2927 22.83617 246.7748 20.77869 247.2569 19.49778 247.7390 19.59734 248.2211 20.28531 248.7033 20.63105 249.1854 20.49314 249.6675 20.32883 250.1496 20.72936 250.6317 21.61617 251.1138 22.19780 251.5960 21.80408 252.0781 21.17140 252.5602 21.26461 253.0423 22.21790 253.5244 23.66891 254.0065 25.70699 254.4887 28.03697 254.9708 29.81719 255.4529 30.33944 255.9350 30.41319 256.4171 31.20150 256.8992 32.90378 257.3813 34.78600 257.8635 36.41429 258.3456 37.86584 258.8277 39.22517 259.3098 40.16148 259.7919 41.21034 260.2740 43.44662 260.7562 47.24069 261.2383 50.61049 261.7204 51.94553 262.2025 52.29501 262.6846 52.86237 263.1667 54.00123 263.6489 55.48793 264.1310 57.21435 264.6131 59.36645 265.0952 60.94456 265.5773 60.94837 266.0594 60.35544 266.5416 60.05173 267.0237 60.31567 267.5058 60.82779 267.9879 61.25538 268.4700 61.65604 268.9521 61.70125 269.4343 61.08904 269.9164 60.16344 270.3985 59.00453 270.8806 57.58554 271.3627 56.37746 271.8448 56.10092 272.3270 56.95544 272.8091 57.69040 273.2912 57.77312 273.7733 57.79397 274.2554 58.05688 274.7375 58.62507 275.2197 59.49303 275.7018 60.82924 276.1839 62.76546 276.6660 64.27505 277.1481 64.82030 277.6302 65.16160 278.1124 65.79881 278.5945 66.69350 279.0766 67.28250 279.5587 66.91109 280.0408 65.47540 280.5229 64.03665 281.0051 63.19257 281.4872 61.83794 281.9693 59.24265 282.4514 55.63824 282.9335 51.86067 283.4156 48.75455 283.8978 46.34860 284.3799 43.24043 284.8620 38.59349 285.3441 34.04645 285.8262 29.84849 286.3083 26.18102 286.7905 23.38769 287.2726 21.97292 287.7547 21.71630 288.2368 20.46197 288.7189 16.89514 289.2010 13.87282 289.6832 12.39062 290.1653 11.89452 290.6474 11.55047 291.1295 10.91801 291.6116 10.03651 292.0938 9.059456 292.5759 7.965042 293.0580 6.797562 293.5401 5.223999 294.0222 3.714851 294.5043 2.920662 294.9865 3.153809 295.4686 3.931068 295.9507 4.064697 296.4328 3.197525 296.9149 2.280411 297.3970 1.204407 297.8792 0.2612230 298.3613 0.1836850 298.8434 5.2795000E-02 299.3255 0.2718730 299.8076 0.1085050 300.2897 0.8907010 300.7719 1.592094 301.2540 1.932716 301.7361 2.023079 302.2182 1.701553 302.7003 1.064629 303.1824 0.6366730 303.6646 1.269821 304.1467 3.585747 304.6288 4.661644 305.1109 3.537598 305.5930 2.101799 306.0751 0.9972080 306.5573 0.3511120 307.0394 0.1428150 307.5215 0.4497380 308.0036 1.335945 308.4857 1.824623 308.9678 1.490776 309.4500 1.161476 309.9321 1.125092 310.4142 1.274643 310.8963 1.343918 311.3784 1.137039 311.8605 1.112051 312.3427 0.4209210 312.8248 0.7063980 313.3069 0.6499560 313.7890 0.2980800 314.2711 1.563179 314.7532 2.346283 315.2354 2.229599 315.7175 1.571014 316.1996 1.406921 316.6817 2.057961 317.1638 2.733559 317.6459 3.257622 318.1281 3.807724 318.6102 4.640282 319.0923 5.808853 319.5744 7.000862 320.0565 7.578979 320.5386 6.926888 321.0208 7.119141 321.5029 8.747948 321.9850 10.72223 322.4671 12.48248 322.9492 13.89664 323.4313 15.06641 323.9135 16.11382 324.3956 17.01350 324.8777 17.94459 325.3598 18.75235 325.8419 19.72823 326.3240 21.05520 326.8062 22.71654 327.2883 24.61968 327.7704 26.70358 328.2525 28.80984 328.7346 30.15677 329.2167 29.89143 329.6989 29.95898 330.1810 30.91650 330.6631 32.50392 331.1452 34.38798 331.6273 36.29134 332.1094 38.06770 332.5916 39.82204 333.0737 41.66354 333.5558 43.40487 334.0379 44.80450 334.5200 46.22209 335.0021 48.02003 335.4843 50.32491 335.9664 52.92795 336.4485 55.44899 336.9306 57.89360 337.4127 59.94800 337.8948 61.12978 338.3770 62.28107 338.8591 64.16286 339.3412 66.69476 339.8233 68.93607 340.3055 69.78008 340.7876 69.05906 341.2697 68.61307 341.7518 68.73409 342.2339 68.86319 342.7160 68.94118 343.1982 68.86210 343.6803 68.42580 344.1624 67.45819 344.6445 66.03188 345.1266 64.41556 345.6087 62.10635 346.0909 60.48431 346.5730 60.39278 347.0551 60.99280 347.5372 61.20752 348.0193 60.55241 348.5014 59.48559 348.9836 58.77374 349.4657 58.41443 349.9478 58.43800 350.4299 59.41302 350.9120 60.43219 351.3941 60.67793 351.8763 60.01588 352.3584 59.26138 352.8405 59.18603 353.3226 59.79892 353.8047 60.87213 354.2868 62.87254 354.7690 64.81343 355.2511 66.17102 355.7332 66.95969 356.2153 67.30698 356.6974 67.11934 357.1795 66.54510 357.6617 66.17860 358.1438 66.09863 358.6259 65.95242 359.1080 65.62134 359.5901 65.11733 360.0722 64.44360 360.5544 63.63058 361.0365 62.62744 361.5186 61.30107 362.0007 59.54762 362.4828 57.49600 362.9649 55.04118 363.4471 52.59598 363.9292 50.57098 364.4113 49.00587 364.8934 47.70071 365.3755 46.63545 365.8576 45.70815 366.3398 44.55681 366.8219 43.11803 367.3040 41.48340 367.7861 39.69347 368.2682 37.75462 368.7503 35.82034 369.2325 33.97791 369.7146 32.19131 370.1967 30.37016 370.6788 28.46639 371.1609 26.55172 371.6430 24.77239 372.1252 23.02294 372.6073 21.11705 373.0894 18.79922 373.5715 16.49863 374.0536 14.58471 374.5357 13.02694 375.0179 11.58253 375.5000 10.17313 375.9821 8.796074 376.4642 7.414421 376.9463 5.973305 377.4284 4.657005 377.9106 3.549736 378.3927 2.614830 378.8748 1.725700 379.3569 0.8230210 379.8390 0.1757200 380.3211 0.2750470 380.8033 1.333221 381.2854 1.862389 381.7675 1.331352 382.2496 0.5393910 382.7317 0.1727680 383.2138 0.2214970 383.6960 0.1260990 384.1781 0.6565700 384.6602 0.5035266 385.1423 0.4927469 385.6244 0.9354550 386.1065 0.4486620 386.5887 1.447052 387.0708 1.954613 387.5529 1.610207 388.0350 0.2045820 388.5171 1.561501 388.9992 2.129684 389.4814 0.2372510 389.9635 0.9654920 390.4456 1.137108 390.9277 0.8609160 391.4098 0.5231020 391.8919 0.2221830 392.3741 0.1038670 392.8562 0.6054920 393.3383 1.428680 393.8204 1.273643 394.3025 1.017479 394.7846 3.019058 395.2668 3.722061 395.7489 3.552086 396.2310 3.387062 396.7131 3.738266 397.1952 4.454842 397.6773 5.003044 398.1595 5.206917 398.6416 5.536987 399.1237 6.158623 399.6058 6.851723 400.0879 7.396820 400.5700 7.756332 401.0522 8.104996 401.5343 8.737404 402.0164 9.751045 402.4985 10.43358 402.9806 10.17274 403.4627 10.13904 403.9449 11.00858 404.4270 12.52954 404.9091 14.02768 405.3912 15.17345 405.8733 15.95213 406.3554 16.18791 406.8376 15.55797 407.3197 15.19907 407.8018 15.93039 408.2839 16.98877 408.7660 17.51142 409.2481 17.20728 409.7303 16.86169 410.2124 17.50365 410.6945 19.03725 411.1766 19.95910 411.6587 19.81044 412.1408 19.10791 412.6230 18.13173 413.1051 16.95918 413.5872 16.22063 414.0693 16.73785 414.5514 17.64516 415.0335 17.31023 415.5157 15.51504 415.9978 13.90741 416.4799 13.63651 416.9620 14.37862 417.4441 14.98935 417.9262 15.46436 418.4084 15.75470 418.8905 15.75440 419.3726 15.54451 419.8547 15.32228 420.3368 15.14741 420.8189 15.00745 421.3011 14.83154 421.7832 14.51253 422.2653 14.60754 422.7474 15.73526 423.2295 16.92557 423.7116 17.19573 424.1938 16.57737 424.6759 15.91544 425.1580 15.86156 425.6401 16.38851 426.1222 16.96124 426.6043 17.36318 427.0865 17.98643 427.5686 19.11578 428.0507 20.49580 428.5328 21.78027 429.0149 22.82842 429.4970 23.69273 429.9792 24.48163 430.4613 25.18614 430.9434 25.93247 431.4255 27.26373 431.9076 28.14148 432.3897 27.70566 432.8719 26.17803 433.3540 24.50525 433.8361 23.46399 434.3182 23.01355 434.8003 22.53987 435.2824 22.15797 435.7646 21.56902 436.2467 20.35193 436.7288 18.95458 437.2109 18.03149 437.6930 17.83360 438.1751 17.80063 438.6573 16.86057 439.1394 14.87022 439.6215 14.01774 440.1036 15.33298 440.5857 16.95883 441.0678 17.53988 441.5500 17.39262 442.0321 17.64955 442.5142 18.97247 442.9963 20.94389 443.4784 23.03047 443.9605 25.26006 444.4427 27.45571 444.9248 29.40401 445.4069 31.33968 445.8890 33.72848 446.3711 36.83500 446.8532 39.48184 447.3354 40.57214 447.8175 40.84119 448.2996 42.14811 448.7817 45.00489 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