#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-04-26 14:00:22 +0300 (Thu, 26 Apr 2018) $
#$Revision: 591 $
#$URL: svn://172.16.1.111/rod/cif/1/00/01/1000131.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000131
loop_
_publ_author_name
'Leone, P.'
'Palvadeau, P.'
'Moelo, Y.'
_publ_section_title
;
 Structure cristalline d'un nouvel hydroxyphosphate naturel de strontium,
 fer et aluminium (lulzacite), Sr2Fe(Fe0,63Mg0,37)2Al4(PO4)4(OH)10
;
_journal_name_full               'Chimie de l etat Solide et Cristallochimie'
_journal_page_first              301
_journal_page_last               308
_journal_volume                  3
_journal_year                    2000
_chemical_compound_source
'Saint-Aubin-des-Chateaux, Loire-Atlantique, France'
_chemical_formula_sum
'Al4 Ba0.08 Fe2.26 H4 Mg0.74 O26 P3.92 Sr1.92 V0.08'
_chemical_name_mineral           Lulzacite
_space_group_IT_number           2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                108.47
_cell_angle_beta                 91.72
_cell_angle_gamma                97.44
_cell_length_a                   5.457
_cell_length_b                   9.131
_cell_length_c                   9.769
_cell_volume                     456.500
_exptl_crystal_density_diffrn    3.553
_cod_original_formula_sum
'(Sr1.92 Ba.08) (P3.92 V.08) Fe2.26 Al4 Mg.74 O26 H4'
_cod_database_code               9014177
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type helium-neon
_raman_measurement_device.excitation_laser_wavelength 780
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 12
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R110147.rod
_rod_data_source.block           3500000
_rod_database.code               1000131
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9014177 COD http://www.crystallography.net/cod/9014177.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
113.2988 0.0000000E+00
113.7809 0.2625320
114.2630 2.2760000E-02
114.7451 8.9180004E-03
115.2272 0.6654710
115.7094 1.844520
116.1915 2.578833
116.6736 2.403507
117.1557 2.301738
117.6378 2.676664
118.1199 3.434442
118.6021 4.183599
119.0842 4.560481
119.5663 4.534884
120.0484 4.808860
120.5305 5.542222
121.0126 6.449203
121.4948 7.278123
121.9769 7.991419
122.4590 8.708336
122.9411 9.765271
123.4232 11.03441
123.9053 11.84709
124.3875 11.77617
124.8696 11.08895
125.3517 10.47893
125.8338 9.986142
126.3159 9.525558
126.7980 8.968543
127.2802 8.365327
127.7623 7.894508
128.2444 7.678517
128.7265 7.733076
129.2086 7.786486
129.6907 8.026079
130.1729 8.130630
130.6550 7.913472
131.1371 7.375541
131.6192 6.690597
132.1013 6.034333
132.5834 5.437755
133.0656 4.942697
133.5477 4.123856
134.0298 3.196762
134.5119 2.384254
134.9940 2.083539
135.4761 1.949503
135.9583 1.830713
136.4404 1.769161
136.9225 1.949147
137.4046 2.084342
137.8867 2.171297
138.3688 2.458847
138.8510 2.864423
139.3331 3.228381
139.8152 3.541384
140.2973 4.030890
140.7794 4.350571
141.2615 4.264742
141.7437 3.860752
142.2258 3.451944
142.7079 3.479684
143.1900 3.802262
143.6721 4.030429
144.1542 4.165430
144.6364 4.144656
145.1185 3.843107
145.6006 3.209888
146.0827 2.672381
146.5648 2.534841
147.0469 2.574085
147.5291 2.599563
148.0112 2.581303
148.4933 2.476076
148.9754 2.151138
149.4575 1.404245
149.9396 0.7875280
150.4218 0.5351160
150.9039 0.4829940
151.3860 0.4008680
151.8681 0.1133260
152.3502 0.3122720
152.8323 1.5343000E-02
153.3145 6.9269999E-03
153.7966 6.7699000E-02
154.2787 0.3236920
154.7608 1.0923000E-02
155.2429 0.1830100
155.7250 5.4044999E-02
156.2072 0.2286800
156.6893 7.9699997E-03
157.1714 0.2422210
157.6535 0.1867250
158.1356 0.2108650
158.6177 0.1843180
159.0999 0.1522220
159.5820 0.4531810
160.0641 0.7287580
160.5462 0.7502370
161.0283 0.2618200
161.5104 0.2991720
161.9926 4.1777000E-02
162.4747 6.5249003E-02
162.9568 0.2231430
163.4389 0.2368620
163.9210 6.5407999E-02
164.4031 7.0358999E-02
164.8853 0.1915940
165.3674 0.3205570
165.8495 0.7002510
166.3316 0.9112330
166.8137 0.9785050
167.2958 0.8915730
167.7780 0.6801180
168.2601 0.4286710
168.7422 8.3700001E-02
169.2243 0.2931650
169.7064 0.1886450
170.1885 0.2811420
170.6707 7.5561002E-02
171.1528 0.7604810
171.6349 1.606610
172.1170 2.265342
172.5991 2.377315
173.0812 1.908937
173.5634 1.538249
174.0455 1.259605
174.5276 1.128164
175.0097 1.274889
175.4918 1.642889
175.9739 2.006388
176.4561 2.104094
176.9382 1.847486
177.4203 1.615240
177.9024 1.362389
178.3845 1.163743
178.8666 1.072269
179.3488 1.089157
179.8309 1.172494
180.3130 1.273855
180.7951 1.418490
181.2772 1.520074
181.7593 1.554914
182.2415 1.568607
182.7236 1.602951
183.2057 1.665583
183.6878 1.732426
184.1699 1.744626
184.6520 1.658645
185.1342 1.612541
185.6163 1.577773
186.0984 1.592613
186.5805 1.781704
187.0626 2.193954
187.5447 2.590545
188.0269 2.508547
188.5090 1.809798
188.9911 1.292837
189.4732 1.187130
189.9553 1.375214
190.4374 1.694500
190.9196 2.148826
191.4017 2.583532
191.8838 2.775396
192.3659 2.735154
192.8480 2.630247
193.3301 2.509090
193.8123 2.375507
194.2944 2.248352
194.7765 2.129467
195.2586 2.027880
195.7407 1.944223
196.2228 1.878518
196.7050 1.835646
197.1871 1.835944
197.6692 1.887007
198.1513 1.923434
198.6334 1.856024
199.1155 1.814880
199.5977 1.917562
200.0798 2.138269
200.5619 2.361325
201.0440 2.475386
201.5261 2.465533
202.0082 2.459754
202.4904 2.511513
202.9725 2.532151
203.4546 2.453876
203.9367 2.283914
204.4188 2.109613
204.9009 2.041171
205.3831 2.109250
205.8652 2.207003
206.3473 2.401668
206.8294 2.565061
207.3115 2.601275
207.7936 2.493281
208.2758 2.320853
208.7579 2.169214
209.2400 1.983310
209.7221 1.952461
210.2042 2.124768
210.6863 2.369490
211.1685 2.614733
211.6506 2.829223
212.1327 2.970861
212.6148 2.996134
213.0969 2.718095
213.5790 2.637065
214.0612 2.889334
214.5433 3.220078
215.0254 3.376951
215.5075 3.322925
215.9896 3.205464
216.4718 3.252165
216.9539 3.568398
217.4360 3.821362
217.9181 4.070710
218.4002 4.241664
218.8823 4.236488
219.3645 4.006735
219.8466 3.726295
220.3287 3.573832
220.8108 3.547120
221.2929 3.567267
221.7750 3.694102
222.2572 3.850500
222.7393 3.927854
223.2214 3.896185
223.7035 3.869450
224.1856 4.087717
224.6677 4.530859
225.1499 4.810500
225.6320 4.706567
226.1141 4.405649
226.5962 4.198720
227.0783 4.104764
227.5604 4.113618
228.0426 4.300066
228.5247 4.631004
229.0068 4.798917
229.4889 4.536666
229.9710 4.043001
230.4531 3.801268
230.9353 3.973466
231.4174 4.149855
231.8995 4.039876
232.3816 3.697008
232.8637 3.235321
233.3458 2.573270
233.8280 1.821206
234.3101 1.344692
234.7922 1.252953
235.2743 1.288215
235.7564 1.349062
236.2385 1.410873
236.7207 1.419504
237.2028 1.319099
237.6849 1.140053
238.1670 1.017155
238.6491 1.010115
239.1312 0.9691160
239.6134 0.8681560
240.0955 0.6938160
240.5776 0.4026840
241.0597 8.7067001E-02
241.5418 0.1659160
242.0239 0.5062060
242.5061 0.4284020
242.9882 0.2644750
243.4703 6.8836004E-02
243.9524 0.1312010
244.4345 0.2521510
244.9166 0.1261900
245.3988 3.9960999E-02
245.8809 2.0768000E-02
246.3630 5.7905000E-02
246.8451 5.5902001E-02
247.3272 3.4910999E-02
247.8093 0.1483910
248.2915 0.1921320
248.7736 0.1108790
249.2557 5.7085000E-02
249.7378 0.1517210
250.2199 5.8030002E-02
250.7020 3.1493001E-02
251.1842 0.1870820
251.6663 0.3993920
252.1484 0.5080100
252.6305 0.4343860
253.1126 0.2402750
253.5947 0.1195940
254.0769 0.2449620
254.5590 0.2330520
255.0411 0.1063020
255.5232 0.1684450
256.0053 5.0686002E-02
256.4874 4.3984000E-02
256.9695 0.3460950
257.4517 0.1266030
257.9338 0.1427270
258.4159 0.2593070
258.8980 0.1247850
259.3801 0.1218910
259.8622 0.3535240
260.3444 0.2494550
260.8265 0.1408760
261.3086 7.1544997E-02
261.7907 1.5495000E-02
262.2728 5.1821001E-02
262.7549 0.2718630
263.2371 0.2797400
263.7192 0.1222070
264.2013 0.1066130
264.6834 0.1216880
265.1655 4.5679999E-03
265.6476 0.3612030
266.1298 0.6458020
266.6119 0.9002910
267.0940 1.055947
267.5761 0.9864290
268.0582 0.6793530
268.5403 0.3426500
269.0225 0.2160230
269.5046 0.3497780
269.9867 0.5272930
270.4688 0.8009630
270.9509 1.079435
271.4330 1.278051
271.9152 1.390019
272.3973 1.468682
272.8794 1.534050
273.3615 1.590198
273.8436 1.805958
274.3257 2.458667
274.8079 3.079197
275.2900 3.157132
275.7721 2.712035
276.2542 2.380176
276.7363 2.731127
277.2184 3.667013
277.7006 4.199356
278.1827 3.961140
278.6648 3.605362
279.1469 3.582086
279.6290 3.868368
280.1111 4.232425
280.5933 4.601146
281.0754 4.916011
281.5575 5.035241
282.0396 4.824989
282.5217 4.585046
283.0038 4.458123
283.4860 4.445325
283.9681 4.561440
284.4502 4.855313
284.9323 5.253906
285.4144 5.605802
285.8965 5.925861
286.3787 6.170967
286.8608 6.236775
287.3429 6.188312
287.8250 6.314657
288.3071 6.851090
288.7892 7.399415
289.2714 7.325338
289.7535 6.562168
290.2356 5.839456
290.7177 5.500784
291.1998 5.459355
291.6819 5.519306
292.1641 5.708121
292.6462 5.849074
293.1283 5.693576
293.6104 5.280724
294.0925 4.906720
294.5746 4.676752
295.0568 4.567613
295.5389 4.582158
296.0210 4.784089
296.5031 4.919877
296.9852 4.653390
297.4673 4.126068
297.9495 3.720956
298.4316 3.638702
298.9137 3.710340
299.3958 3.738633
299.8779 3.723942
300.3600 3.602957
300.8422 3.213973
301.3243 2.696869
301.8064 2.275818
302.2885 1.958794
302.7706 1.807716
303.2527 1.959999
303.7349 2.440868
304.2170 2.834893
304.6991 2.823349
305.1812 2.665158
305.6633 2.744090
306.1454 3.200590
306.6276 3.687829
307.1097 3.829307
307.5918 3.642350
308.0739 3.620911
308.5560 4.092791
309.0381 4.650808
309.5203 4.827841
310.0024 4.587258
310.4845 4.226049
310.9666 3.838049
311.4487 3.463806
311.9308 3.334781
312.4130 3.593086
312.8951 3.965056
313.3772 4.263040
313.8593 4.494112
314.3414 4.571648
314.8235 4.256895
315.3057 3.781446
315.7878 3.736567
316.2699 4.322736
316.7520 4.946342
317.2341 5.100581
317.7162 4.985758
318.1984 4.964485
318.6805 5.207237
319.1626 5.592376
319.6447 5.892296
320.1268 6.142625
320.6089 6.427819
321.0911 6.822271
321.5732 7.263258
322.0553 7.605441
322.5374 7.755972
323.0195 7.834072
323.5016 7.995640
323.9838 8.244220
324.4659 8.625731
324.9480 9.296513
325.4301 9.941950
325.9122 10.15274
326.3943 9.841893
326.8765 9.503986
327.3586 9.546892
327.8407 9.884396
328.3228 10.07519
328.8049 10.00697
329.2870 9.719747
329.7692 9.174725
330.2513 8.420254
330.7334 7.889529
331.2155 8.015304
331.6976 8.451772
332.1797 8.367481
332.6619 7.530074
333.1440 6.643086
333.6261 6.326293
334.1082 6.403639
334.5903 6.503193
335.0724 6.575309
335.5546 6.581300
336.0367 6.447252
336.5188 6.163242
337.0009 5.845912
337.4831 5.493496
337.9652 5.177046
338.4473 5.027418
338.9294 5.092780
339.4115 5.274123
339.8936 5.612046
340.3758 6.061441
340.8579 6.249463
341.3400 5.940362
341.8221 5.392789
342.3042 4.985173
342.7863 4.708923
343.2685 4.576647
343.7506 4.664193
344.2327 4.897560
344.7148 5.110628
345.1969 5.278850
345.6790 5.392410
346.1612 5.451217
346.6433 5.459339
347.1254 5.349082
347.6075 4.925763
348.0896 4.460500
348.5717 4.370052
349.0539 4.702964
349.5360 5.005075
350.0181 4.885226
350.5002 4.444760
350.9823 4.182797
351.4644 4.163760
351.9466 4.299478
352.4287 4.655966
352.9108 5.163935
353.3929 5.488681
353.8750 5.438021
354.3571 5.127094
354.8393 4.852846
355.3214 4.651544
355.8035 4.404354
356.2856 3.939257
356.7677 3.423932
357.2498 3.215511
357.7320 3.450641
358.2141 3.814376
358.6962 3.836102
359.1783 3.434495
359.6604 3.215301
360.1425 3.502962
360.6247 3.843720
361.1068 3.700659
361.5889 3.063437
362.0710 2.500330
362.5531 2.526544
363.0352 3.135837
363.5174 3.494777
363.9995 3.424210
364.4816 3.308719
364.9637 3.410746
365.4458 3.619546
365.9279 3.593749
366.4101 3.116100
366.8922 2.377912
367.3743 2.021200
367.8564 2.400651
368.3385 2.630545
368.8206 2.520532
369.3028 2.236198
369.7849 1.917380
370.2670 1.614420
370.7491 1.402622
371.2312 1.418790
371.7133 1.830887
372.1955 1.936734
372.6776 1.553967
373.1597 1.045312
373.6418 0.5952400
374.1239 0.2235240
374.6060 0.1342930
375.0882 0.5562820
375.5703 0.2035130
376.0524 3.8669001E-02
376.5345 0.6091600
377.0166 0.2425520
377.4987 0.3417220
377.9809 0.5068400
378.4630 6.5035000E-02
378.9451 0.3211600
379.4272 0.5999250
379.9093 0.6175590
380.3914 3.2094002E-02
380.8736 0.2334600
381.3557 0.1180040
381.8378 0.5787930
382.3199 0.7734570
382.8020 0.6544060
383.2841 0.4186140
383.7663 0.2946960
384.2484 0.3147500
384.7305 0.2177950
385.2126 0.1310890
385.6947 0.4724000
386.1768 0.5153960
386.6590 0.2971000
387.1411 0.2045000
387.6232 0.2958440
388.1053 0.4932560
388.5874 0.5110710
389.0695 0.2764740
389.5517 9.9630002E-03
390.0338 0.3786390
390.5159 0.7305150
390.9980 0.9528930
391.4801 1.016831
391.9622 1.030547
392.4444 1.139511
392.9265 1.358672
393.4086 1.528389
393.8907 1.612461
394.3728 1.653605
394.8549 1.667874
395.3371 1.660008
395.8192 1.639163
396.3013 1.566790
396.7834 1.487027
397.2655 1.578657
397.7477 1.923926
398.2298 2.225956
398.7119 2.278673
399.1940 2.210402
399.6761 2.174168
400.1582 2.208052
400.6404 2.283892
401.1225 2.387662
401.6046 2.517572
402.0867 2.623275
402.5688 2.651567
403.0509 2.694782
403.5331 2.851672
404.0152 3.120734
404.4973 3.459248
404.9794 3.951218
405.4615 4.471845
405.9436 4.753656
406.4258 4.735321
406.9079 4.720768
407.3900 5.006676
407.8721 5.520785
408.3542 5.875084
408.8363 5.947438
409.3185 5.938548
409.8006 5.921501
410.2827 5.918746
410.7648 6.024089
411.2469 6.306428
411.7290 6.664353
412.2112 6.842346
412.6933 6.717614
413.1754 6.753210
413.6575 7.158970
414.1396 7.684979
414.6217 8.082919
415.1039 8.311989
415.5860 8.471174
416.0681 8.633683
416.5502 8.768627
417.0323 9.132634
417.5144 9.988604
417.9966 10.77488
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