#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-04-26 14:00:53 +0300 (Thu, 26 Apr 2018) $
#$Revision: 599 $
#$URL: svn://172.16.1.111/rod/cif/1/00/01/1000138.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000138
loop_
_publ_author_name
'Nomura, S. F.'
'Atencio, D.'
'Chukanov, N. V.'
'Rastsvetaeva, R. K.'
'Coutinho, J. M. V.'
'Karipidis, T. K.'
_publ_section_title
;
 Manganoeudialyte - a new mineral from Pocos de Caldas, Minas Gerais,
 Brazil
;
_journal_name_full
'Zapiski Rossiiskogo Mineralogicheskogo Obshchetstva'
_journal_page_first              35
_journal_page_last               47
_journal_volume                  139
_journal_year                    2010
_chemical_compound_source
'Pocos de Caldas massif, Minas Gerais, Brazil'
_chemical_formula_sum
'C2.64 H40.56 Al0.75 Ca18 Ce0.18 F0.39 Fe3.6 K1.17 Mn5.72 Na47.84 Nb0.87 O254.37 Si75.57 Sr2.43 Ti0.57 Zr9.24'
_chemical_name_mineral           Manganoeudialyte
_space_group_IT_number           160
_symmetry_space_group_name_Hall  'R 3 -2"'
_symmetry_space_group_name_H-M   'R 3 m :H'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                120
_cell_length_a                   14.2418
_cell_length_b                   14.2418
_cell_length_c                   30.1143
_cell_volume                     5289.726
_exptl_crystal_density_diffrn    3.096
_cod_original_sg_symbol_H-M      'R 3 m'
_cod_original_formula_sum
'Zr9.24 Ca18 Si75.57 O254.37 Mn5.72 Fe3.6 Na47.84 Al.75 Nb.87 Ti.57 K1.17 Sr2.43 Ce.18 H40.56 C2.64 F.39'
_cod_database_code               9015914
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type helium-neon
_raman_measurement_device.excitation_laser_wavelength 780
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 12
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R110212.rod
_rod_data_source.block           3500000
_rod_database.code               1000138
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9015914 COD http://www.crystallography.net/cod/9015914.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
129.6907 0.0000000E+00
130.1729 0.1265870
130.6550 6.5552004E-02
131.1371 1.721252
131.6192 4.448669
132.1013 7.215942
132.5834 9.433960
133.0656 12.64569
133.5477 17.13940
134.0298 22.19641
134.5119 27.40869
134.9940 32.61615
135.4761 37.76361
135.9583 42.66089
136.4404 46.62512
136.9225 51.08289
137.4046 56.40887
137.8867 62.24023
138.3688 68.17896
138.8510 74.19208
139.3331 80.00641
139.8152 84.60333
140.2973 87.56885
140.7794 90.14160
141.2615 92.91205
141.7437 95.69891
142.2258 97.75232
142.7079 98.35443
143.1900 98.20392
143.6721 98.78717
144.1542 100.9209
144.6364 102.9341
145.1185 102.9520
145.6006 100.7643
146.0827 97.93604
146.5648 95.13977
147.0469 92.55969
147.5291 89.35651
148.0112 85.11029
148.4933 80.89520
148.9754 77.80713
149.4575 76.26392
149.9396 74.30408
150.4218 70.95032
150.9039 67.04590
151.3860 62.98499
151.8681 58.98682
152.3502 55.17041
152.8323 51.15277
153.3145 46.26385
153.7966 42.08966
154.2787 39.47870
154.7608 38.09454
155.2429 36.51526
155.7250 33.46130
156.2072 28.83734
156.6893 25.39398
157.1714 23.86053
157.6535 22.41626
158.1356 20.28162
158.6177 17.55457
159.0999 14.93469
159.5820 13.08258
160.0641 12.14380
160.5462 11.12317
161.0283 9.875549
161.5104 8.651184
161.9926 7.760437
162.4747 7.236084
162.9568 6.606445
163.4389 5.136047
163.9210 2.889404
164.4031 1.328064
164.8853 1.259583
165.3674 1.859314
165.8495 1.887695
166.3316 1.053162
166.8137 3.2837000E-02
167.2958 0.8575440
167.7780 1.463989
168.2601 1.939209
168.7422 2.351929
169.2243 2.673889
169.7064 2.754883
170.1885 2.389954
170.6707 2.016235
171.1528 2.004395
171.6349 2.268188
172.1170 2.436279
172.5991 2.144958
173.0812 1.366882
173.5634 0.7202150
174.0455 0.3547360
174.5276 3.6132999E-02
175.0097 0.3305660
175.4918 0.7433470
175.9739 1.135254
176.4561 1.327576
176.9382 1.078003
177.4203 1.500122
177.9024 3.468811
178.3845 5.344971
178.8666 6.042725
179.3488 5.549072
179.8309 4.744019
180.3130 4.855408
180.7951 6.288635
181.2772 8.010925
181.7593 10.72296
182.2415 13.39557
182.7236 14.84613
183.2057 14.77148
183.6878 14.12878
184.1699 14.84570
184.6520 18.11444
185.1342 20.93695
185.6163 23.50671
186.0984 25.58484
186.5805 26.77368
187.0626 27.12360
187.5447 27.67828
188.0269 29.04364
188.5090 31.40100
188.9911 33.72302
189.4732 35.79175
189.9553 37.67279
190.4374 39.40729
190.9196 40.95886
191.4017 42.50525
191.8838 44.26843
192.3659 46.19446
192.8480 48.42419
193.3301 51.47479
193.8123 54.98608
194.2944 57.57178
194.7765 58.45215
195.2586 58.75885
195.7407 59.71753
196.2228 61.33301
196.7050 63.11700
197.1871 64.80267
197.6692 66.38788
198.1513 67.82727
198.6334 69.26520
199.1155 70.38721
199.5977 70.84796
200.0798 70.67145
200.5619 70.41113
201.0440 70.70691
201.5261 71.69867
202.0082 72.34814
202.4904 72.42047
202.9725 72.18518
203.4546 71.65381
203.9367 70.87299
204.4188 70.02020
204.9009 69.32794
205.3831 68.87592
205.8652 68.34003
206.3473 67.80920
206.8294 67.12164
207.3115 66.23602
207.7936 65.11938
208.2758 63.68805
208.7579 61.70044
209.2400 58.43292
209.7221 56.28601
210.2042 56.22882
210.6863 56.41785
211.1685 55.54926
211.6506 53.39514
212.1327 50.67291
212.6148 48.39441
213.0969 46.84564
213.5790 45.21771
214.0612 43.38660
214.5433 41.54480
215.0254 39.89722
215.5075 38.48480
215.9896 37.09503
216.4717 35.42285
216.9539 33.26868
217.4360 31.28320
217.9181 29.62335
218.4002 28.07159
218.8823 26.36914
219.3644 24.45288
219.8466 22.51331
220.3287 20.76276
220.8108 19.15118
221.2929 17.95538
221.7750 17.58508
222.2571 17.48395
222.7393 17.03558
223.2214 16.12659
223.7035 14.88336
224.1856 13.23962
224.6677 11.19946
225.1498 9.453003
225.6320 8.392456
226.1141 7.708862
226.5962 6.899231
227.0783 5.879517
227.5604 4.781616
228.0425 3.658875
228.5247 2.545532
229.0068 1.627808
229.4889 1.108093
229.9710 0.8173220
230.4531 0.3783570
230.9352 0.2873540
231.4174 0.9382930
231.8995 1.345459
232.3816 1.595947
232.8637 1.923950
233.3458 2.482483
233.8279 3.215332
234.3101 3.973022
234.7922 4.888855
235.2743 5.598694
235.7564 5.985107
236.2385 6.050293
236.7206 5.723206
237.2028 4.690857
237.6849 3.227722
238.1670 2.529541
238.6491 3.140198
239.1312 3.702576
239.6133 3.497437
240.0955 2.886475
240.5776 2.530273
241.0597 3.017639
241.5418 4.024231
242.0239 3.876221
242.5060 1.403503
242.9882 0.6763310
243.4703 1.494385
243.9524 1.463135
244.4345 1.144470
244.9166 0.7885740
245.3987 0.4721680
245.8809 0.5710450
246.3630 1.283997
246.8451 2.210022
247.3272 3.468018
247.8093 4.820068
248.2914 6.016174
248.7736 6.940491
249.2557 7.546082
249.7378 7.611084
250.2199 6.484009
250.7020 5.602234
251.1841 5.337769
251.6663 5.354614
252.1484 5.232361
252.6305 4.767761
253.1126 4.087341
253.5947 3.588501
254.0768 3.453003
254.5590 3.302673
255.0411 2.965271
255.5232 2.659363
256.0053 2.625916
256.4874 2.966125
256.9695 3.612854
257.4517 4.401733
257.9338 5.731445
258.4159 6.716797
258.8980 7.185608
259.3801 7.380066
259.8622 7.454041
260.3444 7.470886
260.8265 7.610352
261.3086 8.227905
261.7907 9.848450
262.2728 11.13879
262.7549 12.14716
263.2371 12.79169
263.7192 12.83484
264.2013 12.23907
264.6834 11.42261
265.1655 10.95496
265.6476 10.77356
266.1298 11.26978
266.6119 13.15485
267.0940 15.34198
267.5761 16.69067
268.0582 17.01221
268.5403 17.14026
269.0225 18.18933
269.5046 20.56378
269.9867 21.80658
270.4688 21.07898
270.9509 19.68567
271.4330 18.62799
271.9152 18.04645
272.3973 17.74213
272.8794 17.59424
273.3615 17.61560
273.8436 17.50012
274.3257 17.15900
274.8079 16.73706
275.2900 16.13031
275.7721 15.39166
276.2542 15.15308
276.7363 16.08893
277.2184 18.05084
277.7006 19.46753
278.1827 19.95123
278.6648 20.17767
279.1469 20.57123
279.6290 21.12073
280.1111 21.70264
280.5933 22.33160
281.0754 22.88983
281.5575 23.08710
282.0396 22.77301
282.5217 22.29315
283.0038 21.75055
283.4860 21.18250
283.9681 20.77411
284.4502 20.60669
284.9323 20.67334
285.4144 20.84497
285.8965 20.96637
286.3787 21.52979
286.8608 23.27502
287.3429 25.79724
287.8250 27.57074
288.3071 27.84540
288.7892 27.45398
289.2714 27.62579
289.7535 28.39478
290.2356 29.33197
290.7177 30.41156
291.1998 31.49609
291.6819 32.29974
292.1641 32.82538
292.6462 32.89490
293.1283 31.97534
293.6104 30.22656
294.0925 29.08282
294.5746 29.45251
295.0568 30.81104
295.5389 32.09399
296.0210 33.12384
296.5031 34.00604
296.9852 34.79553
297.4673 35.57025
297.9495 36.50970
298.4316 38.07495
298.9137 39.62390
299.3958 40.08624
299.8779 39.31744
300.3600 38.42413
300.8422 37.77032
301.3243 37.39093
301.8064 37.45520
302.2885 37.87677
302.7706 38.88287
303.2527 41.25775
303.7349 45.17273
304.2170 48.10229
304.6991 47.94733
305.1812 46.52246
305.6633 46.39587
306.1454 48.28479
306.6276 50.47247
307.1097 51.38165
307.5918 51.08521
308.0739 50.87598
308.5560 51.26691
309.0381 51.83423
309.5203 52.03625
310.0024 51.81995
310.4845 51.67023
310.9666 52.18982
311.4487 53.15192
311.9308 53.36639
312.4130 52.31848
312.8951 50.84149
313.3772 49.60693
313.8593 48.60437
314.3414 47.86774
314.8235 47.59442
315.3057 47.58899
315.7878 47.30359
316.2699 46.57867
316.7520 45.85205
317.2341 45.66693
317.7162 45.73944
318.1984 45.39642
318.6805 43.94531
319.1626 42.15393
319.6447 41.25653
320.1268 41.36078
320.6089 41.84113
321.0911 42.63257
321.5732 43.51898
322.0553 44.12427
322.5374 44.13751
323.0195 44.24719
323.5016 45.37537
323.9838 47.53949
324.4659 49.39435
324.9480 50.24976
325.4301 50.63733
325.9122 51.11450
326.3943 51.66199
326.8765 52.58301
327.3586 54.16705
327.8407 56.34894
328.3228 58.85376
328.8049 62.04919
329.2870 64.91315
329.7692 66.06000
330.2513 65.66162
330.7334 65.75330
331.2155 67.77167
331.6976 70.93713
332.1797 73.40594
332.6619 74.85248
333.1440 75.97711
333.6261 77.18951
334.1082 78.50232
334.5903 80.01526
335.0724 81.83649
335.5546 83.82098
336.0367 85.90234
336.5188 88.11017
337.0009 90.00604
337.4830 91.33929
337.9651 92.15955
338.4473 92.58105
338.9294 92.57941
339.4115 92.24139
339.8936 91.53394
340.3757 90.49530
340.8578 89.41083
341.3400 88.32483
341.8221 87.30249
342.3042 86.48804
342.7863 85.94623
343.2684 85.23541
343.7505 84.04004
344.2327 82.51758
344.7148 81.07800
345.1969 79.85956
345.6790 78.59674
346.1611 76.99908
346.6432 75.10925
347.1254 72.93616
347.6075 70.13300
348.0896 67.21851
348.5717 64.87054
349.0538 63.14392
349.5359 61.77930
350.0181 60.78894
350.5002 60.01849
350.9823 58.80945
351.4644 56.67694
351.9465 54.48834
352.4286 53.02881
352.9108 52.10779
353.3929 50.64496
353.8750 47.80658
354.3571 44.43774
354.8392 42.72498
355.3214 43.30737
355.8035 43.91736
356.2856 43.89276
356.7677 43.24084
357.2498 41.97931
357.7319 40.12793
358.2141 37.92505
358.6962 35.39984
359.1783 32.31757
359.6604 30.04657
360.1425 29.52258
360.6246 29.35712
361.1068 28.11420
361.5889 25.75201
362.0710 23.55481
362.5531 22.71509
363.0352 23.14868
363.5173 22.48145
363.9995 19.39099
364.4816 16.59650
364.9637 15.63550
365.4458 16.02808
365.9279 16.49524
366.4100 16.40759
366.8922 15.89526
367.3743 15.34583
367.8564 14.26984
368.3385 13.86780
368.8206 14.60999
369.3027 15.73938
369.7849 16.53271
370.2670 16.81030
370.7491 16.72839
371.2312 16.41132
371.7133 15.62421
372.1954 15.16797
372.6776 15.42352
373.1597 15.62885
373.6418 15.32458
374.1239 14.57227
374.6060 13.64624
375.0881 12.69525
375.5703 11.74640
376.0524 11.52014
376.5345 13.10632
377.0166 14.16016
377.4987 13.85352
377.9808 12.76654
378.4630 11.68475
378.9451 10.96777
379.4272 10.59711
379.9093 10.52777
380.3914 10.76392
380.8735 11.34888
381.3557 12.47546
381.8378 13.76794
382.3199 15.21045
382.8020 16.65796
383.2841 17.56445
383.7662 16.99432
384.2484 14.47803
384.7305 13.76562
385.2126 16.71344
385.6947 19.75067
386.1768 21.62805
386.6589 22.74530
387.1411 24.11249
387.6232 26.39844
388.1053 29.29443
388.5874 31.73969
389.0695 33.88251
389.5516 35.21594
390.0338 35.08423
390.5159 34.52161
390.9980 34.26617
391.4801 34.54218
391.9622 35.60297
392.4443 38.36841
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393.4086 46.23926
393.8907 45.47485
394.3728 44.23511
394.8549 44.55872
395.3370 46.15906
395.8192 47.60779
396.3013 47.99506
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397.2655 46.93195
397.7476 46.22571
398.2297 45.26379
398.7119 43.64893
399.1940 41.82159
399.6761 40.43823
400.1582 39.87274
400.6403 39.31415
401.1224 37.81342
401.6046 35.41705
402.0867 33.11060
402.5688 31.07922
403.0509 29.39685
403.5330 28.18640
404.0151 27.45404
404.4973 26.71747
404.9794 25.87708
405.4615 24.86493
405.9436 23.55890
406.4257 21.95062
406.9078 20.07404
407.3900 17.91644
407.8721 15.50122
408.3542 12.96472
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410.2827 5.208252
410.7648 4.883301
411.2469 4.078674
411.7290 2.973083
412.2111 1.908447
412.6932 0.7130130
413.1754 5.1879998E-02
413.6575 0.2577510
414.1396 0.7498780
414.6217 0.3240970
415.1038 1.143066
415.5859 2.765442
416.0681 3.675232
416.5502 3.808777
417.0323 3.848877
417.5144 3.383911
417.9965 3.266418
418.4786 4.159424
418.9608 5.618591
419.4429 6.795715
419.9250 7.250610
420.4071 7.166382
420.8892 7.039185
421.3713 6.823853
421.8535 6.627563
422.3356 6.387695
422.8177 6.206238
423.2998 6.104187
423.7819 6.117371
424.2640 6.394653
424.7462 7.291931
425.2283 8.939209
425.7104 9.288696
426.1925 6.592102
426.6746 4.455383
427.1567 4.379639
427.6389 5.423157
428.1210 6.128418
428.6031 5.811157
429.0852 4.761597
429.5673 3.483337
430.0494 1.887329
430.5316 0.3682860
431.0137 0.8204960
431.4958 2.009094
431.9779 3.433472
432.4600 5.099915
432.9421 6.788696
433.4243 8.357300
433.9064 9.815918
434.3885 11.11743
434.8706 12.03571
435.3527 13.34155
435.8348 15.98022
436.3170 19.27161
436.7991 22.06946
437.2812 23.73364
437.7633 25.30829
438.2454 28.02191
438.7275 31.67444
439.2097 34.69971
439.6918 36.26233
440.1739 37.38367
440.6560 39.72748
441.1381 43.38000
441.6202 46.79303
442.1024 49.25708
442.5845 51.40741
443.0666 54.00177
443.5487 57.09186
444.0308 60.13391
444.5129 62.66791
444.9951 64.76898
445.4772 67.29004
445.9593 70.61633
446.4414 73.83130
446.9235 76.55432
447.4056 79.02435
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