#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-04-26 14:01:13 +0300 (Thu, 26 Apr 2018) $
#$Revision: 604 $
#$URL: svn://172.16.1.111/rod/cif/1/00/01/1000143.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000143
loop_
_publ_author_name
'Orlandi, P.'
'Demartin, F.'
'Pasero, M.'
'Leverett, P.'
'Williams, P. A.'
'Hibbs, D. E.'
_publ_section_title
;
 Gelosaite, BiMo6+(2-5x)Mo5+6xO7(OH)*H2O (0<=x<=0.4), a new mineral from
 Su Senargiu (CA), Sardinia, Italy, and a second occurrence from
 Kingsgate, New England, Australia
;
_journal_name_full               'American Mineralogist'
_journal_page_first              268
_journal_page_last               273
_journal_paper_doi               10.2138/am.2011.3597
_journal_volume                  96
_journal_year                    2011
_chemical_compound_source        'Su Senargiu, Sardinia, Italy'
_chemical_formula_sum            'Bi H3 Mo2.102 O9'
_chemical_name_mineral           Gelosaite
_space_group_IT_number           14
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_cell_angle_alpha                90
_cell_angle_beta                 100.42
_cell_angle_gamma                90
_cell_length_a                   5.8505
_cell_length_b                   9.0421
_cell_length_c                   13.9173
_cell_volume                     724.095
_exptl_crystal_density_diffrn    5.115
_cod_original_formula_sum        'Bi Mo2.102 O9 H3'
_cod_database_code               9015598
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type helium-neon
_raman_measurement_device.excitation_laser_wavelength 780
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 12
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R120031.rod
_rod_data_source.block           3500000
_rod_database.code               1000143
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9015598 COD http://www.crystallography.net/cod/9015598.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
92.56775 0.0000000E+00
93.04987 17.17871
93.53198 57.03210
94.01410 90.04980
94.49622 113.0217
94.97833 129.7305
95.46045 143.7352
95.94257 154.9434
96.42468 165.1552
96.90680 177.8367
97.38892 187.4156
97.87103 192.9105
98.35315 192.9475
98.83527 187.0912
99.31738 178.2972
99.79950 165.0804
100.2816 149.7856
100.7637 130.1050
101.2458 108.9480
101.7280 88.78381
102.2101 69.99854
102.6922 53.15173
103.1743 39.40320
103.6564 30.35706
104.1385 26.13586
104.6207 23.92761
105.1028 24.49915
105.5849 28.76965
106.0670 33.33142
106.5491 33.62634
107.0313 31.37463
107.5134 28.77307
107.9955 26.45471
108.4776 24.89221
108.9597 24.16785
109.4418 23.73206
109.9240 24.09094
110.4061 24.39490
110.8882 23.99121
111.3703 22.66809
111.8524 20.68396
112.3345 18.64526
112.8167 17.06732
113.2988 14.37439
113.7809 9.150574
114.2630 2.951904
114.7451 2.270447
115.2272 5.181030
115.7094 5.948547
116.1915 6.955505
116.6736 8.384888
117.1557 9.883118
117.6378 12.09692
118.1199 14.53870
118.6021 15.67999
119.0842 14.15747
119.5663 9.621582
120.0484 4.435791
120.5305 2.076355
121.0126 8.817261
121.4948 15.01990
121.9769 20.65021
122.4590 25.45789
122.9411 28.67218
123.4232 30.68762
123.9053 32.57410
124.3875 34.62103
124.8696 36.79340
125.3517 38.98126
125.8338 41.12085
126.3159 43.36157
126.7980 45.97559
127.2802 48.99359
127.7623 51.92712
128.2444 54.33832
128.7265 56.25824
129.2086 58.04431
129.6907 58.98602
130.1729 60.87354
130.6550 64.37201
131.1371 69.45386
131.6192 75.50629
132.1013 81.51257
132.5834 86.54047
133.0656 92.93188
133.5477 101.1227
134.0298 110.5626
134.5119 121.3629
134.9940 133.8575
135.4761 148.1442
135.9583 164.2120
136.4404 184.7981
136.9225 203.9165
137.4046 220.9688
137.8867 236.4281
138.3688 251.0402
138.8510 265.2754
139.3331 278.3572
139.8152 287.2443
140.2973 292.0042
140.7794 293.8322
141.2615 292.4877
141.7437 288.3523
142.2258 283.0261
142.7079 277.2936
143.1900 270.8669
143.6721 263.1554
144.1542 253.2087
144.6364 243.0760
145.1185 234.9182
145.6006 229.0202
146.0827 223.4041
146.5648 216.3361
147.0469 209.2003
147.5291 203.6284
148.0112 200.5820
148.4933 199.0318
148.9754 196.7180
149.4575 193.4285
149.9396 189.6096
150.4218 186.0959
150.9039 182.3837
151.3860 178.9370
151.8681 176.2212
152.3502 173.9335
152.8323 169.8615
153.3145 161.9495
153.7966 154.0325
154.2787 147.0781
154.7608 140.6649
155.2429 133.6926
155.7250 125.1059
156.2072 114.7151
156.6893 105.8652
157.1714 98.83240
157.6535 92.65454
158.1356 87.29266
158.6177 82.53241
159.0999 77.79724
159.5820 72.62207
160.0641 66.92706
160.5462 60.67499
161.0283 53.34314
161.5104 45.86676
161.9926 38.69116
162.4747 31.91235
162.9568 25.95282
163.4389 21.83691
163.9210 19.43958
164.4031 16.42889
164.8853 11.72015
165.3674 6.392212
165.8495 2.156799
166.3316 0.6134030
166.8137 2.668274
167.2958 4.644897
167.7780 6.536682
168.2601 8.237976
168.7422 9.819031
169.2243 11.20782
169.7064 12.07440
170.1885 12.45612
170.6707 12.09796
171.1528 10.79456
171.6349 8.711914
172.1170 6.491211
172.5991 4.555481
173.0812 2.775940
173.5634 1.676636
174.0455 2.693970
174.5276 3.322876
175.0097 2.154419
175.4918 0.5756840
175.9739 3.549072
176.4561 5.512451
176.9382 6.572998
177.4203 7.146606
177.9024 6.758301
178.3845 6.477661
178.8666 6.826477
179.3488 7.693237
179.8309 8.202881
180.3130 7.051819
180.7951 2.942322
181.2772 7.1167000E-02
181.7593 1.077942
182.2415 1.478333
182.7236 1.849243
183.2057 2.352539
183.6878 2.618713
184.1699 2.042297
184.6520 2.9663000E-02
185.1342 1.725464
185.6163 2.758911
186.0984 3.517517
186.5805 4.281433
187.0626 5.108643
187.5447 6.236267
188.0269 8.270264
188.5090 11.48462
188.9911 14.32343
189.4732 15.98596
189.9553 17.11700
190.4374 18.71179
190.9196 20.95801
191.4017 24.03735
191.8838 28.25793
192.3659 33.53137
192.8480 39.49939
193.3301 46.15497
193.8123 53.40295
194.2944 60.92975
194.7765 68.57507
195.2586 76.60529
195.7407 85.31091
196.2228 94.68195
196.7050 104.1270
197.1871 112.8735
197.6692 120.9968
198.1513 130.2528
198.6334 141.9862
199.1155 154.1803
199.5977 165.4370
200.0798 175.7128
200.5619 185.7543
201.0440 196.6627
201.5261 208.8403
202.0082 219.6030
202.4904 228.2695
202.9725 235.6552
203.4546 242.3427
203.9367 248.2912
204.4188 252.7958
204.9009 255.0824
205.3831 255.2470
205.8652 252.6417
206.3473 246.5196
206.8294 238.5145
207.3115 229.0907
207.7936 218.5530
208.2758 207.3091
208.7579 195.8385
209.2400 183.3869
209.7221 172.5508
210.2042 164.5093
210.6863 157.0009
211.1685 148.3242
211.6506 138.2077
212.1327 127.6893
212.6148 118.1821
213.0969 110.2695
213.5790 102.4686
214.0612 94.52216
214.5433 86.85248
215.0254 79.78345
215.5075 73.42517
215.9896 67.39355
216.4717 61.20587
216.9539 54.64325
217.4360 48.40991
217.9181 41.53424
218.4002 35.46222
218.8823 31.81409
219.3644 30.98212
219.8466 31.66608
220.3287 32.33325
220.8108 33.00677
221.2929 33.58118
221.7750 33.78534
222.2571 33.97589
222.7393 34.39996
223.2214 35.00012
223.7035 36.29169
224.1856 39.65417
224.6677 44.92560
225.1498 49.20361
225.6320 51.20245
226.1141 51.89886
226.5962 52.97083
227.0783 54.88721
227.5604 56.66864
228.0425 57.17969
228.5247 56.72577
229.0068 56.29938
229.4889 56.06458
229.9710 56.17920
230.4531 57.10956
230.9352 59.21881
231.4174 61.41547
231.8995 62.85187
232.3816 63.66455
232.8637 64.17175
233.3458 64.03516
233.8279 63.56512
234.3101 64.26074
234.7922 66.43402
235.2743 69.36841
235.7564 72.90100
236.2385 76.76276
236.7206 80.45624
237.2028 83.76111
237.6849 86.65698
238.1670 89.12335
238.6491 91.18958
239.1312 92.63269
239.6133 93.07715
240.0955 92.99176
240.5776 93.17145
241.0597 94.19348
241.5418 95.82550
242.0239 96.85248
242.5060 96.54333
242.9882 96.67566
243.4703 98.16797
243.9524 100.3077
244.4345 102.1047
244.9166 103.0135
245.3987 103.1167
245.8809 102.7578
246.3630 101.5164
246.8451 100.3271
247.3272 99.12543
247.8093 98.14154
248.2914 97.86450
248.7736 98.64178
249.2557 99.99768
249.7378 99.92877
250.2199 96.36102
250.7020 93.88855
251.1841 93.70966
251.6663 94.73590
252.1484 95.79413
252.6305 96.32782
253.1126 96.36993
253.5947 96.00024
254.0768 94.67841
254.5590 93.58710
255.0411 92.87585
255.5232 92.40021
256.0053 91.93481
256.4874 91.39093
256.9695 90.93201
257.4517 90.95624
257.9338 92.93042
258.4159 93.56543
258.8980 91.77966
259.3801 89.09662
259.8622 86.95044
260.3444 85.85205
260.8265 85.61035
261.3086 85.88257
261.7907 86.85992
262.2728 88.13562
262.7549 89.87079
263.2371 91.82086
263.7192 93.61633
264.2013 95.18616
264.6834 96.96204
265.1655 99.65753
265.6476 103.8807
266.1298 107.5623
266.6119 110.1413
267.0940 112.4716
267.5761 115.3674
268.0582 118.9938
268.5403 122.8874
269.0225 126.6599
269.5046 130.2838
269.9867 134.3065
270.4688 139.1373
270.9509 143.8960
271.4330 147.6516
271.9152 150.3178
272.3973 152.6561
272.8794 155.2712
273.3615 158.2583
273.8436 161.7859
274.3257 166.2354
274.8079 170.9445
275.2900 175.2013
275.7721 179.0071
276.2542 183.0146
276.7363 187.8052
277.2184 193.2787
277.7006 198.5562
278.1827 203.3371
278.6648 208.0251
279.1469 212.8314
279.6290 217.7587
280.1111 222.7989
280.5933 227.9561
281.0754 233.2187
281.5575 238.5732
282.0396 244.1748
282.5217 249.6480
283.0038 254.8813
283.4860 259.8792
283.9681 264.5410
284.4502 268.6247
284.9323 272.3718
285.4144 276.5178
285.8965 281.4740
286.3787 285.8765
286.8608 288.7078
287.3429 290.3127
287.8250 291.9214
288.3071 293.8047
288.7892 296.0472
289.2714 298.8379
289.7535 302.2330
290.2356 305.5740
290.7177 308.6789
291.1998 311.4991
291.6819 313.8214
292.1641 315.3452
292.6462 316.8517
293.1283 319.0549
293.6104 321.8885
294.0925 325.4777
294.5746 330.5453
295.0568 336.2836
295.5389 341.0101
296.0210 344.3603
296.5031 347.2021
296.9852 349.9096
297.4673 352.6420
297.9495 356.0103
298.4316 361.7166
298.9137 367.5880
299.3958 370.1445
299.8779 368.9192
300.3600 366.2552
300.8422 363.7450
301.3243 360.7993
301.8064 356.2921
302.2885 349.7973
302.7706 341.7400
303.2527 332.4030
303.7349 321.7064
304.2170 310.2872
304.6991 298.1701
305.1812 285.5810
305.6633 272.8669
306.1454 260.1166
306.6276 247.2149
307.1097 234.1037
307.5918 220.8054
308.0739 207.0589
308.5560 192.3425
309.0381 177.7181
309.5203 164.2349
310.0024 151.8669
310.4845 140.5692
310.9666 130.8478
311.4487 122.3636
311.9308 113.3820
312.4130 103.0278
312.8951 92.99744
313.3772 84.87744
313.8593 78.45917
314.3414 72.84564
314.8235 67.86285
315.3057 63.33148
315.7878 58.82159
316.2699 54.50171
316.7520 49.75421
317.2341 43.35712
317.7162 36.19727
318.1984 30.28485
318.6805 27.03955
319.1626 25.16711
319.6447 22.63098
320.1268 19.29730
320.6089 15.98578
321.0911 12.89954
321.5732 10.19574
322.0553 8.250793
322.5374 7.436646
323.0195 6.895447
323.5016 5.553955
323.9838 3.390198
324.4659 1.853394
324.9480 2.354187
325.4301 3.130493
325.9122 1.816711
326.3943 2.113403
326.8765 6.095520
327.3586 8.574402
327.8407 9.621826
328.3228 9.348755
328.8049 7.039551
329.2870 4.424194
329.7692 3.148621
330.2513 3.132935
330.7334 3.828979
331.2155 5.633728
331.6976 7.906860
332.1797 8.985718
332.6619 8.366943
333.1440 7.481323
333.6261 7.587097
334.1082 8.337952
334.5903 8.956360
335.0724 9.420837
335.5546 9.519226
336.0367 8.708557
336.5188 6.879456
337.0009 5.316406
337.4830 4.997375
337.9651 5.368835
338.4473 5.374329
338.9294 4.771057
339.4115 3.985352
339.8936 3.162781
340.3757 2.357971
340.8578 2.125671
341.3400 3.148621
341.8221 4.338867
342.3042 4.017395
342.7863 1.988403
343.2684 0.2903440
343.7505 2.189941
344.2327 3.810791
344.7148 5.379578
345.1969 6.933838
345.6790 8.469604
346.1611 9.908142
346.6432 11.27161
347.1254 12.83765
347.6075 14.69971
348.0896 16.79053
348.5717 19.18042
349.0538 21.90790
349.5359 24.29053
350.0181 25.55853
350.5002 26.03058
350.9823 27.20123
351.4644 29.55450
351.9465 32.27765
352.4286 35.08136
352.9108 37.87195
353.3929 40.13348
353.8750 41.30499
354.3571 42.09589
354.8392 44.38702
355.3214 48.90375
355.8035 53.05048
356.2856 55.56848
356.7677 57.14203
357.2498 58.89160
357.7319 61.10089
358.2141 63.76715
358.6962 67.10175
359.1783 71.28210
359.6604 75.00940
360.1425 78.12225
360.6246 80.74890
361.1068 83.05768
361.5889 85.06024
362.0710 86.39746
362.5531 86.50061
363.0352 85.43677
363.5173 85.78790
363.9995 88.50183
364.4816 91.54492
364.9637 94.26202
365.4458 96.55005
365.9279 98.25482
366.4100 99.26941
366.8922 99.70288
367.3743 99.87683
367.8564 100.1407
368.3385 99.67841
368.8206 97.75055
369.3027 95.30353
369.7849 93.51001
370.2670 92.68488
370.7491 92.19519
371.2312 91.18890
371.7133 89.55603
372.1954 87.66119
372.6776 85.63635
373.1597 83.27954
373.6418 80.17639
374.1239 76.53339
374.6060 73.01208
375.0881 70.03076
375.5703 67.62152
376.0524 66.30835
376.5345 68.33057
377.0166 68.88007
377.4987 65.90448
377.9808 61.02209
378.4630 56.49402
378.9451 53.36066
379.4272 51.26526
379.9093 49.46167
380.3914 48.59979
380.8735 46.88654
381.3557 43.41510
381.8378 39.74677
382.3199 37.03156
382.8020 35.41565
383.2841 34.31793
383.7662 33.16943
384.2484 31.83521
384.7305 29.92389
385.2126 26.89056
385.6947 24.06183
386.1768 21.90259
386.6589 20.46466
387.1411 19.63129
387.6232 19.34351
388.1053 19.26239
388.5874 18.26996
389.0695 15.39801
389.5516 13.24750
390.0338 12.74908
390.5159 13.14520
390.9980 13.86151
391.4801 14.65961
391.9622 15.22546
392.4443 15.08704
392.9265 14.15112
393.4086 13.57202
393.8907 13.80896
394.3728 14.33411
394.8549 15.13385
395.3370 15.91901
395.8192 15.94110
396.3013 14.08472
396.7834 11.19580
397.2655 10.10620
397.7476 11.34064
398.2297 13.03076
398.7119 13.99402
399.1940 14.75671
399.6761 16.28339
400.1582 19.34839
400.6403 22.46490
401.1224 23.54504
401.6046 22.68256
402.0867 22.73071
402.5688 24.96655
403.0509 28.04639
403.5330 30.30658
404.0151 31.73273
404.4973 33.18280
404.9794 35.36713
405.4615 37.72461
405.9436 39.21838
406.4257 39.67120
406.9078 39.68060
407.3900 39.52216
407.8721 39.28888
408.3542 39.40613
408.8363 40.35675
409.3184 41.26550
409.8005 41.44031
410.2827 41.07104
410.7648 40.83026
411.2469 41.03503
411.7290 41.49524
412.2111 41.72931
412.6932 41.45129
413.1754 41.66614
413.6575 43.09961
414.1396 44.80988
414.6217 45.69659
415.1038 45.61621
415.5859 45.32391
416.0681 45.51727
416.5502 46.21283
417.0323 47.34686
417.5144 49.67865
417.9965 51.58826
418.4786 52.02264
418.9608 51.59393
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