#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-04-26 14:01:29 +0300 (Thu, 26 Apr 2018) $
#$Revision: 608 $
#$URL: svn://172.16.1.111/rod/cif/1/00/01/1000147.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000147
loop_
_publ_author_name
'Sokolova, E.'
'Camara, F.'
_publ_section_title
;
 From structure topology to chemical composition. III. Titanium silicates:
 The crystal chemistry of barytolamprophyllite Locality: Mt. Yuksporr,
 Khibina alkaline massif, Kola Peninsula, Russia
;
_journal_name_full               'The Canadian Mineralogist'
_journal_page_first              403
_journal_page_last               412
_journal_paper_doi               10.3749/canmin.46.2.403
_journal_volume                  46
_journal_year                    2008
_chemical_compound_source        R120087
_chemical_formula_sum
'Al0.03 Ba0.88 Ca0.13 Fe0.35 K0.61 Mg0.05 Mn0.28 Na2.09 Nb0.01 O18 Si4 Sr0.33 Ti2.91'
_chemical_name_mineral           Barytolamprophyllite
_space_group_IT_number           12
_symmetry_space_group_name_Hall  '-C 2y'
_symmetry_space_group_name_H-M   'C 1 2/m 1'
_cell_angle_alpha                90
_cell_angle_beta                 96.676
_cell_angle_gamma                90
_cell_length_a                   19.8971
_cell_length_b                   7.1165
_cell_length_c                   5.4108
_cell_volume                     760.962
_exptl_crystal_density_diffrn    3.511
_cod_original_formula_sum
;Al0.03 Ba0.88 Ca0.13 Fe0.35 K0.61 Mg0.05 Mn0.28 Na2.09 Nb0.01 O18 Si4 Sr0.33
 Ti2.91
;
_cod_database_code               9010662
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type helium-neon
_raman_measurement_device.excitation_laser_wavelength 780
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 12
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R120087.rod
_rod_data_source.block           3500000
_rod_database.code               1000147
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9010662 COD http://www.crystallography.net/cod/9010662.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
134.9940 0.0000000E+00
135.4761 0.2596890
135.9583 7.6309003E-02
136.4404 0.3159480
136.9225 0.2125550
137.4046 6.3735999E-02
137.8867 0.2832640
138.3688 0.1007540
138.8510 0.7002870
139.3331 1.889969
139.8152 2.691116
140.2973 2.690598
140.7794 2.942398
141.2615 4.101089
141.7437 5.992996
142.2258 7.753571
142.7079 8.700455
143.1900 9.318893
143.6721 10.65495
144.1542 13.07205
144.6364 15.81610
145.1185 18.10249
145.6006 19.83495
146.0827 21.68257
146.5648 24.17833
147.0469 26.96669
147.5291 29.71313
148.0112 32.26057
148.4933 34.72012
148.9754 37.39128
149.4575 40.41530
149.9396 43.33841
150.4218 45.84027
150.9039 48.20576
151.3860 50.77641
151.8681 53.73911
152.3502 57.11012
152.8323 60.84116
153.3145 65.60611
153.7966 70.11160
154.2787 73.90588
154.7608 77.25046
155.2429 80.69673
155.7250 84.70148
156.2072 89.29361
156.6893 93.93338
157.1714 98.20001
157.6535 103.0435
158.1356 109.4409
158.6177 117.0083
159.0999 124.4716
159.5820 130.7040
160.0641 134.8238
160.5462 140.2299
161.0283 147.3108
161.5104 154.4212
161.9926 161.4652
162.4747 167.9671
162.9568 173.8792
163.4389 179.5374
163.9210 184.6858
164.4031 188.0170
164.8853 189.2343
165.3674 188.6958
165.8495 186.7797
166.3316 183.5180
166.8137 179.0048
167.2958 173.3986
167.7780 166.7825
168.2601 158.9146
168.7422 149.1393
169.2243 137.8717
169.7064 126.9247
170.1885 116.5150
170.6707 106.4888
171.1528 96.47537
171.6349 86.59897
172.1170 77.28886
172.5991 68.83064
173.0812 61.22543
173.5634 54.43483
174.0455 49.01242
174.5276 43.99734
175.0097 39.01041
175.4918 34.05060
175.9739 29.36879
176.4561 25.27393
176.9382 21.80176
177.4203 18.74098
177.9024 16.09702
178.3845 13.80263
178.8666 11.94427
179.3488 10.48430
179.8309 9.214371
180.3130 7.859497
180.7951 6.249878
181.2772 4.983307
181.7593 4.360229
182.2415 3.843170
182.7236 2.930939
183.2057 1.541733
183.6878 0.1138920
184.1699 0.6603240
184.6520 0.2689060
185.1342 0.1931150
185.6163 0.8932190
186.0984 1.734009
186.5805 1.929825
187.0626 1.218826
187.5447 0.1722110
188.0269 0.1719670
188.5090 0.4000240
188.9911 0.6872100
189.4732 0.1607360
189.9553 0.7812810
190.4374 1.377655
190.9196 1.301788
191.4017 1.071777
191.8838 1.457565
192.3659 2.451569
192.8480 3.792130
193.3301 5.204239
193.8123 6.637619
194.2944 7.871063
194.7765 8.636566
195.2586 9.446030
195.7407 10.86026
196.2228 12.89442
196.7050 15.01187
197.1871 16.77907
197.6692 18.21754
198.1513 19.82263
198.6334 21.81934
199.1155 23.91599
199.5977 25.89499
200.0798 27.75972
200.5619 29.67027
201.0440 31.72476
201.5261 33.90599
202.0082 36.41095
202.4904 39.44531
202.9725 42.75722
203.4546 46.20522
203.9367 49.78090
204.4188 53.63651
204.9009 58.13293
205.3831 63.71706
205.8652 68.54941
206.3473 71.89700
206.8294 74.95248
207.3115 78.22311
207.7936 81.89249
208.2758 86.03894
208.7579 90.79675
209.2400 96.86757
209.7221 101.7505
210.2042 105.4120
210.6863 108.2087
211.1685 110.0961
211.6506 111.1253
212.1327 111.7179
212.6148 112.6848
213.0969 114.5254
213.5790 115.9907
214.0612 116.9999
214.5433 117.6168
215.0254 117.8953
215.5075 117.8397
215.9896 117.4589
216.4717 116.8107
216.9539 115.8627
217.4360 114.6166
217.9181 113.0614
218.4002 111.2113
218.8823 108.9937
219.3644 106.3957
219.8466 103.6406
220.3287 101.0714
220.8108 98.75690
221.2929 96.17026
221.7750 93.04178
222.2571 89.68181
222.7393 86.47046
223.2214 83.49976
223.7035 80.63245
224.1856 77.75378
224.6677 74.87447
225.1498 71.93228
225.6320 68.70264
226.1141 65.45181
226.5962 62.68036
227.0783 60.56485
227.5604 58.64641
228.0425 56.46210
228.5247 54.07942
229.0068 51.67383
229.4889 49.26723
229.9710 46.90578
230.4531 44.63412
230.9352 42.38072
231.4174 40.41995
231.8995 39.17209
232.3816 38.39769
232.8637 37.44409
233.3458 35.79811
233.8279 33.70929
234.3101 31.92226
234.7922 30.37625
235.2743 29.34612
235.7564 29.17314
236.2385 29.54414
236.7206 29.83882
237.2028 29.69136
237.6849 29.18460
238.1670 28.67119
238.6491 28.15596
239.1312 27.60934
239.6133 26.91525
240.0955 26.20219
240.5776 25.68158
241.0597 25.50121
241.5418 25.56696
242.0239 25.54652
242.5060 25.52132
242.9882 25.44679
243.4703 25.26790
243.9524 24.98546
244.4345 24.66695
244.9166 24.39680
245.3987 24.16669
245.8809 23.77112
246.3630 22.88370
246.8451 22.13968
247.3272 21.96707
247.8093 22.00621
248.2914 21.68004
248.7736 20.63528
249.2557 19.09370
249.7378 18.02380
250.2199 17.97778
250.7020 17.77687
251.1841 17.29573
251.6663 16.56198
252.1484 15.57893
252.6305 14.33730
253.1126 12.92227
253.5947 11.58420
254.0768 10.23308
254.5590 9.087143
255.0411 8.340195
255.5232 7.732544
256.0053 6.970825
256.4874 5.932770
256.9695 4.713684
257.4517 3.544891
257.9338 2.348755
258.4159 1.309875
258.8980 0.6149140
259.3801 5.0960002E-03
259.8622 0.8688660
260.3444 2.082672
260.8265 3.466019
261.3086 4.678116
261.7907 5.627975
262.2728 6.538025
262.7549 7.621109
263.2371 8.568756
263.7192 8.959976
264.2013 8.700607
264.6834 8.221359
265.1655 8.191360
265.6476 8.965469
266.1298 9.309006
266.6119 8.821411
267.0940 8.098160
267.5761 7.831192
268.0582 8.126663
268.5403 8.321426
269.0225 7.497360
269.5046 5.256546
269.9867 3.908569
270.4688 4.330750
270.9509 5.156128
271.4330 5.311569
271.9152 4.655075
272.3973 3.448929
272.8794 1.816055
273.3615 0.2885590
273.8436 2.139923
274.3257 3.558792
274.8079 4.851288
275.2900 6.156296
275.7721 7.507690
276.2542 9.039413
276.7363 10.95664
277.2184 13.17940
277.7006 15.12376
278.1827 16.47046
278.6648 17.77216
279.1469 19.35820
279.6290 21.22200
280.1111 23.34872
280.5933 25.97606
281.0754 28.75969
281.5575 30.65739
282.0396 30.93994
282.5217 31.22603
283.0038 32.49971
283.4860 34.65030
283.9681 37.14412
284.4502 39.86932
284.9323 42.69943
285.4144 45.35185
285.8965 47.73196
286.3787 50.16782
286.8608 52.94743
287.3429 55.95010
287.8250 58.73099
288.3071 60.98613
288.7892 63.17868
289.2714 66.08218
289.7535 69.78177
290.2356 73.32605
290.7177 76.00528
291.1998 78.18344
291.6819 80.95102
292.1641 84.75391
292.6462 88.80359
293.1283 92.07599
293.6104 94.67270
294.0925 97.63260
294.5746 101.6965
295.0568 106.3349
295.5389 110.3408
296.0210 113.3182
296.5031 116.4246
296.9852 121.0836
297.4673 126.7538
297.9495 132.0112
298.4316 136.0838
298.9137 139.5803
299.3958 143.3419
299.8779 147.4010
300.3600 151.6761
300.8422 156.1280
301.3243 160.7598
301.8064 165.5474
302.2885 170.6438
302.7706 175.8095
303.2527 180.6156
303.7349 185.0252
304.2170 189.9326
304.6991 196.2502
305.1812 203.0891
305.6633 209.2411
306.1454 214.4557
306.6276 219.1829
307.1097 223.6138
307.5918 227.7676
308.0739 232.2114
308.5560 237.3453
309.0381 242.6025
309.5203 247.3262
310.0024 251.4892
310.4845 255.4417
310.9666 259.6702
311.4487 263.9770
311.9308 267.2063
312.4130 268.5897
312.8951 269.5696
313.3772 271.7133
313.8593 274.8105
314.3414 277.3694
314.8235 278.5005
315.3057 278.5499
315.7878 278.5217
316.2699 278.7233
316.7520 278.2479
317.2341 276.2271
317.7162 273.0537
318.1984 269.4359
318.6805 265.8110
319.1626 261.8172
319.6447 256.6331
320.1268 250.0075
320.6089 243.4915
321.0911 238.7577
321.5732 234.4655
322.0553 228.6089
322.5374 220.2252
323.0195 211.0433
323.5016 202.7210
323.9838 195.2425
324.4659 188.3015
324.9480 182.2594
325.4301 176.3580
325.9122 169.6441
326.3943 161.8687
326.8765 154.1586
327.3586 147.2796
327.8407 141.1025
328.3228 135.2677
328.8049 129.6555
329.2870 124.4821
329.7692 120.0622
330.2513 116.3726
330.7334 112.8259
331.2155 108.8133
331.6976 104.6943
332.1797 101.5976
332.6619 99.90033
333.1440 98.49875
333.6261 96.21408
334.1082 93.49042
334.5903 91.45819
335.0724 90.78479
335.5546 90.83524
336.0367 91.02539
336.5188 91.40814
337.0009 91.29843
337.4830 89.91464
337.9651 87.87613
338.4473 86.37302
338.9294 85.71237
339.4115 85.32660
339.8936 84.81018
340.3757 84.18106
340.8578 83.59467
341.3400 83.14035
341.8221 82.71817
342.3042 82.14310
342.7863 81.36737
343.2684 80.68881
343.7505 80.56653
344.2327 80.63855
344.7148 79.92905
345.1969 78.06763
345.6790 75.83130
346.1611 73.96436
346.6432 72.42346
347.1254 71.26859
347.6075 71.00711
348.0896 70.90454
348.5717 69.88867
349.0538 67.83069
349.5359 65.83481
350.0181 64.88388
350.5002 64.69168
350.9823 63.90195
351.4644 61.66779
351.9465 59.48508
352.4286 58.59039
352.9108 58.72638
353.3929 58.61661
353.8750 57.60162
354.3571 56.00146
354.8392 54.62079
355.3214 53.51099
355.8035 52.46613
356.2856 51.41211
356.7677 50.37903
357.2498 49.38800
357.7319 48.42673
358.2141 47.60947
358.6962 47.13748
359.1783 47.07373
359.6604 46.95261
360.1425 46.64722
360.6246 46.30746
361.1068 46.13510
361.5889 46.12634
362.0710 46.01328
362.5531 45.50043
363.0352 44.60623
363.5173 44.15771
363.9995 44.54752
364.4816 44.94687
364.9637 44.94614
365.4458 44.63770
365.9279 44.30582
366.4100 44.10776
366.8922 43.96292
367.3743 43.59814
367.8564 42.50797
368.3385 41.91779
368.8206 42.52673
369.3027 43.48541
369.7849 43.68649
370.2670 42.85071
370.7491 41.72098
371.2312 41.34665
371.7133 42.07675
372.1954 42.55630
372.6776 42.15674
373.1597 42.04254
373.6418 43.20685
374.1239 45.43039
374.6060 47.57501
375.0881 48.65491
375.5703 48.72873
376.0524 49.94339
376.5345 53.70428
377.0166 56.98404
377.4987 58.66263
377.9808 59.55859
378.4630 60.89200
378.9451 63.22629
379.4272 66.23947
379.9093 69.14496
380.3914 71.61072
380.8735 74.65479
381.3557 78.53723
381.8378 82.83978
382.3199 87.43906
382.8020 92.19235
383.2841 96.71504
383.7662 100.3784
384.2484 102.8983
384.7305 106.4499
385.2126 112.2757
385.6947 117.9562
386.1768 122.7590
386.6589 126.8282
387.1411 130.5906
387.6232 134.3052
388.1053 137.8927
388.5874 141.0642
389.0695 143.6521
389.5516 146.0383
390.0338 148.6187
390.5159 150.8892
390.9980 152.3816
391.4801 152.9779
391.9622 152.9291
392.4443 152.6044
392.9265 152.0465
393.4086 150.7753
393.8907 148.5352
394.3728 145.6841
394.8549 142.1406
395.3370 138.1136
395.8192 134.3290
396.3013 131.6584
396.7834 129.5691
397.2655 126.0690
397.7476 120.4748
398.2297 115.2668
398.7119 112.0500
399.1940 109.8976
399.6761 107.7128
400.1582 105.1506
400.6403 102.6352
401.1224 100.5463
401.6046 98.86186
402.0867 97.62888
402.5688 97.13641
403.0509 96.79715
403.5330 95.69701
404.0151 93.80136
404.4973 92.47208
404.9794 92.69254
405.4615 93.75768
405.9436 94.39911
406.4257 94.42160
406.9078 94.43701
407.3900 94.98895
407.8721 95.98395
408.3542 96.86636
408.8363 97.59477
409.3184 98.20663
409.8005 98.62909
410.2827 98.93390
410.7648 99.41422
411.2469 100.2612
411.7290 101.2350
412.2111 101.7451
412.6932 101.6197
413.1754 101.5436
413.6575 101.7745
414.1396 102.0345
414.6217 101.9221
415.1038 101.4095
415.5859 100.9644
416.0681 101.1218
416.5502 101.9852
417.0323 102.2434
417.5144 101.3146
417.9965 100.4884
418.4786 100.3893
418.9608 100.7672
419.4429 101.0995
419.9250 101.1213
420.4071 100.9016
420.8892 100.6365
421.3713 100.5094
421.8535 100.0363
422.3356 98.97742
422.8177 97.74927
423.2998 96.76263
423.7819 96.01181
424.2640 95.14629
424.7462 93.86694
425.2283 92.18509
425.7104 89.80148
426.1925 85.96056
426.6746 82.18185
427.1567 79.02119
427.6389 76.19516
428.1210 73.26849
428.6031 70.02217
429.0852 66.50481
429.5673 62.86014
430.0494 59.07823
430.5316 55.24284
431.0137 51.52153
431.4958 47.64732
431.9779 43.47964
432.4600 39.00706
432.9421 34.31842
433.4243 29.09122
433.9064 23.61591
434.3885 19.24428
434.8706 16.34879
435.3527 13.79803
435.8348 10.80710
436.3170 7.661011
436.7991 4.824722
437.2812 2.524582
437.7633 0.4223330
438.2454 1.938934
438.7275 4.468704
439.2097 6.408798
439.6918 7.332108
440.1739 7.773727
440.6560 8.581451
441.1381 9.817154
441.6202 10.75594
442.1024 11.01714
442.5845 10.96596
443.0666 11.02554
443.5487 11.22379
444.0308 11.32784
444.5129 11.18312
444.9951 10.79433
445.4772 10.22467
445.9593 9.576843
446.4414 8.655197
446.9235 7.217926
447.4056 5.434296
447.8878 3.594208
448.3699 1.853241
448.8520 0.3074190
449.3341 0.8952030
449.8162 1.461578
450.2983 2.535583
450.7805 4.409515
451.2626 6.445465
451.7447 8.454956
452.2268 10.36404
452.7089 12.08076
453.1910 13.51964
453.6732 14.72725
454.1553 15.92979
454.6374 17.19530
455.1195 18.30721
455.6016 19.22647
456.0837 20.02751
456.5659 20.71172
457.0480 21.27888
457.5301 21.82533
458.0122 22.56442
458.4943 23.49211
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