#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-04-26 14:02:33 +0300 (Thu, 26 Apr 2018) $
#$Revision: 624 $
#$URL: svn://172.16.1.111/rod/cif/1/00/01/1000161.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000161
loop_
_publ_author_name
'Cooper, M. A.'
'Hawthorne, F. C.'
_publ_section_title
;
 Boleite: Resolution of the formula, KPb26Ag9Cu24Cl62(OH)48
;
_journal_name_full               'The Canadian Mineralogist'
_journal_page_first              801
_journal_page_last               808
_journal_paper_doi               10.2113/gscanmin.38.4.801
_journal_volume                  38
_journal_year                    2000
_chemical_compound_source        R130099
_chemical_formula_sum            'Ag9 Cl62 Cu24 H48 K O48 Pb26'
_chemical_name_mineral           Boleite
_space_group_IT_number           221
_symmetry_space_group_name_Hall  '-P 4 2 3'
_symmetry_space_group_name_H-M   'P m -3 m'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_length_a                   15.288
_cell_length_b                   15.288
_cell_length_c                   15.288
_cell_volume                     3573.156
_exptl_crystal_density_diffrn    5.083
_cod_original_formula_sum        'K Pb26 Ag9 Cu24 Cl62 O48 H48'
_cod_database_code               9004592
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type helium-neon
_raman_measurement_device.excitation_laser_wavelength 780
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 12
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R130099.rod
_rod_data_source.block           3500000
_rod_database.code               1000161
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9004592 COD http://www.crystallography.net/cod/9004592.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
108.0737 0.0000000E+00
108.5558 0.4123080
109.0379 0.5895840
109.5200 0.6988370
110.0021 0.6066280
110.4842 0.2380910
110.9664 1.9501001E-02
111.4485 5.8136001E-02
111.9306 2.1400000E-04
112.4127 6.2583998E-02
112.8948 0.1194310
113.3769 0.2341920
113.8591 0.5307690
114.3412 1.180504
114.8233 1.684242
115.3054 1.999802
115.7875 2.188095
116.2696 2.297813
116.7517 2.316216
117.2339 2.317787
117.7160 2.537697
118.1981 3.040543
118.6802 3.631035
119.1623 4.366234
119.6444 5.121330
120.1266 5.556099
120.6087 5.357277
121.0908 4.776711
121.5729 4.362770
122.0550 4.163780
122.5371 3.993896
123.0193 3.731392
123.5014 3.368134
123.9835 3.013153
124.4656 2.717178
124.9477 2.500137
125.4298 2.385323
125.9120 2.391808
126.3941 2.517654
126.8762 2.785103
127.3583 3.392372
127.8404 3.743355
128.3225 3.549118
128.8047 3.054688
129.2868 2.585258
129.7689 2.347054
130.2510 2.323067
130.7331 2.266197
131.2152 1.952644
131.6974 1.820045
132.1795 2.114456
132.6616 2.707176
133.1437 3.286507
133.6258 3.572754
134.1079 3.506897
134.5901 3.509071
135.0722 3.518074
135.5543 3.622665
136.0364 3.941124
136.5185 4.458786
137.0006 4.997276
137.4828 5.349510
137.9649 5.432495
138.4470 5.704376
138.9291 6.402893
139.4112 7.244438
139.8933 7.858261
140.3755 8.137268
140.8576 8.403023
141.3397 9.018135
141.8218 9.940193
142.3039 10.82283
142.7860 11.39806
143.2681 11.83014
143.7503 12.46072
144.2324 13.25326
144.7145 14.18270
145.1966 15.16961
145.6787 16.12696
146.1608 17.04683
146.6430 18.20452
147.1251 19.64825
147.6072 20.68542
148.0893 20.84241
148.5714 20.76498
149.0535 20.72176
149.5357 20.80035
150.0178 21.07365
150.4999 21.75689
150.9820 23.30383
151.4641 24.28589
151.9462 24.17086
152.4284 23.76698
152.9105 23.72116
153.3926 24.27737
153.8747 25.19108
154.3568 25.83999
154.8389 26.03511
155.3211 26.14026
155.8032 26.11367
156.2853 26.03365
156.7674 26.00414
157.2495 26.08227
157.7316 26.23392
158.2138 26.29619
158.6959 26.46181
159.1780 26.34463
159.6601 25.76183
160.1422 24.82394
160.6243 23.76406
161.1065 22.73755
161.5886 21.68135
162.0707 20.38680
162.5528 18.49670
163.0349 16.72821
163.5170 15.67937
163.9991 15.26876
164.4813 14.70583
164.9634 13.38282
165.4455 11.58074
165.9276 10.14285
166.4097 8.989052
166.8918 8.033955
167.3740 7.254955
167.8561 6.703579
168.3382 6.091915
168.8203 5.109394
169.3024 4.004314
169.7845 3.085617
170.2667 2.515697
170.7488 2.175137
171.2309 1.789162
171.7130 1.310192
172.1951 0.8798600
172.6772 0.4869350
173.1594 0.1693530
173.6415 3.4139999E-03
174.1236 4.7657002E-02
174.6057 0.2743230
175.0878 0.3816870
175.5699 0.2136150
176.0521 9.8034002E-02
176.5342 0.2199940
177.0163 0.4518130
177.4984 0.5650750
177.9805 0.3761060
178.4626 0.1191060
178.9448 0.5429530
179.4269 0.9110150
179.9090 1.196033
180.3911 1.393646
180.8732 1.499294
181.3553 1.498337
181.8375 1.377098
182.3196 1.128201
182.8017 0.8067820
183.2838 0.2667240
183.7659 0.2026900
184.2480 0.4028930
184.7301 0.3657110
185.2123 0.3040580
185.6944 0.4160080
186.1765 0.7306900
186.6586 0.9958530
187.1407 1.128716
187.6228 1.272976
188.1050 1.590542
188.5871 2.088058
189.0692 2.545086
189.5513 2.717125
190.0334 2.613293
190.5155 2.556736
190.9977 2.565090
191.4798 2.644730
191.9619 2.847515
192.4440 3.209362
192.9261 3.541969
193.4082 3.582596
193.8904 3.423809
194.3725 3.345982
194.8546 3.487869
195.3367 3.757748
195.8188 3.962902
196.3009 4.051247
196.7831 4.163967
197.2652 4.448677
197.7473 4.840347
198.2294 5.175499
198.7115 5.317413
199.1936 5.321617
199.6758 5.419613
200.1579 5.621971
200.6400 5.922401
201.1221 6.404068
201.6042 6.979095
202.0863 7.429581
202.5685 7.536667
203.0506 7.326763
203.5327 7.264763
204.0148 7.429886
204.4969 7.683369
204.9790 8.029964
205.4612 8.427040
205.9433 8.790222
206.4254 9.039536
206.9075 9.166771
207.3896 9.309769
207.8717 9.468300
208.3539 9.647102
208.8360 9.848709
209.3181 10.07184
209.8002 10.32224
210.2823 10.62362
210.7644 10.99958
211.2466 11.21163
211.7287 11.00801
212.2108 10.88772
212.6929 11.13064
213.1750 11.66325
213.6571 12.20341
214.1393 12.49102
214.6214 12.48858
215.1035 12.47375
215.5856 12.44843
216.0677 12.41401
216.5498 12.35109
217.0320 12.27031
217.5141 12.21422
217.9962 12.23427
218.4783 12.34630
218.9604 12.37795
219.4425 12.15468
219.9247 11.99939
220.4068 12.16891
220.8889 12.64223
221.3710 13.15560
221.8531 13.49177
222.3352 13.63001
222.8174 13.73787
223.2995 13.82774
223.7816 13.87553
224.2637 13.85019
224.7458 13.75387
225.2279 13.63808
225.7100 13.52354
226.1922 13.42479
226.6743 13.40298
227.1564 13.57773
227.6385 13.75365
228.1206 13.70420
228.6027 13.41227
229.0849 13.15629
229.5670 13.20501
230.0491 13.44690
230.5312 13.56838
231.0133 13.44693
231.4954 13.22080
231.9776 13.06230
232.4597 12.99230
232.9418 12.90857
233.4239 12.66859
233.9060 12.37484
234.3881 12.21695
234.8703 12.35135
235.3524 12.54826
235.8345 12.42892
236.3166 11.87502
236.7987 11.39061
237.2808 11.37561
237.7630 11.54425
238.2451 11.59639
238.7272 11.44223
239.2093 11.13962
239.6914 10.73983
240.1735 10.19338
240.6557 9.754814
241.1378 9.632305
241.6199 9.621014
242.1020 9.513248
242.5841 9.223104
243.0662 8.845957
243.5484 8.538918
244.0305 8.312439
244.5126 8.143450
244.9947 8.079021
245.4768 8.033197
245.9589 7.938824
246.4410 7.773785
246.9232 7.553026
247.4053 7.275791
247.8874 6.878387
248.3695 6.577948
248.8516 6.511278
249.3337 6.486692
249.8159 6.346794
250.2980 6.047129
250.7801 5.679596
251.2622 5.393944
251.7443 5.230494
252.2264 5.058308
252.7086 4.883905
253.1907 4.691935
253.6728 4.444273
254.1549 4.139740
254.6370 3.839436
255.1191 3.651279
255.6013 3.672974
256.0834 3.593115
256.5655 3.261028
257.0476 2.945810
257.5297 2.874203
258.0118 3.061625
258.4940 3.305376
258.9761 3.318377
259.4582 2.961767
259.9403 2.722834
260.4224 2.635496
260.9045 2.604269
261.3867 2.620930
261.8688 2.658548
262.3509 2.635035
262.8330 2.435720
263.3151 1.965010
263.7972 1.678604
264.2794 1.741407
264.7615 1.812138
265.2436 1.655928
265.7257 1.299774
266.2078 0.9581910
266.6899 0.8487890
267.1721 1.016386
267.6542 1.145966
268.1363 1.173431
268.6184 1.229822
269.1005 1.429871
269.5826 1.734961
270.0648 1.990522
270.5469 2.068535
271.0290 1.972383
271.5111 1.882729
271.9932 1.863503
272.4753 1.790693
272.9575 1.521660
273.4396 1.143312
273.9217 0.8943880
274.4038 0.9515550
274.8859 1.285610
275.3680 1.538919
275.8501 1.715136
276.3322 1.831085
276.8144 1.902531
277.2965 1.919111
277.7786 1.839607
278.2607 1.625240
278.7428 1.324329
279.2249 1.140488
279.7071 1.157890
280.1892 1.165873
280.6713 1.081472
281.1534 0.9533880
281.6355 0.8793560
282.1176 0.9116780
282.5998 1.000914
283.0819 1.010424
283.5640 0.8905240
284.0461 0.8004670
284.5282 0.7924730
285.0103 0.8285180
285.4925 0.8535330
285.9746 0.8487260
286.4567 0.8306330
286.9388 0.8212470
287.4209 0.8098140
287.9030 0.8432620
288.3852 1.042679
288.8673 1.245707
289.3494 1.186216
289.8315 0.7926290
290.3136 0.3703990
290.7957 0.3348730
291.2779 0.7542920
291.7600 1.038488
292.2421 1.031219
292.7242 0.9191780
293.2063 0.9026390
293.6884 1.005096
294.1706 1.070723
294.6527 0.8866960
295.1348 0.4624790
295.6169 0.3600580
296.0990 0.9776120
296.5811 1.649879
297.0633 1.738745
297.5454 1.277004
298.0275 0.9375740
298.5096 1.298733
298.9917 2.201374
299.4738 2.587879
299.9560 2.077387
300.4381 1.409101
300.9202 0.9366380
301.4023 0.6536330
301.8844 0.5094700
302.3665 0.5050350
302.8487 0.6067300
303.3308 0.7058390
303.8129 0.8275260
304.2950 0.9092240
304.7771 0.8872280
305.2592 0.8013690
305.7414 0.7708930
306.2235 0.8649010
306.7056 0.9890460
307.1877 0.9261760
307.6698 0.6147630
308.1519 0.3906150
308.6341 0.4586160
309.1162 0.6648640
309.5983 0.7281860
310.0804 0.5598050
310.5625 0.3135990
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312.0089 0.2108970
312.4910 0.2466740
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314.4195 0.3082960
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315.3837 0.4342290
315.8658 0.4295690
316.3479 0.2098850
316.8300 1.4233000E-02
317.3121 3.4285001E-02
317.7943 0.1413400
318.2764 0.3115860
318.7585 0.3510780
319.2406 0.2697530
319.7227 0.1633000
320.2048 7.0355996E-02
320.6870 0.2302300
321.1691 0.1528780
321.6512 0.1038340
322.1333 0.3441770
322.6154 0.4901240
323.0975 0.5441110
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324.0618 0.3446880
324.5439 0.1884170
325.0260 0.1116850
325.5081 6.0265999E-02
325.9902 6.4181998E-02
326.4724 0.3196530
326.9545 0.5410080
327.4366 0.4292350
327.9187 7.0441999E-02
328.4008 0.5009350
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329.3651 1.031624
329.8472 0.9675830
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330.8114 0.2485600
331.2935 8.4908001E-02
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335.1505 0.1474210
335.6326 2.6121000E-02
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346.7213 2.9859999E-02
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383.8442 1.0059000E-02
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386.2548 3.6942001E-02
386.7369 6.4884000E-02
387.2190 0.1154750
387.7011 0.1427100
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388.6654 8.2728997E-02
389.1475 7.3870003E-02
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390.1117 0.1938720
390.5938 4.5357000E-02
391.0760 7.4514002E-02
391.5581 0.1105540
392.0402 9.7134002E-02
392.5223 5.5482998E-02
393.0044 2.6366999E-02
393.4865 1.7998001E-02
393.9687 0.2398660
394.4508 0.5846710
394.9329 0.7431560
395.4150 0.6680430
395.8971 0.5021380
396.3792 0.3483870
396.8614 0.2122650
397.3435 0.1031720
397.8256 2.0013999E-02
398.3077 8.4495999E-02
398.7898 1.4210000E-03
399.2719 0.1900750
399.7540 0.3652920
400.2361 0.4792460
400.7183 0.5081370
401.2004 0.3507920
401.6825 0.2109930
402.1646 0.5500680
402.6467 0.4238300
403.1288 8.1377000E-02
403.6110 0.2176230
404.0931 0.4074230
404.5752 0.5369680
405.0573 0.6723820
405.5394 0.8416940
406.0215 0.8532890
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406.9858 0.2466050
407.4679 0.1672760
407.9500 0.2512970
408.4321 0.3433150
408.9142 0.3470380
409.3964 0.2815270
409.8785 0.2349640
410.3606 0.2165050
410.8427 0.2072300
411.3248 0.1443860
411.8069 0.1222860
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412.7712 0.6759760
413.2533 1.052999
413.7354 1.114267
414.2175 0.7553770
414.6996 0.4995540
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415.6639 0.3285100
416.1460 0.4122160
416.6281 0.5743540
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