#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-04-26 14:02:37 +0300 (Thu, 26 Apr 2018) $
#$Revision: 625 $
#$URL: svn://172.16.1.111/rod/cif/1/00/01/1000162.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000162
loop_
_publ_author_name
'Kampf, A. R.'
'Housley, R. M.'
'Mills, S. J.'
'Marty, J.'
'Thorne, B.'
_publ_section_title
;
 Lead-tellurium oxysalts from Otto Mountain near Baker, California: I.
 Ottoite, Pb2TeO5, a new mineral with chains of tellurate octahedra
;
_journal_name_full               'American Mineralogist'
_journal_page_first              1329
_journal_page_last               1336
_journal_paper_doi               10.2138/am.2010.3510
_journal_volume                  95
_journal_year                    2010
_chemical_compound_source        'Otto Mountain, Baker, California, USA'
_chemical_formula_sum            'O5 Pb2 Te'
_chemical_name_mineral           Ottoite
_space_group_IT_number           15
_symmetry_space_group_name_Hall  '-I 2ya'
_symmetry_space_group_name_H-M   'I 1 2/a 1'
_cell_angle_alpha                90
_cell_angle_beta                 91.330
_cell_angle_gamma                90
_cell_length_a                   7.5353
_cell_length_b                   5.7142
_cell_length_c                   10.8981
_cell_volume                     469.126
_exptl_crystal_density_diffrn    8.807
_cod_original_formula_sum        'Pb2 Te O5'
_cod_database_code               9015570
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type helium-neon
_raman_measurement_device.excitation_laser_wavelength 780
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 12
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R130126.rod
_rod_data_source.block           3500000
_rod_database.code               1000162
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9015570 COD http://www.crystallography.net/cod/9015570.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
152.4284 0.0000000E+00
152.9105 0.5962830
153.3926 1.063492
153.8747 1.337830
154.3568 0.8592070
154.8389 0.2651820
155.3211 1.6083000E-02
155.8032 3.2607999E-02
156.2853 7.5820997E-02
156.7674 0.1128690
157.2495 2.0111000E-02
157.7316 0.1629180
158.2138 0.2586670
158.6959 0.2460330
159.1780 0.1895290
159.6601 0.1899870
160.1422 0.1715240
160.6243 3.4042001E-02
161.1065 0.5061340
161.5886 1.263840
162.0707 2.273651
162.5528 3.867020
163.0349 5.375336
163.5170 6.241608
163.9991 6.540558
164.4813 6.982315
164.9634 7.927872
165.4455 9.381042
165.9276 11.25677
166.4097 13.63860
166.8918 16.38025
167.3740 19.34021
167.8561 22.52423
168.3382 25.86880
168.8203 29.36798
169.3024 32.97781
169.7845 36.68753
170.2667 40.47433
170.7488 44.35129
171.2309 48.38702
171.7130 52.73509
172.1951 56.94720
172.6772 60.84677
173.1594 64.55722
173.6415 68.27618
174.1236 72.11206
174.6057 76.03992
175.0878 79.85742
175.5699 83.52954
176.0521 87.12067
176.5342 90.54922
177.0163 93.91396
177.4984 97.31851
177.9805 100.8303
178.4626 104.4555
178.9448 108.4236
179.4269 112.6239
179.9090 117.2700
180.3911 122.6512
180.8732 128.5799
181.3553 134.5408
181.8375 140.0729
182.3196 145.0885
182.8017 150.5392
183.2838 156.5182
183.7659 162.7302
184.2480 169.0270
184.7301 175.3985
185.2123 181.9190
185.6944 188.6368
186.1765 195.5835
186.6586 202.5141
187.1407 209.7169
187.6228 216.6514
188.1050 223.1882
188.5871 229.2405
189.0692 234.3123
189.5513 238.1891
190.0334 240.7107
190.5155 240.5107
190.9977 236.6425
191.4798 230.3312
191.9619 222.8825
192.4440 214.4540
192.9261 204.7309
193.4082 192.5320
193.8904 178.5537
194.3725 164.7600
194.8546 151.3910
195.3367 138.6196
195.8188 126.7334
196.3009 115.7839
196.7831 105.7390
197.2652 96.52881
197.7473 88.03600
198.2294 80.30267
198.7115 73.28955
199.1936 66.99623
199.6758 61.53317
200.1579 57.10983
200.6400 53.30409
201.1221 50.00058
201.6042 47.07205
202.0863 44.25986
202.5685 41.31458
203.0506 38.25894
203.5327 35.60698
204.0148 33.62558
204.4969 31.83124
204.9790 29.96945
205.4612 28.13802
205.9433 26.57887
206.4254 25.53635
206.9075 25.03424
207.3896 24.58284
207.8717 24.25243
208.3539 23.91055
208.8360 23.51765
209.3181 23.07826
209.8002 22.59445
210.2823 21.94868
210.7644 21.15274
211.2466 20.83862
211.7287 21.27219
212.2108 21.88997
212.6929 22.42632
213.1750 22.92865
213.6571 23.64081
214.1393 24.79390
214.6214 26.47800
215.1035 28.36324
215.5856 30.41132
216.0677 32.57027
216.5498 34.74178
217.0320 37.00441
217.5141 39.62875
217.9962 42.83310
218.4783 46.65247
218.9604 50.44379
219.4425 54.10555
219.9247 57.86057
220.4068 61.80435
220.8889 65.94258
221.3710 70.27917
221.8531 74.83444
222.3352 79.68661
222.8174 84.84198
223.2995 90.61339
223.7816 96.37813
224.2637 101.6343
224.7458 106.3785
225.2279 110.9173
225.7100 115.4171
226.1922 119.9039
226.6743 124.5909
227.1564 129.5902
227.6385 134.7370
228.1206 139.8345
228.6027 144.8666
229.0849 149.9222
229.5670 154.9981
230.0491 160.1263
230.5312 165.4216
231.0133 170.4020
231.4954 175.8206
231.9776 183.1050
232.4597 192.6231
232.9418 201.4032
233.4239 206.6481
233.9060 210.0891
234.3881 214.3234
234.8703 220.3652
235.3524 227.1663
235.8345 233.3958
236.3166 239.0263
236.7987 244.3289
237.2808 249.7051
237.7630 254.7722
238.2451 259.0987
238.7272 262.6203
239.2093 265.2425
239.6914 266.8314
240.1735 267.4226
240.6557 266.8202
241.1378 265.3933
241.6199 262.6316
242.1020 257.7103
242.5841 250.1899
243.0662 240.9397
243.5484 231.3944
244.0305 221.6886
244.5126 211.3159
244.9947 199.8211
245.4768 187.8603
245.9589 175.8331
246.4410 163.8263
246.9232 152.1310
247.4053 141.0553
247.8874 130.6751
248.3695 120.8614
248.8516 111.5647
249.3337 102.7750
249.8159 94.48448
250.2980 86.68092
250.7801 79.46240
251.2622 72.96146
251.7443 67.40723
252.2264 62.18362
252.7086 57.04630
253.1907 52.26546
253.6728 48.02548
254.1549 44.37830
254.6370 41.19856
255.1191 38.34464
255.6013 36.11089
256.0834 33.58102
256.5655 30.34167
257.0476 27.14224
257.5297 24.45953
258.0118 22.38452
258.4940 20.66876
258.9761 18.95306
259.4582 17.03455
259.9403 15.68484
260.4224 15.21745
260.9045 14.93729
261.3867 14.51448
261.8688 13.86205
262.3509 12.99944
262.8330 11.93321
263.3151 10.62260
263.7972 9.231491
264.2794 7.453613
264.7615 5.865372
265.2436 4.837204
265.7257 4.346649
266.2078 4.129288
266.6899 3.968430
267.1721 3.912048
267.6542 3.569016
268.1363 2.634476
268.6184 1.750381
269.1005 1.253891
269.5826 1.108871
270.0648 1.107040
270.5469 1.118546
271.0290 1.154541
271.5111 0.8212280
271.9932 0.2784580
272.4753 1.276505
272.9575 1.699677
273.4396 1.697128
273.9217 1.748260
274.4038 2.211731
274.8859 3.026489
275.3680 3.403503
275.8501 3.086075
276.3322 2.726425
276.8144 2.547943
277.2965 2.492615
277.7786 2.385345
278.2607 2.103760
278.7428 1.736115
279.2249 1.686249
279.7071 2.364349
280.1892 2.816345
280.6713 2.710831
281.1534 2.230286
281.6355 1.669907
282.1176 1.141785
282.5998 0.6484990
283.0819 0.2121580
283.5640 0.1618500
284.0461 0.5075530
284.5282 0.8418730
285.0103 1.150604
285.4925 1.359360
285.9746 1.422134
286.4567 1.518509
286.9388 1.982437
287.4209 2.879593
287.9030 3.866058
288.3852 4.883545
288.8673 5.963257
289.3494 7.153763
289.8315 8.469193
290.3136 9.830429
290.7957 11.13428
291.2779 12.35065
291.7600 13.72740
292.2421 15.31409
292.7242 17.05731
293.2063 18.87561
293.6884 20.76814
294.1706 22.84149
294.6527 25.22487
295.1348 27.94553
295.6169 30.75252
296.0990 33.23338
296.5811 36.09840
297.0633 40.16060
297.5454 45.33330
298.0275 50.56194
298.5096 55.07866
298.9917 58.98999
299.4738 63.19469
299.9560 68.10103
300.4381 72.88699
300.9202 76.81148
301.4023 80.11057
301.8844 83.89645
302.3665 88.73225
302.8487 94.53735
303.3308 101.0386
303.8129 109.1424
304.2950 116.4875
304.7771 121.3950
305.2592 124.6994
305.7414 128.5479
306.2235 133.7540
306.7056 139.8587
307.1877 146.0444
307.6698 152.3635
308.1519 158.5686
308.6341 164.4572
309.1162 170.1956
309.5983 175.9630
310.0804 181.7542
310.5625 187.7085
311.0446 194.0527
311.5268 200.8153
312.0089 207.4701
312.4910 213.7549
312.9731 219.9450
313.4552 226.5667
313.9373 233.7014
314.4195 240.6374
314.9016 246.5201
315.3837 251.4645
315.8658 257.0528
316.3479 264.5711
316.8300 271.9572
317.3121 277.5410
317.7943 281.3216
318.2764 284.0820
318.7585 286.3950
319.2406 287.9866
319.7227 288.2304
320.2048 287.0545
320.6870 284.6787
321.1691 281.2711
321.6512 276.7883
322.1333 270.9827
322.6154 263.7490
323.0975 255.1092
323.5797 245.2543
324.0618 233.8090
324.5439 222.1786
325.0260 210.8087
325.5081 199.5802
325.9902 188.0730
326.4724 176.0666
326.9545 164.0152
327.4366 152.5591
327.9187 141.6555
328.4008 131.3448
328.8829 121.6631
329.3651 112.5973
329.8472 104.0794
330.3293 96.09904
330.8114 88.77637
331.2935 82.28665
331.7756 76.72130
332.2578 71.27354
332.7399 65.97337
333.2220 60.76570
333.7041 55.27513
334.1862 49.68660
334.6683 45.02509
335.1505 42.26459
335.6326 41.09479
336.1147 39.11075
336.5968 35.58110
337.0789 32.08325
337.5610 29.19347
338.0432 26.80634
338.5253 24.74240
339.0074 22.97760
339.4895 21.38460
339.9716 19.58141
340.4537 17.30818
340.9359 15.32523
341.4180 13.92305
341.9001 12.82680
342.3822 11.66333
342.8643 10.32751
343.3464 9.025131
343.8286 8.058990
344.3107 7.569168
344.7928 7.056152
345.2749 6.635925
345.7570 6.113159
346.2391 5.234207
346.7213 4.040237
347.2034 2.867859
347.6855 2.032883
348.1676 1.551498
348.6497 1.104126
349.1318 0.5300290
349.6140 0.1420440
350.0961 0.2927700
350.5782 0.7462620
351.0603 0.9214320
351.5424 0.4445650
352.0245 0.4888760
352.5067 1.040131
352.9888 0.8623810
353.4709 0.7337040
353.9530 0.7627260
354.4351 0.8829800
354.9172 1.056686
355.3994 1.264511
355.8815 1.422501
356.3636 1.390305
356.8457 1.120621
357.3278 0.7283780
357.8099 0.1354370
358.2920 0.5081790
358.7741 1.089264
359.2563 1.607193
359.7384 2.131485
360.2205 2.724411
360.7026 3.380692
361.1847 4.163116
361.6668 5.291229
362.1490 6.308914
362.6311 6.887756
363.1132 7.259354
363.5953 7.865707
364.0774 8.987930
364.5595 10.51463
365.0417 11.98351
365.5238 13.50392
366.0059 14.78819
366.4880 15.61853
366.9701 16.29997
367.4522 17.09848
367.9344 18.10373
368.4165 19.28419
368.8986 20.65532
369.3807 22.38913
369.8628 23.82883
370.3449 24.67273
370.8271 25.47708
371.3092 26.56589
371.7913 27.91637
372.2734 29.30144
372.7555 30.48807
373.2376 31.48619
373.7198 32.67905
374.2019 34.28218
374.6840 35.82462
375.1661 37.07715
375.6482 38.19006
376.1303 39.42122
376.6125 40.94846
377.0946 42.55684
377.5767 43.76625
378.0588 44.49515
378.5409 45.04373
379.0230 45.51392
379.5052 45.82668
379.9873 45.88939
380.4694 45.68448
380.9515 45.31216
381.4336 44.92752
381.9157 44.52307
382.3979 43.78793
382.8800 42.64212
383.3621 41.16049
383.8442 39.33220
384.3263 37.23788
384.8084 35.10707
385.2906 33.06401
385.7727 31.09042
386.2548 29.11520
386.7369 27.12303
387.2190 25.20833
387.7011 23.42586
388.1833 21.75136
388.6654 20.18193
389.1475 18.79266
389.6296 17.37222
390.1117 15.57179
390.5938 13.47305
391.0760 11.77684
391.5581 10.73726
392.0402 10.19133
392.5223 9.982986
393.0044 10.14383
393.4865 10.19720
393.9687 9.958954
394.4508 9.498978
394.9329 8.819855
395.4150 7.878540
395.8971 7.112366
396.3792 6.986328
396.8614 7.451859
397.3435 7.751099
397.8256 7.609741
398.3077 7.503571
398.7898 7.687531
399.2719 8.159668
399.7540 8.932266
400.2361 10.07397
400.7183 11.41716
401.2004 12.44386
401.6825 12.93257
402.1646 13.54550
402.6467 14.38133
403.1288 15.40834
403.6110 16.75621
404.0931 18.40527
404.5752 19.86520
405.0573 20.48300
405.5394 19.98444
406.0215 20.01346
406.5037 20.76627
406.9858 21.78450
407.4679 22.91478
407.9500 24.13089
408.4321 25.44583
408.9142 26.87350
409.3964 28.37755
409.8785 29.78804
410.3606 31.08366
410.8427 32.31032
411.3248 33.34016
411.8069 34.39787
412.2891 35.77296
412.7712 37.50418
413.2533 39.28716
413.7354 40.65848
414.2175 41.44112
414.6996 42.51569
415.1818 44.27118
415.6639 45.99026
416.1460 47.53764
416.6281 48.81593
417.1102 49.67387
417.5923 50.02325
418.0745 49.88411
418.5566 49.30748
419.0387 48.24040
419.5208 46.86455
420.0029 45.34538
420.4850 43.48566
420.9672 41.04843
421.4493 37.99374
421.9314 34.72394
422.4135 31.38121
422.8956 27.96150
423.3777 25.20868
423.8599 23.66283
424.3420 22.26877
424.8241 20.05914
425.3062 17.25754
425.7883 14.69334
426.2704 12.71465
426.7526 11.20714
427.2347 10.12817
427.7168 9.468628
428.1989 8.703766
428.6810 7.399048
429.1631 5.917252
429.6453 5.037521
430.1274 4.962967
430.6095 5.082642
431.0916 5.171097
431.5737 5.181808
432.0558 5.054611
432.5380 4.768204
433.0201 4.455475
433.5022 4.231781
433.9843 4.092911
434.4664 4.187256
434.9485 4.760178
435.4307 5.372452
435.9128 5.726730
436.3949 5.850113
436.8770 5.909058
437.3591 5.993622
437.8412 6.115875
438.3234 6.307968
438.8055 6.663452
439.2876 6.947128
439.7697 6.959564
440.2518 7.013824
440.7339 7.476654
441.2160 8.375336
441.6982 9.391556
442.1803 10.19827
442.6624 10.82091
443.1445 11.09932
443.6266 10.39198
444.1087 9.988907
444.5909 10.63008
445.0730 11.78462
445.5551 12.54373
446.0372 12.41600
446.5193 11.76012
447.0014 11.35135
447.4836 11.24982
447.9657 11.21512
448.4478 11.24619
448.9299 11.30070
449.4120 11.36853
449.8941 11.44102
450.3763 11.48393
450.8584 11.56490
451.3405 11.61275
451.8226 11.25754
452.3047 10.32600
452.7868 9.414185
453.2690 8.965179
453.7511 8.735291
454.2332 8.380417
454.7153 7.788712
455.1974 7.139786
455.6795 6.616455
456.1617 6.173660
456.6438 5.551620
457.1259 4.585648
457.6080 3.611206
458.0901 3.201706
458.5722 3.361481
459.0544 3.196854
459.5365 2.135773
460.0186 0.9873500
460.5007 0.4631650
460.9828 0.5401920
461.4649 0.8507230
461.9471 1.212387
462.4292 1.593933
462.9113 1.863678
463.3934 2.204346
463.8755 2.207047
464.3576 1.499237
464.8398 0.6041110
465.3219 4.4464000E-02
465.8040 7.8139998E-02
466.2861 4.9026001E-02
466.7682 0.2649690
467.2503 0.6070560
467.7325 0.6642300
468.2146 0.1417240
468.6967 0.3578030
469.1788 0.6959380
469.6609 0.9040370
470.1430 1.044388
470.6252 1.145340
471.1073 1.179214
471.5894 1.060928
472.0715 0.7318730
472.5536 0.5068820
473.0357 0.5110020
473.5179 0.5649410
474.0000 0.5847020
474.4821 0.5654300
474.9642 0.5239110
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