#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-04-26 14:03:00 +0300 (Thu, 26 Apr 2018) $
#$Revision: 631 $
#$URL: svn://172.16.1.111/rod/cif/1/00/01/1000166.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000166
loop_
_publ_author_name
'Xu, K.'
'Xue, J.'
'Ding, Y.'
'Lu, G.'
_publ_section_title
;
 Discovery of stolzite in China and refinement of its crystal structure
;
_journal_name_full               'Acta Geologica Sinica'
_journal_page_first              111
_journal_page_last               116
_journal_paper_doi               10.1111/j.1755-6724.1995.mp8001009.x
_journal_volume                  8
_journal_year                    1995
_chemical_compound_source        'Yaogangxian, Hunan Province, China'
_chemical_formula_sum            'O4 Pb W'
_chemical_name_mineral           Stolzite
_space_group_IT_number           88
_symmetry_space_group_name_Hall  'I 4bw -1bw'
_symmetry_space_group_name_H-M   'I 41/a :1'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_length_a                   5.44505
_cell_length_b                   5.44503
_cell_length_c                   12.0495
_cell_volume                     357.249
_exptl_crystal_density_diffrn    8.460
_cod_original_sg_symbol_H-M      'I 41/a'
_cod_original_formula_sum        'Pb W O4'
_cod_database_code               9014025
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type helium-neon
_raman_measurement_device.excitation_laser_wavelength 780
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 12
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R130615.rod
_rod_data_source.block           3500000
_rod_database.code               1000166
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9014025 COD http://www.crystallography.net/cod/9014025.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
93.12805 0.0000000E+00
93.61017 0.9499210
94.09229 2.119415
94.57440 2.218536
95.05651 2.406921
95.53863 3.180756
96.02074 4.141693
96.50286 4.799103
96.98498 4.710968
97.46709 3.600845
97.94921 2.723160
98.43133 2.170410
98.91344 2.066620
99.39556 2.186234
99.87768 2.524353
100.3598 3.005020
100.8419 3.486511
101.3240 3.895035
101.8061 4.513611
102.2883 6.044144
102.7704 7.662354
103.2525 8.066788
103.7346 8.009567
104.2167 8.474136
104.6988 8.559448
105.1810 8.453873
105.6631 8.159866
106.1452 7.481766
106.6273 6.440979
107.1094 5.452591
107.5915 4.531281
108.0737 3.836945
108.5558 3.582642
109.0379 3.633286
109.5200 3.542648
110.0021 2.768509
110.4842 1.165176
110.9664 2.3848999E-02
111.4485 0.6629180
111.9306 0.9481510
112.4127 0.8419190
112.8948 0.4240880
113.3769 1.0544000E-02
113.8591 0.1087950
114.3412 1.259216
114.8233 1.855484
115.3054 1.613785
115.7875 0.9284520
116.2696 0.2978520
116.7517 0.1051480
117.2339 0.3847810
117.7160 0.6997530
118.1981 0.8860780
118.6802 1.184174
119.1623 1.806122
119.6444 2.648102
120.1266 3.377853
120.6087 3.837921
121.0908 4.089203
121.5729 4.250610
122.0550 4.243546
122.5371 4.197281
123.0193 4.341202
123.5014 4.656525
123.9835 4.845337
124.4656 4.605789
124.9477 4.303497
125.4298 4.299225
125.9120 4.778748
126.3941 5.537292
126.8762 6.109787
127.3583 6.404922
127.8404 6.651047
128.3225 7.016830
128.8047 7.370285
129.2868 7.507217
129.7689 7.261047
130.2510 6.669693
130.7331 6.296356
131.2152 6.389343
131.6974 6.472626
132.1795 6.417755
132.6616 6.254349
133.1437 6.088028
133.6258 6.028702
134.1079 6.121384
134.5901 6.018265
135.0722 5.474655
135.5543 4.966629
136.0364 4.890182
136.5185 5.233597
137.0006 5.544495
137.4828 5.228363
137.9649 4.095352
138.4470 3.350601
138.9291 3.338898
139.4112 3.641006
139.8933 3.801117
140.3755 3.726608
140.8576 3.481369
141.3397 3.016663
141.8218 2.345215
142.3039 1.878632
142.7860 1.860870
143.2681 2.201904
143.7503 2.593140
144.2324 3.014526
144.7145 3.412827
145.1966 3.729843
145.6787 3.964691
146.1608 4.213516
146.6430 4.564911
147.1251 5.028854
147.6072 5.516144
148.0893 5.816101
148.5714 6.281479
149.0535 7.016876
149.5357 8.095139
150.0178 9.642593
150.4999 12.13611
150.9820 17.63687
151.4641 21.41467
151.9462 22.12578
152.4284 21.88358
152.9105 22.26633
153.3926 23.87752
153.8747 26.35547
154.3568 28.80655
154.8389 31.29874
155.3211 33.66718
155.8032 35.73892
156.2853 37.73488
156.7674 39.93106
157.2495 42.47922
157.7316 45.27789
158.2138 47.89131
158.6959 49.99254
159.1780 52.32225
159.6601 55.16362
160.1422 58.38467
160.6243 61.67979
161.1065 64.86911
161.5886 67.97704
162.0707 71.02136
162.5528 73.83708
163.0349 76.74435
163.5170 79.75560
163.9991 82.90791
164.4813 86.56810
164.9634 91.26263
165.4455 96.59984
165.9276 101.6154
166.4097 105.9981
166.8918 110.2298
167.3740 114.8102
167.8561 119.7546
168.3382 124.8852
168.8203 130.1905
169.3024 135.5544
169.7845 140.9467
170.2667 146.4704
170.7488 151.9715
171.2309 157.0945
171.7130 161.9379
172.1951 165.9699
172.6772 169.4399
173.1594 172.2036
173.6415 174.0340
174.1236 174.8070
174.6057 174.4891
175.0878 172.9425
175.5699 169.6000
176.0521 165.4718
176.5342 160.6602
177.0163 155.3083
177.4984 149.6060
177.9805 143.6134
178.4626 137.3121
178.9448 131.2545
179.4269 125.0686
179.9090 119.4686
180.3911 114.6044
180.8732 110.5164
181.3553 107.2880
181.8375 105.0209
182.3196 103.7781
182.8017 103.0381
183.2838 102.8821
183.7659 103.0287
184.2480 103.2173
184.7301 103.5114
185.2123 104.2767
185.6944 105.8726
186.1765 108.4426
186.6586 111.2900
187.1407 114.8509
187.6228 118.3282
188.1050 121.2756
188.5871 123.5942
189.0692 125.1571
189.5513 125.7597
190.0334 125.4191
190.5155 124.6161
190.9977 123.6539
191.4798 122.0714
191.9619 119.2405
192.4440 114.9701
192.9261 109.9469
193.4082 104.6007
193.8904 99.01340
194.3725 93.32253
194.8546 87.31677
195.3367 81.17642
195.8188 75.25565
196.3009 69.52495
196.7831 64.21785
197.2652 59.54907
197.7473 55.37173
198.2294 51.47319
198.7115 47.51651
199.1936 43.61552
199.6758 40.50642
200.1579 38.65129
200.6400 37.07152
201.1221 35.11852
201.6042 32.94298
202.0863 30.97443
202.5685 29.54742
203.0506 28.64005
203.5327 27.90424
204.0148 27.63191
204.4969 27.21669
204.9790 26.31123
205.4612 25.09573
205.9433 24.00891
206.4254 23.40201
206.9075 23.27245
207.3896 22.82837
207.8717 21.69835
208.3539 20.67374
208.8360 19.97998
209.3181 19.60378
209.8002 19.44868
210.2823 19.47832
210.7644 19.73402
211.2466 19.78400
211.7287 19.47714
212.2108 19.13458
212.6929 18.81683
213.1750 18.55730
213.6571 18.40128
214.1393 18.37999
214.6214 18.48402
215.1035 18.85817
215.5856 20.06567
216.0677 20.99692
216.5498 20.83601
217.0320 19.75841
217.5141 18.72711
217.9962 18.66318
218.4783 19.72836
218.9604 20.35947
219.4425 20.22762
219.9247 19.99165
220.4068 20.09785
220.8889 20.53537
221.3710 20.95352
221.8531 21.03687
222.3352 20.75482
222.8174 20.55994
223.2995 20.47308
223.7816 20.45618
224.2637 20.53265
224.7458 20.69345
225.2279 20.76831
225.7100 20.54550
226.1922 20.08041
226.6743 19.84579
227.1564 20.14075
227.6385 20.50836
228.1206 20.42453
228.6027 19.84821
229.0849 19.33887
229.5670 19.48511
230.0491 20.00720
230.5312 20.12723
231.0133 19.41742
231.4954 18.41174
231.9776 17.69788
232.4597 17.30350
232.9418 17.00766
233.4239 16.72333
233.9060 16.44342
234.3881 16.15363
234.8703 15.81509
235.3524 15.49399
235.8345 15.33936
236.3166 15.42395
236.7987 15.39410
237.2808 15.15057
237.7630 14.66867
238.2451 13.84586
238.7272 12.55118
239.2093 11.04562
239.6914 9.725983
240.1735 8.614899
240.6557 7.624756
241.1378 6.757568
241.6199 5.973297
242.1020 5.276245
242.5841 4.696655
243.0662 4.110748
243.5484 3.247772
244.0305 1.940216
244.5126 0.8197020
244.9947 4.6569999E-02
245.4768 0.4814150
245.9589 0.7052920
246.4410 0.5746460
246.9232 0.4776310
247.4053 1.169098
247.8874 3.097656
248.3695 4.754578
248.8516 5.856384
249.3337 6.641174
249.8159 7.188446
250.2980 7.535889
250.7801 7.861115
251.2622 8.512665
251.7443 9.798615
252.2264 10.70746
252.7086 10.94397
253.1907 10.97440
253.6728 11.08597
254.1549 11.36539
254.6370 11.75244
255.1191 12.18668
255.6013 12.83063
256.0834 13.14722
256.5655 12.92261
257.0476 12.58389
257.5297 12.46179
258.0118 12.58810
258.4940 12.68759
258.9761 12.37408
259.4582 11.48242
259.9403 10.58578
260.4224 9.694183
260.9045 8.770355
261.3867 7.721130
261.8688 6.564575
262.3509 5.522827
262.8330 4.919586
263.3151 5.113861
263.7972 4.389008
264.2794 2.176605
264.7615 0.2926330
265.2436 2.325836
265.7257 3.892151
266.2078 5.388214
266.6899 7.211273
267.1721 9.419861
267.6542 11.58502
268.1363 13.77853
268.6184 15.88547
269.1005 17.70850
269.5826 19.33307
270.0648 21.08191
270.5469 23.26025
271.0290 25.86752
271.5111 28.20871
271.9932 29.87280
272.4753 31.72684
272.9575 34.18289
273.4396 37.15204
273.9217 40.30026
274.4038 43.42050
274.8859 46.49548
275.3680 49.36902
275.8501 51.81165
276.3322 54.41159
276.8144 57.48621
277.2965 60.86774
277.7786 64.16663
278.2607 67.17343
278.7428 69.95270
279.2249 72.80020
279.7071 75.62158
280.1892 78.60300
280.6713 81.95889
281.1534 85.49301
281.6355 88.86432
282.1176 91.92004
282.5998 94.74731
283.0819 97.40811
283.5640 99.57397
284.0461 102.2197
284.5282 105.9121
285.0103 110.1154
285.4925 114.0673
285.9746 117.5305
286.4567 120.6475
286.9388 123.6299
287.4209 126.3482
287.9030 129.3163
288.3852 132.7043
288.8673 136.3260
289.3494 139.8768
289.8315 143.2800
290.3136 146.7701
290.7957 150.7482
291.2779 155.2617
291.7600 159.7465
292.2421 164.2529
292.7242 168.6444
293.2063 172.5660
293.6884 176.0141
294.1706 179.7316
294.6527 184.4999
295.1348 190.3657
295.6169 196.1117
296.0990 201.1841
296.5811 206.4944
297.0633 212.8304
297.5454 220.1437
298.0275 227.8112
298.5096 235.2264
298.9917 242.6715
299.4738 251.4229
299.9560 262.0195
300.4381 273.3077
300.9202 284.3765
301.4023 295.4685
301.8844 307.9071
302.3665 322.5006
302.8487 339.0544
303.3308 356.6731
303.8129 375.2972
304.2950 395.0739
304.7771 415.9138
305.2592 437.8986
305.7414 461.3773
306.2235 486.6008
306.7056 513.2702
307.1877 540.3553
307.6698 567.2218
308.1519 596.3510
308.6341 628.6046
309.1162 663.5491
309.5983 699.8635
310.0804 736.8799
310.5625 776.1816
311.0446 819.5481
311.5268 866.7759
312.0089 917.8908
312.4910 973.3079
312.9731 1032.387
313.4552 1094.200
313.9373 1158.393
314.4195 1227.459
314.9016 1304.823
315.3837 1390.599
315.8658 1478.802
316.3479 1567.215
316.8300 1659.170
317.3121 1758.212
317.7943 1864.472
318.2764 1973.487
318.7585 2083.694
319.2406 2194.032
319.7227 2302.302
320.2048 2413.722
320.6870 2518.617
321.1691 2615.504
321.6512 2702.316
322.1333 2774.488
322.6154 2831.624
323.0975 2869.126
323.5797 2875.931
324.0618 2854.773
324.5439 2806.492
325.0260 2726.803
325.5081 2620.908
325.9902 2495.155
326.4724 2349.285
326.9545 2191.312
327.4366 2029.878
327.9187 1862.906
328.4008 1704.341
328.8829 1555.337
329.3651 1417.298
329.8472 1291.869
330.3293 1179.324
330.8114 1079.179
331.2935 991.0942
331.7756 916.4995
332.2578 851.4632
332.7399 798.8576
333.2220 753.9420
333.7041 713.3957
334.1862 677.3361
334.6683 646.6801
335.1505 622.6160
335.6326 604.9333
336.1147 590.5215
336.5968 579.6981
337.0789 571.1896
337.5610 564.7386
338.0432 560.1753
338.5253 557.2097
339.0074 555.7175
339.4895 555.7001
339.9716 557.3896
340.4537 561.0757
340.9359 565.5913
341.4180 571.0406
341.9001 577.0939
342.3822 583.3467
342.8643 589.6575
343.3464 596.0460
343.8286 602.4731
344.3107 608.7820
344.7928 615.7388
345.2749 624.2283
345.7570 632.6967
346.2391 639.8359
346.7213 645.5801
347.2034 650.9718
347.6855 656.9536
348.1676 663.6162
348.6497 668.9396
349.1318 672.3520
349.6140 675.2683
350.0961 677.9363
350.5782 680.5463
351.0603 683.8171
351.5424 688.4150
352.0245 693.4088
352.5067 694.6880
352.9888 689.6691
353.4709 684.2027
353.9530 679.4526
354.4351 674.4317
354.9172 668.1559
355.3994 660.2503
355.8815 650.5654
356.3636 638.6868
356.8457 623.6005
357.3278 608.0925
357.8099 591.4537
358.2920 574.9047
358.7741 559.3911
359.2563 544.8980
359.7384 530.9816
360.2205 517.1518
360.7026 503.4039
361.1847 489.7811
361.6668 475.8016
362.1490 462.3846
362.6311 450.1542
363.1132 438.6829
363.5953 427.3320
364.0774 415.6558
364.5595 403.8513
365.0417 392.7778
365.5238 382.6850
366.0059 373.0779
366.4880 363.7531
366.9701 354.9594
367.4522 347.0191
367.9344 340.0261
368.4165 333.5790
368.8986 327.0212
369.3807 320.1765
369.8628 313.7971
370.3449 308.3868
370.8271 302.9581
371.3092 296.7024
371.7913 289.8064
372.2734 283.0872
372.7555 277.3074
373.2376 272.4751
373.7198 267.9056
374.2019 263.9149
374.6840 259.7932
375.1661 255.0789
375.6482 250.1338
376.1303 245.6068
376.6125 241.8519
377.0946 238.5126
377.5767 234.7355
378.0588 230.3157
378.5409 226.0274
379.0230 222.4311
379.5052 218.8267
379.9873 214.4330
380.4694 209.1111
380.9515 203.9150
381.4336 200.1796
381.9157 197.8574
382.3979 195.0342
382.8800 191.1881
383.3621 187.0856
383.8442 183.3044
384.3263 179.7551
384.8084 175.9792
385.2906 171.6172
385.7727 166.9200
386.2548 162.4493
386.7369 158.2917
387.2190 154.1068
387.7011 149.7600
388.1833 145.2242
388.6654 140.3747
389.1475 135.0078
389.6296 129.6572
390.1117 125.0667
390.5938 121.0661
391.0760 116.2800
391.5581 109.5961
392.0402 102.7899
392.5223 98.69684
393.0044 97.54419
393.4865 95.69287
393.9687 91.11816
394.4508 85.16846
394.9329 80.00739
395.4150 75.92267
395.8971 72.27948
396.3792 68.52332
396.8614 64.68689
397.3435 61.07391
397.8256 57.87848
398.3077 54.69794
398.7898 51.06525
399.2719 47.16187
399.7540 43.67273
400.2361 40.98175
400.7183 38.85785
401.2004 36.72247
401.6825 34.65430
402.1646 32.43781
402.6467 29.89075
403.1288 27.23950
403.6110 24.87360
404.0931 22.86304
404.5752 20.72296
405.0573 17.78137
405.5394 13.73627
406.0215 10.60004
406.5037 8.710327
406.9858 7.295837
407.4679 6.203674
407.9500 5.270874
408.4321 4.215637
408.9142 2.829102
409.3964 1.197510
409.8785 0.3206180
410.3606 1.754456
410.8427 3.016724
411.3248 4.007568
411.8069 4.884155
412.2891 5.812134
412.7712 6.823547
413.2533 7.824341
413.7354 8.707520
414.2175 9.499878
414.6996 10.08600
415.1818 10.25287
415.6639 10.39191
416.1460 10.61334
416.6281 10.92688
417.1102 11.33698
417.5923 11.94879
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