#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-04-26 14:03:16 +0300 (Thu, 26 Apr 2018) $
#$Revision: 635 $
#$URL: svn://172.16.1.111/rod/cif/1/00/01/1000169.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000169
loop_
_publ_author_name
'Keller, P.'
'Lissner, F.'
'Schleid, T.'
_publ_section_title
;
 The crystal structure of arsendescloizite, PbZn(OH)[AsO4], from Tsumeb
 (Namibia) Locality: Tsumeb, Namibia
;
_journal_name_full               'Neues Jahrbuch fur Mineralogie, Monatshefte'
_journal_page_first              374
_journal_page_last               384
_journal_volume                  2003
_journal_year                    2003
_chemical_compound_source        R140430
_chemical_formula_sum            'As H O5 Pb Zn'
_chemical_name_mineral           Arsendescloizite
_space_group_IT_number           19
_symmetry_space_group_name_Hall  'P 2ac 2ab'
_symmetry_space_group_name_H-M   'P 21 21 21'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_length_a                   7.646
_cell_length_b                   9.363
_cell_length_c                   6.077
_cell_volume                     435.049
_exptl_crystal_density_diffrn    6.542
_cod_original_formula_sum        'Pb Zn As O5 H'
_cod_database_code               9009424
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type helium-neon
_raman_measurement_device.excitation_laser_wavelength 780
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 12
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R140430.rod
_rod_data_source.block           3500000
_rod_database.code               1000169
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9009424 COD http://www.crystallography.net/cod/9009424.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
91.55994 0.0000000E+00
92.04205 3.487793
92.52417 30.71448
93.00629 88.50513
93.48840 146.2766
93.97052 186.8972
94.45264 202.4347
94.93475 217.9722
95.41687 235.8561
95.89898 255.6421
96.38110 278.8608
96.86321 306.2516
97.34533 336.4723
97.82745 365.8750
98.30956 404.9510
98.79168 453.8533
99.27380 509.7795
99.75591 572.1516
100.2380 640.0922
100.7201 712.4194
101.2023 789.8154
101.6844 871.4672
102.1665 951.5663
102.6486 1039.032
103.1307 1120.189
103.6128 1183.760
104.0950 1230.503
104.5771 1256.894
105.0592 1255.408
105.5413 1232.703
106.0234 1194.470
106.5055 1137.813
106.9877 1066.451
107.4698 994.9510
107.9519 920.4958
108.4340 849.0686
108.9161 780.8102
109.3982 716.5295
109.8804 658.7732
110.3625 610.1306
110.8446 570.7363
111.3267 542.0293
111.8088 528.3967
112.2909 521.8384
112.7731 520.3263
113.2552 522.5166
113.7373 528.4055
114.2194 535.7091
114.7015 541.2031
115.1836 551.5405
115.6658 568.9619
116.1479 588.5898
116.6300 606.5015
117.1121 621.9637
117.5942 635.6293
118.0763 648.7480
118.5584 664.1573
119.0406 672.4788
119.5227 671.0659
120.0048 660.9061
120.4869 643.5804
120.9690 618.2605
121.4511 587.1570
121.9333 554.9521
122.4154 520.0092
122.8975 484.5311
123.3796 450.6149
123.8617 418.3431
124.3438 387.0084
124.8260 357.8953
125.3081 329.5853
125.7902 300.3683
126.2723 269.4385
126.7544 237.8201
127.2365 208.2559
127.7187 180.9556
128.2008 155.7596
128.6829 131.9543
129.1650 109.6511
129.6471 89.20459
130.1292 70.88507
130.6114 54.64569
131.0935 39.89709
131.5756 26.04858
132.0577 14.28851
132.5398 5.640503
133.0219 0.3688350
133.5041 4.956848
133.9862 9.146912
134.4683 12.92334
134.9504 16.53223
135.4325 21.19507
135.9146 24.83734
136.3968 25.57123
136.8789 23.46393
137.3610 20.67407
137.8431 19.77911
138.3252 21.37811
138.8073 22.29388
139.2895 22.22589
139.7716 21.52814
140.2537 20.50244
140.7358 19.11334
141.2179 17.70215
141.7000 16.97076
142.1821 16.91626
142.6643 16.89941
143.1464 16.88525
143.6285 16.75385
144.1106 15.78070
144.5927 13.20233
145.0748 10.34064
145.5570 8.339111
146.0391 7.212036
146.5212 6.534668
147.0033 5.927490
147.4854 5.356079
147.9675 5.167603
148.4497 5.058044
148.9318 5.659729
149.4139 5.147400
149.8960 5.860291
150.3781 6.847168
150.8602 7.129639
151.3424 7.150696
151.8245 5.623962
152.3066 2.061462
152.7887 2.468689
153.2708 7.117188
153.7529 11.57019
154.2351 16.07898
154.7172 21.29095
155.1993 27.53876
155.6814 34.21564
156.1635 41.62903
156.6456 49.33624
157.1278 56.91315
157.6099 64.17297
158.0920 71.03418
158.5741 77.07922
159.0562 81.28149
159.5383 85.91455
160.0205 91.63452
160.5026 98.19672
160.9847 105.1716
161.4668 112.5315
161.9489 119.9518
162.4310 126.1531
162.9131 131.0211
163.3953 134.9309
163.8774 137.5189
164.3595 138.9440
164.8416 140.7993
165.3237 144.0119
165.8058 148.4650
166.2880 153.6907
166.7701 160.1270
167.2522 166.9496
167.7343 173.1550
168.2164 178.5946
168.6985 184.0950
169.1807 189.8634
169.6628 196.0153
170.1449 202.9088
170.6270 211.0677
171.1091 219.7879
171.5912 227.2606
172.0734 232.4964
172.5555 238.3478
173.0376 246.4265
173.5197 255.6224
174.0018 264.4202
174.4839 271.9274
174.9661 278.3040
175.4482 284.5138
175.9303 292.0480
176.4124 297.5466
176.8945 299.7870
177.3766 299.4545
177.8588 297.7859
178.3409 295.6586
178.8230 293.0653
179.3051 289.1973
179.7872 284.0189
180.2693 277.6326
180.7515 269.2464
181.2336 259.5187
181.7157 250.0450
182.1978 242.2134
182.6799 236.2352
183.1620 229.9683
183.6441 222.5607
184.1263 215.6568
184.6084 210.0430
185.0905 205.7437
185.5726 202.3898
186.0547 199.6751
186.5368 197.5870
187.0190 196.1885
187.5011 195.1241
187.9832 194.9831
188.4653 196.9470
188.9474 200.9888
189.4296 204.6407
189.9117 204.9363
190.3938 201.9985
190.8759 200.3898
191.3580 200.9771
191.8401 202.8556
192.3223 205.4397
192.8044 208.9187
193.2865 212.2823
193.7686 214.0251
194.2507 214.8693
194.7328 217.0349
195.2150 221.9476
195.6971 228.3234
196.1792 233.5713
196.6613 236.8436
197.1434 240.8354
197.6255 247.5348
198.1077 256.4446
198.5898 266.4154
199.0719 276.9814
199.5540 288.0606
200.0361 299.4798
200.5182 310.9399
201.0004 323.3537
201.4825 336.5354
201.9646 350.8539
202.4467 367.0202
202.9288 385.8166
203.4109 407.0497
203.8930 428.2680
204.3752 448.5126
204.8573 469.7618
205.3394 492.9098
205.8215 517.4242
206.3036 542.2621
206.7857 566.5125
207.2679 590.3180
207.7500 615.1830
208.2321 641.9285
208.7142 668.8069
209.1963 695.8214
209.6784 722.5984
210.1606 748.6442
210.6427 774.1464
211.1248 799.6394
211.6069 818.3139
212.0890 829.5012
212.5711 835.2429
213.0533 836.1803
213.5354 832.3383
214.0175 823.3336
214.4996 808.4958
214.9817 787.1818
215.4638 763.7634
215.9460 737.0767
216.4281 709.7550
216.9102 682.2039
217.3923 654.9516
217.8744 628.7670
218.3565 604.4980
218.8387 582.3651
219.3208 561.4944
219.8029 541.2529
220.2850 522.4655
220.7671 505.7483
221.2492 491.0466
221.7314 477.7096
222.2135 465.1745
222.6956 453.6023
223.1777 443.4665
223.6598 435.9003
224.1419 428.9165
224.6240 421.2550
225.1062 412.8099
225.5883 403.7929
226.0704 393.9849
226.5525 383.6408
227.0346 374.2984
227.5167 366.9029
227.9989 360.0460
228.4810 352.7571
228.9631 345.0189
229.4452 336.5574
229.9273 326.8705
230.4094 316.3132
230.8916 305.8265
231.3737 295.8365
231.8558 285.8126
232.3379 275.0072
232.8200 263.3028
233.3021 251.6610
233.7843 240.9114
234.2664 230.5394
234.7485 219.7111
235.2306 207.9153
235.7127 195.8315
236.1948 184.3247
236.6770 173.4142
237.1591 162.7576
237.6412 152.0313
238.1233 141.4626
238.6054 131.2444
239.0875 121.3742
239.5697 111.9666
240.0518 103.2315
240.5339 95.15369
241.0160 87.72070
241.4981 81.27802
241.9802 75.28448
242.4624 69.18060
242.9445 62.70007
243.4266 56.34711
243.9087 51.09875
244.3908 47.36121
244.8729 43.66675
245.3550 39.62354
245.8372 35.44659
246.3193 31.30798
246.8014 27.26495
247.2835 23.30219
247.7656 19.19971
248.2477 14.50586
248.7299 10.80957
249.2120 9.411499
249.6941 8.412109
250.1762 6.162231
250.6583 2.195496
251.1404 2.382996
251.6226 5.781433
252.1047 7.693787
252.5868 9.003601
253.0689 9.270813
253.5510 9.394653
254.0331 10.04663
254.5153 11.38092
254.9974 13.07654
255.4795 14.72449
255.9616 16.56641
256.4437 17.76965
256.9258 18.04688
257.4080 18.01697
257.8901 17.93237
258.3722 17.91052
258.8543 18.08569
259.3364 18.69275
259.8185 20.03601
260.3007 21.03571
260.7828 21.48993
261.2649 21.83374
261.7470 22.54132
262.2291 23.53918
262.7112 24.18854
263.1934 23.60162
263.6755 21.08087
264.1576 19.92542
264.6397 21.52606
265.1218 23.06769
265.6039 23.04755
266.0861 21.42468
266.5682 18.92017
267.0503 16.09601
267.5324 12.78064
268.0145 10.43304
268.4966 9.757507
268.9788 9.199280
269.4609 8.073914
269.9430 6.385498
270.4251 4.498657
270.9072 2.762817
271.3893 1.232422
271.8715 1.293457
272.3536 5.353821
272.8357 9.635559
273.3178 13.32086
273.7999 16.71100
274.2820 20.69598
274.7642 25.92255
275.2463 32.30579
275.7284 38.68048
276.2105 44.60522
276.6926 51.00146
277.1747 58.16669
277.6568 66.07611
278.1389 74.62982
278.6211 83.82343
279.1032 93.54669
279.5853 103.4863
280.0674 113.6002
280.5495 123.9642
281.0316 134.2208
281.5138 144.7909
281.9959 156.2749
282.4780 168.8165
282.9601 182.7489
283.4422 198.9045
283.9243 218.1565
284.4065 237.6706
284.8886 256.3161
285.3707 275.0355
285.8528 295.1727
286.3349 317.2170
286.8170 340.7383
287.2992 365.2031
287.7813 389.8994
288.2634 417.2988
288.7455 448.2917
289.2276 481.8719
289.7097 517.0015
290.1919 553.5085
290.6740 590.4294
291.1561 626.6013
291.6382 661.4712
292.1203 699.3625
292.6024 743.0573
293.0846 788.6470
293.5667 832.2317
294.0488 873.5047
294.5309 914.3443
295.0130 957.4801
295.4951 1002.699
295.9773 1042.519
296.4594 1076.039
296.9415 1104.515
297.4236 1128.558
297.9057 1148.197
298.3878 1164.188
298.8700 1177.214
299.3521 1186.501
299.8342 1190.988
300.3163 1187.545
300.7984 1182.232
301.2805 1177.268
301.7627 1173.031
302.2448 1170.771
302.7269 1170.760
303.2090 1173.689
303.6911 1180.842
304.1732 1192.562
304.6554 1207.261
305.1375 1222.910
305.6196 1240.891
306.1017 1265.139
306.5838 1297.668
307.0659 1336.364
307.5481 1376.490
308.0302 1416.452
308.5123 1461.808
308.9944 1514.799
309.4765 1574.193
309.9586 1637.365
310.4408 1703.349
310.9229 1773.380
311.4050 1848.795
311.8871 1929.401
312.3692 2014.501
312.8513 2104.682
313.3335 2198.869
313.8156 2297.158
314.2977 2399.440
314.7798 2503.857
315.2619 2609.963
315.7440 2717.809
316.2262 2823.896
316.7083 2928.603
317.1904 3030.922
317.6725 3132.223
318.1546 3232.251
318.6367 3323.629
319.1188 3401.497
319.6010 3465.469
320.0831 3522.415
320.5652 3578.062
321.0473 3621.899
321.5294 3647.857
322.0115 3657.077
322.4937 3653.919
322.9758 3640.101
323.4579 3615.214
323.9400 3578.614
324.4221 3529.395
324.9042 3473.656
325.3864 3411.608
325.8685 3344.679
326.3506 3274.458
326.8327 3200.931
327.3148 3125.836
327.7969 3050.566
328.2791 2974.057
328.7612 2902.804
329.2433 2837.965
329.7254 2779.279
330.2075 2727.292
330.6896 2682.104
331.1718 2640.918
331.6539 2600.463
332.1360 2560.905
332.6181 2526.790
333.1002 2498.935
333.5823 2476.265
334.0645 2459.191
334.5466 2447.234
335.0287 2437.249
335.5108 2427.363
335.9929 2417.654
336.4750 2408.844
336.9572 2403.424
337.4393 2396.110
337.9214 2384.321
338.4035 2368.890
338.8856 2351.845
339.3677 2334.034
339.8499 2315.420
340.3320 2295.900
340.8141 2275.966
341.2962 2254.540
341.7783 2230.250
342.2604 2204.737
342.7426 2180.921
343.2247 2159.738
343.7068 2138.230
344.1889 2112.279
344.6710 2080.256
345.1531 2047.665
345.6353 2015.538
346.1174 1982.420
346.5995 1948.060
347.0816 1912.221
347.5637 1872.859
348.0458 1828.563
348.5280 1778.956
349.0101 1726.286
349.4922 1671.005
349.9743 1612.899
350.4564 1552.163
350.9385 1489.012
351.4207 1423.003
351.9028 1353.909
352.3849 1282.650
352.8670 1212.337
353.3491 1144.821
353.8312 1076.159
354.3134 1003.469
354.7955 930.4611
355.2776 861.0193
355.7597 796.5946
356.2418 735.9409
356.7239 676.3217
357.2061 616.5294
357.6882 560.8013
358.1703 508.5948
358.6524 460.3029
359.1345 416.9709
359.6166 378.1532
360.0987 342.6165
360.5808 308.9912
361.0630 277.2427
361.5451 247.8086
362.0272 220.2123
362.5093 195.2849
362.9914 173.3914
363.4735 154.3169
363.9557 138.2906
364.4378 125.5314
364.9199 115.4746
365.4020 105.6335
365.8841 94.03784
366.3662 85.91608
366.8484 82.85291
367.3305 82.75690
367.8126 83.76410
368.2947 85.33002
368.7768 87.99738
369.2589 92.49396
369.7411 98.70154
370.2232 106.9597
370.7053 117.1708
371.1874 129.2874
371.6695 143.8152
372.1516 160.4426
372.6338 178.2639
373.1159 196.2654
373.5980 214.4584
374.0801 234.3294
374.5622 256.2786
375.0443 279.7443
375.5265 304.4408
376.0086 330.3239
376.4907 357.0551
376.9728 384.4678
377.4549 413.1138
377.9370 444.1153
378.4192 477.2416
378.9013 514.2386
379.3834 556.7048
379.8655 602.4850
380.3476 649.6987
380.8297 698.0089
381.3119 749.7991
381.7940 806.8242
382.2761 869.1747
382.7582 936.7689
383.2403 1009.791
383.7224 1088.612
384.2046 1172.166
384.6867 1260.493
385.1688 1356.069
385.6509 1460.654
386.1330 1572.455
386.6151 1689.129
387.0973 1811.315
387.5794 1934.944
388.0615 2064.532
388.5436 2192.631
389.0257 2309.454
389.5078 2417.070
389.9900 2505.807
390.4721 2572.289
390.9542 2615.092
391.4363 2620.574
391.9184 2581.967
392.4005 2504.570
392.8827 2394.622
393.3648 2251.806
393.8469 2097.041
394.3290 1930.573
394.8111 1760.001
395.2932 1597.300
395.7754 1442.366
396.2575 1299.427
396.7396 1171.368
397.2217 1059.129
397.7038 958.8061
398.1859 871.8690
398.6681 794.3716
399.1501 724.7477
399.6323 662.3989
400.1144 606.0128
400.5965 555.5318
401.0786 509.7715
401.5607 466.0632
402.0428 422.1115
402.5250 383.3179
403.0071 352.8002
403.4892 326.9737
403.9713 302.2401
404.4534 277.7622
404.9355 253.9659
405.4177 231.2502
405.8998 209.6039
406.3819 190.6086
406.8640 174.7670
407.3461 160.8176
407.8282 148.5485
408.3104 137.5762
408.7925 127.1118
409.2746 116.4492
409.7567 105.9971
410.2388 97.40375
410.7209 92.52869
411.2031 87.41547
411.6852 80.75494
412.1673 74.19556
412.6494 69.31335
413.1315 66.46448
413.6136 64.85999
414.0958 63.79376
414.5779 63.69128
415.0600 62.43982
415.5421 58.65399
416.0242 55.06421
416.5063 53.31458
416.9885 52.65295
417.4706 51.26080
417.9527 47.88733
418.4348 42.95398
418.9169 37.59357
419.3990 31.29340
419.8812 25.80206
420.3633 22.61017
420.8454 19.92700
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