#\#CIF_2.0 #------------------------------------------------------------------------------ #$Date: 2018-04-26 14:03:20 +0300 (Thu, 26 Apr 2018) $ #$Revision: 636 $ #$URL: svn://172.16.1.111/rod/cif/1/00/01/1000170.rod $ #------------------------------------------------------------------------------ # # This file is available in the Raman Open Database (ROD), # http://solsa.crystallography.net/rod/ # # All data on this site have been placed in the public domain by the # contributors. # data_1000170 loop_ _publ_author_name 'Balassone, G.' 'Franco, E.' 'Mattia, C. A.' 'Puliti, R.' _publ_section_title ; Indialite in xenolithic rocks from Somma-Vesuvius volcano (Southern Italy): Crystal chemistry and petrogenetic features ; _journal_name_full 'American Mineralogist' _journal_page_first 1 _journal_page_last 6 _journal_volume 89 _journal_year 2004 _chemical_compound_source R140777 _chemical_formula_sum 'Al4.251 Ca0.084 Fe0.06 K0.336 Mg1.94 O18 Si4.749' _chemical_name_mineral Indialite _space_group_IT_number 192 _symmetry_space_group_name_Hall '-P 6 2c' _symmetry_space_group_name_H-M 'P 6/m c c' _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 120 _cell_length_a 9.775 _cell_length_b 9.775 _cell_length_c 9.354 _cell_volume 774.037 _exptl_crystal_density_diffrn 2.588 _cod_original_formula_sum '(Al4.251 Si4.749) (Mg1.94 Fe.06) O18 K.336 Ca.084' _cod_database_code 9003098 _raman_determination_method experimental _raman_measurement_device.location 'Arizona University' _raman_measurement_device.company 'Thermo Scientific' _raman_measurement_device.model 'Nicolet Almega XR' _raman_measurement_device.optics_type microscope _raman_measurement_device.microscope_system dispersive _raman_measurement_device.microscope_objective_magnification 50 _raman_measurement_device.microscope_numerical_aperture 0.5 _raman_measurement_device.excitation_laser_type helium-neon _raman_measurement_device.excitation_laser_wavelength 780 _raman_measurement_device.configuration simple _raman_measurement_device.resolution 4 _raman_measurement_device.power_on_sample 12 _raman_measurement_device.direction_polarization unoriented _raman_measurement_device.spot_size 1 _raman_measurement_device.diffraction_grating 400 _raman_measurement.environment Air _raman_measurement.environment_details ; The sample was measured in air. ; _raman_measurement.temperature 300 _raman_measurement.pressure 100 _raman_measurement.background_subtraction no _raman_measurement.background_subtraction_details ; No background subtraction method was applied. ; _raman_measurement.baseline_correction no _raman_measurement.baseline_correction_details ; No baseline correction method was applied. ; _raman_measurement.integration_time 10 _rod_data_source.file R140777.rod _rod_data_source.block 3500000 _rod_database.code 1000170 loop_ _raman_complementary.id _raman_complementary.method 1 XRD loop_ _raman_measurement_device_calibration.id _raman_measurement_device_calibration.standard 1 neon_lamp loop_ _rod_related_entry.id _rod_related_entry.code _rod_related_entry.database _rod_related_entry.uri _rod_related_entry.description 1 9003098 COD http://www.crystallography.net/cod/9003098.html ; XRD analysis data was done. ; loop_ _raman_spectrum.raman_shift _raman_spectrum.intensity 101.6844 0.0000000E+00 102.1665 1.1963000E-02 102.6486 2.170654 103.1307 7.167969 103.6128 7.017090 104.0950 2.520020 104.5771 0.4494630 105.0592 1.189453 105.5413 5.367432 106.0234 9.583496 106.5055 12.21045 106.9877 13.79175 107.4698 17.28906 107.9519 24.57324 108.4340 31.06079 108.9161 34.63599 109.3982 35.85107 109.8804 36.21338 110.3625 37.15723 110.8446 38.25903 111.3267 40.02832 111.8088 41.81177 112.2909 44.67871 112.7731 49.73828 113.2552 56.77588 113.7373 64.31714 114.2194 70.09668 114.7015 71.62158 115.1836 76.15112 115.6658 84.71387 116.1479 95.75000 116.6300 108.4463 117.1121 122.4529 117.5942 136.8428 118.0763 151.4668 118.5584 168.7715 119.0406 183.4929 119.5227 194.2576 120.0048 199.4309 120.4869 198.8247 120.9690 191.3098 121.4511 178.9360 121.9333 166.4585 122.4154 152.9941 122.8975 140.3574 123.3796 130.8884 123.8617 124.6633 124.3438 118.2375 124.8260 109.5173 125.3081 100.2681 125.7902 92.10034 126.2723 85.86133 126.7544 80.69727 127.2365 74.73242 127.7187 67.25781 128.2008 60.36060 128.6829 55.17651 129.1650 50.72559 129.6471 45.61792 130.1292 38.79297 130.6114 30.46631 131.0935 23.63916 131.5756 19.03711 132.0577 15.38477 132.5398 13.35791 133.0219 12.15576 133.5041 10.10840 133.9862 5.518311 134.4683 2.441895 134.9504 7.604980 135.4325 9.511963 135.9146 9.641357 136.3968 8.536621 136.8789 6.393066 137.3610 3.320068 137.8431 0.9587400 138.3252 7.002197 138.8073 11.30811 139.2895 13.23853 139.7716 13.50732 140.2537 12.55298 140.7358 10.26538 141.2179 7.556641 141.7000 5.510254 142.1821 4.041748 142.6643 2.990234 143.1464 2.393555 143.6285 2.189697 144.1106 2.104492 144.5927 1.916504 145.0748 2.077637 145.5570 2.993896 146.0391 4.660645 146.5212 6.521484 147.0033 8.234131 147.4854 9.817627 147.9675 10.94531 148.4497 11.32715 148.9318 11.36890 149.4139 11.09155 149.8960 10.53809 150.3781 10.03613 150.8602 9.976563 151.3424 10.10254 151.8245 11.37720 152.3066 14.87500 152.7887 18.77051 153.2708 21.37280 153.7529 22.08984 154.2351 21.94653 154.7172 23.51099 155.1993 28.67285 155.6814 33.45605 156.1635 38.60693 156.6456 43.02515 157.1278 45.04712 157.6099 43.72900 158.0920 39.98633 158.5741 37.68896 159.0562 39.13257 159.5383 39.75293 160.0205 37.15747 160.5026 32.23145 160.9847 26.74414 161.4668 21.43481 161.9489 16.59106 162.4310 13.22827 162.9131 12.06226 163.3953 11.68506 163.8774 11.60010 164.3595 11.75684 164.8416 11.70581 165.3237 10.94019 165.8058 9.833740 166.2880 9.284912 166.7701 9.982910 167.2522 10.79883 167.7343 10.23584 168.2164 7.980957 168.6985 5.820801 169.1807 4.953125 169.6628 4.772705 170.1449 4.562988 170.6270 3.864502 171.1091 3.088379 171.5912 3.281006 172.0734 4.993408 172.5555 6.713135 173.0376 8.183838 173.5197 9.248291 174.0018 9.521973 174.4839 8.440674 174.9661 6.431152 175.4482 6.174805 175.9303 9.711670 176.4124 12.81201 176.8945 13.87915 177.3766 13.75317 177.8588 13.98218 178.3409 15.73511 178.8230 19.02979 179.3051 22.14575 179.7872 25.06152 180.2693 27.81641 180.7515 30.41528 181.2336 32.84766 181.7157 35.21460 182.1978 37.78027 182.6799 40.79126 183.1620 41.04810 183.6441 35.88403 184.1263 30.94629 184.6084 29.41602 185.0905 31.05493 185.5726 33.27026 186.0547 33.56860 186.5368 31.56714 187.0190 31.07373 187.5011 33.86450 187.9832 36.87329 188.4653 37.69189 188.9474 36.11255 189.4296 33.63574 189.9117 31.48486 190.3938 29.69995 190.8759 28.21411 191.3580 26.65601 191.8401 25.50220 192.3223 25.41187 192.8044 26.77441 193.2865 28.19458 193.7686 27.75342 194.2507 26.14600 194.7328 25.43262 195.2150 27.46167 195.6971 30.72266 196.1792 31.74976 196.6613 29.33618 197.1434 26.25537 197.6255 24.56421 198.1077 23.84473 198.5898 23.16821 199.0719 21.45508 199.5540 19.21753 200.0361 19.01025 200.5182 22.81812 201.0004 25.96411 201.4825 25.51929 201.9646 22.49585 202.4467 19.42358 202.9288 18.12134 203.4109 18.50342 203.8930 18.68506 204.3752 17.47656 204.8573 17.41748 205.3394 20.36108 205.8215 25.31567 206.3036 29.97632 206.7857 32.59863 207.2679 33.15186 207.7500 32.21997 208.2321 27.87988 208.7142 23.72290 209.1963 20.41821 209.6784 18.21924 210.1606 17.43823 210.6427 18.62842 211.1248 22.16650 211.6069 24.13477 212.0890 24.02173 212.5711 22.99072 213.0533 20.82129 213.5354 18.09521 214.0175 15.85303 214.4996 14.95996 214.9817 15.41382 215.4638 16.23975 215.9460 17.43237 216.4281 18.98120 216.9102 21.40942 217.3923 24.42627 217.8744 26.90625 218.3565 27.67163 218.8387 26.42041 219.3208 25.41968 219.8029 24.55640 220.2850 23.94678 220.7671 23.68042 221.2492 23.76929 221.7314 24.25195 222.2135 25.28662 222.6956 26.89697 223.1777 28.01465 223.6598 28.05591 224.1419 28.03345 224.6240 28.92432 225.1062 30.73022 225.5883 32.34424 226.0704 32.66553 226.5525 31.89355 227.0346 31.77271 227.5167 32.89844 227.9989 34.42578 228.4810 35.40454 228.9631 35.76392 229.4452 36.58716 229.9273 39.51440 230.4094 43.50366 230.8916 45.64746 231.3737 43.78687 231.8558 40.78345 232.3379 39.85986 232.8200 41.19409 233.3021 43.30615 233.7843 45.74048 234.2664 48.28784 234.7485 50.59717 235.2306 52.45581 235.7127 54.14282 236.1948 56.05371 236.6770 58.24609 237.1591 60.46533 237.6412 62.79956 238.1233 65.03296 238.6054 66.92432 239.0875 68.44336 239.5697 69.52856 240.0518 69.88623 240.5339 69.19092 241.0160 68.82959 241.4981 69.83569 241.9802 71.21680 242.4624 71.94482 242.9445 71.55371 243.4266 70.72266 243.9087 70.59155 244.3908 71.26489 244.8729 72.36670 245.3550 74.41162 245.8372 76.47852 246.3193 77.60376 246.8014 77.41382 247.2835 76.70996 247.7656 76.75708 248.2477 77.49121 248.7299 79.23438 249.2120 83.11206 249.6941 87.25439 250.1762 89.90674 250.6583 90.59448 251.1404 90.72217 251.6226 92.76025 252.1047 97.69263 252.5868 102.3801 253.0689 106.4810 253.5510 110.3970 254.0331 114.1321 254.5153 117.6897 254.9974 121.5049 255.4795 126.0808 255.9616 131.2632 256.4437 137.8164 256.9258 145.9189 257.4080 154.8337 257.8901 164.7949 258.3722 175.4675 258.8543 185.5327 259.3364 193.5198 259.8185 200.4763 260.3007 202.0598 260.7828 199.4387 261.2649 191.9419 261.7470 177.1184 262.2291 155.8721 262.7112 132.9509 263.1934 113.5642 263.6755 98.47632 264.1576 84.48535 264.6397 71.77246 265.1218 59.79224 265.6039 47.63477 266.0861 35.71704 266.5682 25.67090 267.0503 19.24609 267.5324 16.98267 268.0145 15.39014 268.4966 16.08374 268.9788 15.87305 269.4609 12.53589 269.9430 6.660400 270.4251 0.5034180 270.9072 4.282959 271.3893 7.675049 271.8715 8.947998 272.3536 6.763916 272.8357 4.271973 273.3178 2.445801 273.7999 1.375977 274.2820 1.109375 274.7642 1.825684 275.2463 3.389893 275.7284 4.066406 276.2105 3.674316 276.6926 2.854736 277.1747 1.647217 277.6568 0.1755370 278.1389 1.389404 278.6211 3.012207 279.1032 4.579834 279.5853 5.551758 280.0674 5.158203 280.5495 5.200195 281.0316 6.872559 281.5138 9.207031 281.9959 10.29639 282.4780 9.185547 282.9601 6.843750 283.4422 5.799805 283.9243 6.387451 284.4065 7.372803 284.8886 8.922119 285.3707 10.62573 285.8528 11.59888 286.3349 11.42480 286.8170 11.23145 287.2992 13.18921 287.7813 18.03516 288.2634 22.29956 288.7455 25.09985 289.2276 27.16138 289.7097 29.26855 290.1919 31.59521 290.6740 34.06152 291.1561 36.76440 291.6382 39.81787 292.1203 41.99609 292.6024 42.82861 293.0846 42.91895 293.5667 42.53467 294.0488 41.73389 294.5309 41.33276 295.0130 42.40161 295.4951 44.92798 295.9773 46.22168 296.4594 45.13477 296.9415 43.53247 297.4236 42.91040 297.9057 43.26416 298.3878 43.61743 298.8700 43.22754 299.3521 42.22559 299.8342 41.63013 300.3163 42.27515 300.7984 42.56787 301.2805 41.11499 301.7627 38.31470 302.2448 36.00928 302.7269 35.27197 303.2090 35.62085 303.6911 35.52832 304.1732 34.95410 304.6554 34.10107 305.1375 33.35840 305.6196 32.44507 306.1017 30.34253 306.5838 26.26855 307.0659 21.60400 307.5481 19.41138 308.0302 20.36865 308.5123 20.57544 308.9944 18.72095 309.4765 15.32422 309.9586 10.55859 310.4408 3.989990 310.9229 1.777588 311.4050 1.996338 311.8871 3.546387 312.3692 6.894775 312.8513 4.163574 313.3335 0.5075680 313.8156 2.031738 314.2977 0.3842770 314.7798 4.070068 315.2619 7.226563 315.7440 9.687256 316.2262 10.19873 316.7083 7.048584 317.1904 3.033447 317.6725 2.1970000E-03 318.1546 1.931396 318.6367 2.357422 319.1188 0.4704590 319.6010 3.157471 320.0831 5.539307 320.5652 5.825928 321.0473 5.771484 321.5294 6.338135 322.0115 7.405029 322.4937 8.541748 322.9758 9.707275 323.4579 10.64624 323.9400 10.53247 324.4221 8.587646 324.9042 7.258057 325.3864 8.025879 325.8685 9.968018 326.3506 11.20435 326.8327 11.02393 327.3148 10.47485 327.7969 11.47852 328.2791 14.44312 328.7612 16.27539 329.2433 16.02954 329.7254 14.61377 330.2075 12.78418 330.6896 10.65356 331.1718 8.987549 331.6539 8.824219 332.1360 10.21362 332.6181 10.65503 333.1002 8.842041 333.5823 6.960449 334.0645 6.702637 334.5466 8.032715 335.0287 9.915527 335.5108 11.78491 335.9929 13.53442 336.4750 14.75000 336.9572 14.79517 337.4393 15.12109 337.9214 17.12598 338.4035 19.64990 338.8856 20.18677 339.3677 17.39087 339.8499 12.96729 340.3320 11.11792 340.8141 12.96777 341.2962 14.22583 341.7783 13.88110 342.2604 12.91382 342.7426 12.29224 343.2247 12.18286 343.7068 12.43628 344.1889 13.02441 344.6710 14.14893 345.1531 15.11377 345.6353 15.80396 346.1174 16.58203 346.5995 17.98828 347.0816 19.82837 347.5637 21.02246 348.0458 20.52954 348.5280 18.25439 349.0101 16.77100 349.4922 16.79688 349.9743 16.89868 350.4564 16.27856 350.9385 15.07031 351.4207 13.88403 351.9028 13.11230 352.3849 12.71167 352.8670 12.26685 353.3491 10.99780 353.8312 10.49463 354.3134 11.42651 354.7955 13.14746 355.2776 14.92017 355.7597 16.47534 356.2418 17.75732 356.7239 18.48120 357.2061 18.18506 357.6882 18.26172 358.1703 18.16113 358.6524 18.80298 359.1345 21.36768 359.6166 25.56519 360.0987 29.63184 360.5808 31.80835 361.0630 31.89893 361.5451 31.86206 362.0272 30.93042 362.5093 30.65552 362.9914 32.00952 363.4735 34.37378 363.9557 36.52075 364.4378 37.67529 364.9199 38.14185 365.4020 39.20923 365.8841 41.29175 366.3662 43.48047 366.8484 46.30396 367.3305 48.87036 367.8126 50.43506 368.2947 50.73267 368.7768 49.76025 369.2589 47.55957 369.7411 43.94336 370.2232 39.78394 370.7053 34.77856 371.1874 29.51978 371.6695 23.56055 372.1516 17.51611 372.6338 12.69653 373.1159 10.75317 373.5980 11.57544 374.0801 11.25391 374.5622 8.248779 375.0443 5.991455 375.5265 6.134033 376.0086 7.519287 376.4907 8.585449 376.9728 8.693848 377.4549 7.928955 377.9370 6.310791 378.4192 3.331543 378.9013 0.9589840 379.3834 5.6150001E-03 379.8655 0.3195800 380.3476 0.6010740 380.8297 0.9636230 381.3119 0.8945310 381.7940 0.3449710 382.2761 2.731689 382.7582 5.007080 383.2403 7.666260 383.7224 9.305908 384.2046 8.501709 384.6867 5.883545 385.1688 3.691162 385.6509 3.209961 386.1330 3.988037 386.6151 5.418213 387.0973 7.965088 387.5794 9.417236 388.0615 6.820801 388.5436 2.749756 389.0257 1.099365 389.5078 3.605713 389.9900 6.807617 390.4721 7.514160 390.9542 6.017822 391.4363 4.611084 391.9184 3.814941 392.4005 3.723145 392.8827 5.045898 393.3648 8.067383 393.8469 9.304199 394.3290 5.504883 394.8111 0.2998050 395.2932 2.796143 395.7754 0.9968260 396.2575 1.354492 396.7396 0.6071780 397.2217 2.855225 397.7038 4.394287 398.1859 1.673584 398.6681 1.139648 399.1501 0.8210450 399.6323 1.869629 400.1144 3.996094 400.5965 4.064453 401.0786 2.683594 401.5607 1.496582 402.0428 0.2507320 402.5250 0.3886720 403.0071 0.4040530 403.4892 1.558105 403.9713 1.771484 404.4534 0.7707520 404.9355 0.8037110 405.4177 2.367676 405.8998 4.156006 406.3819 4.482910 406.8640 1.785889 407.3461 0.6872560 407.8282 1.020508 408.3104 0.2128910 408.7925 1.266846 409.2746 1.013184 409.7567 0.1916500 410.2388 0.7165530 410.7209 0.3410640 411.2031 0.9316410 411.6852 0.1206050 412.1673 1.160645 412.6494 0.1186520 413.1315 3.323730 413.6136 7.166992 414.0958 8.646973 414.5779 7.167969 415.0600 5.728271 415.5421 3.380127 416.0242 1.997803 416.5063 2.674316 416.9885 4.955566 417.4706 7.742676 417.9527 10.48340 418.4348 13.09399 418.9169 15.09497 419.3990 15.74365 419.8812 17.46387 420.3633 22.22485 420.8454 27.65942 421.3275 31.70068 421.8096 33.85352 422.2917 34.64795 422.7739 33.88818 423.2560 31.70117 423.7381 30.90820 424.2202 32.38745 424.7023 34.75537 425.1844 37.80298 425.6666 40.99487 426.1487 42.31592 426.6308 38.79468 427.1129 33.87158 427.5950 33.45215 428.0771 37.85327 428.5593 41.54517 429.0414 41.56006 429.5235 38.91382 430.0056 36.26343 430.4877 33.55371 430.9698 31.00562 431.4520 29.01050 431.9341 27.23901 432.4162 24.77710 432.8983 21.30396 433.3804 17.94116 433.8625 16.03979 434.3447 15.80981 434.8268 15.75488 435.3089 16.23560 435.7910 16.51904 436.2731 16.33813 436.7552 15.54810 437.2374 13.45923 437.7195 9.343750 438.2016 4.375732 438.6837 3.170166 439.1658 11.01660 439.6479 15.99438 440.1301 14.80518 440.6122 11.74683 441.0943 11.20459 441.5764 13.89062 442.0585 17.15063 442.5406 17.80713 443.0227 15.35327 443.5049 14.05688 443.9870 15.12964 444.4691 16.14429 444.9512 16.59619 445.4333 16.44971 445.9154 15.51709 446.3976 13.58618 446.8797 11.41187 447.3618 10.98901 447.8439 12.96021 448.3260 14.61328 448.8081 14.39624 449.2903 14.46387 449.7724 16.79688 450.2545 21.18677 450.7366 25.06738 451.2187 26.10669 451.7008 24.93054 452.1830 24.12500 452.6651 23.59082 453.1472 23.37659 453.6293 23.95618 454.1114 25.10583 454.5935 26.45813 455.0757 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