#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-04-26 14:03:20 +0300 (Thu, 26 Apr 2018) $
#$Revision: 636 $
#$URL: svn://172.16.1.111/rod/cif/1/00/01/1000170.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000170
loop_
_publ_author_name
'Balassone, G.'
'Franco, E.'
'Mattia, C. A.'
'Puliti, R.'
_publ_section_title
;
 Indialite in xenolithic rocks from Somma-Vesuvius volcano (Southern
 Italy): Crystal chemistry and petrogenetic features
;
_journal_name_full               'American Mineralogist'
_journal_page_first              1
_journal_page_last               6
_journal_volume                  89
_journal_year                    2004
_chemical_compound_source        R140777
_chemical_formula_sum
'Al4.251 Ca0.084 Fe0.06 K0.336 Mg1.94 O18 Si4.749'
_chemical_name_mineral           Indialite
_space_group_IT_number           192
_symmetry_space_group_name_Hall  '-P 6 2c'
_symmetry_space_group_name_H-M   'P 6/m c c'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                120
_cell_length_a                   9.775
_cell_length_b                   9.775
_cell_length_c                   9.354
_cell_volume                     774.037
_exptl_crystal_density_diffrn    2.588
_cod_original_formula_sum
'(Al4.251 Si4.749) (Mg1.94 Fe.06) O18 K.336 Ca.084'
_cod_database_code               9003098
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type helium-neon
_raman_measurement_device.excitation_laser_wavelength 780
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 12
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R140777.rod
_rod_data_source.block           3500000
_rod_database.code               1000170
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9003098 COD http://www.crystallography.net/cod/9003098.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
101.6844 0.0000000E+00
102.1665 1.1963000E-02
102.6486 2.170654
103.1307 7.167969
103.6128 7.017090
104.0950 2.520020
104.5771 0.4494630
105.0592 1.189453
105.5413 5.367432
106.0234 9.583496
106.5055 12.21045
106.9877 13.79175
107.4698 17.28906
107.9519 24.57324
108.4340 31.06079
108.9161 34.63599
109.3982 35.85107
109.8804 36.21338
110.3625 37.15723
110.8446 38.25903
111.3267 40.02832
111.8088 41.81177
112.2909 44.67871
112.7731 49.73828
113.2552 56.77588
113.7373 64.31714
114.2194 70.09668
114.7015 71.62158
115.1836 76.15112
115.6658 84.71387
116.1479 95.75000
116.6300 108.4463
117.1121 122.4529
117.5942 136.8428
118.0763 151.4668
118.5584 168.7715
119.0406 183.4929
119.5227 194.2576
120.0048 199.4309
120.4869 198.8247
120.9690 191.3098
121.4511 178.9360
121.9333 166.4585
122.4154 152.9941
122.8975 140.3574
123.3796 130.8884
123.8617 124.6633
124.3438 118.2375
124.8260 109.5173
125.3081 100.2681
125.7902 92.10034
126.2723 85.86133
126.7544 80.69727
127.2365 74.73242
127.7187 67.25781
128.2008 60.36060
128.6829 55.17651
129.1650 50.72559
129.6471 45.61792
130.1292 38.79297
130.6114 30.46631
131.0935 23.63916
131.5756 19.03711
132.0577 15.38477
132.5398 13.35791
133.0219 12.15576
133.5041 10.10840
133.9862 5.518311
134.4683 2.441895
134.9504 7.604980
135.4325 9.511963
135.9146 9.641357
136.3968 8.536621
136.8789 6.393066
137.3610 3.320068
137.8431 0.9587400
138.3252 7.002197
138.8073 11.30811
139.2895 13.23853
139.7716 13.50732
140.2537 12.55298
140.7358 10.26538
141.2179 7.556641
141.7000 5.510254
142.1821 4.041748
142.6643 2.990234
143.1464 2.393555
143.6285 2.189697
144.1106 2.104492
144.5927 1.916504
145.0748 2.077637
145.5570 2.993896
146.0391 4.660645
146.5212 6.521484
147.0033 8.234131
147.4854 9.817627
147.9675 10.94531
148.4497 11.32715
148.9318 11.36890
149.4139 11.09155
149.8960 10.53809
150.3781 10.03613
150.8602 9.976563
151.3424 10.10254
151.8245 11.37720
152.3066 14.87500
152.7887 18.77051
153.2708 21.37280
153.7529 22.08984
154.2351 21.94653
154.7172 23.51099
155.1993 28.67285
155.6814 33.45605
156.1635 38.60693
156.6456 43.02515
157.1278 45.04712
157.6099 43.72900
158.0920 39.98633
158.5741 37.68896
159.0562 39.13257
159.5383 39.75293
160.0205 37.15747
160.5026 32.23145
160.9847 26.74414
161.4668 21.43481
161.9489 16.59106
162.4310 13.22827
162.9131 12.06226
163.3953 11.68506
163.8774 11.60010
164.3595 11.75684
164.8416 11.70581
165.3237 10.94019
165.8058 9.833740
166.2880 9.284912
166.7701 9.982910
167.2522 10.79883
167.7343 10.23584
168.2164 7.980957
168.6985 5.820801
169.1807 4.953125
169.6628 4.772705
170.1449 4.562988
170.6270 3.864502
171.1091 3.088379
171.5912 3.281006
172.0734 4.993408
172.5555 6.713135
173.0376 8.183838
173.5197 9.248291
174.0018 9.521973
174.4839 8.440674
174.9661 6.431152
175.4482 6.174805
175.9303 9.711670
176.4124 12.81201
176.8945 13.87915
177.3766 13.75317
177.8588 13.98218
178.3409 15.73511
178.8230 19.02979
179.3051 22.14575
179.7872 25.06152
180.2693 27.81641
180.7515 30.41528
181.2336 32.84766
181.7157 35.21460
182.1978 37.78027
182.6799 40.79126
183.1620 41.04810
183.6441 35.88403
184.1263 30.94629
184.6084 29.41602
185.0905 31.05493
185.5726 33.27026
186.0547 33.56860
186.5368 31.56714
187.0190 31.07373
187.5011 33.86450
187.9832 36.87329
188.4653 37.69189
188.9474 36.11255
189.4296 33.63574
189.9117 31.48486
190.3938 29.69995
190.8759 28.21411
191.3580 26.65601
191.8401 25.50220
192.3223 25.41187
192.8044 26.77441
193.2865 28.19458
193.7686 27.75342
194.2507 26.14600
194.7328 25.43262
195.2150 27.46167
195.6971 30.72266
196.1792 31.74976
196.6613 29.33618
197.1434 26.25537
197.6255 24.56421
198.1077 23.84473
198.5898 23.16821
199.0719 21.45508
199.5540 19.21753
200.0361 19.01025
200.5182 22.81812
201.0004 25.96411
201.4825 25.51929
201.9646 22.49585
202.4467 19.42358
202.9288 18.12134
203.4109 18.50342
203.8930 18.68506
204.3752 17.47656
204.8573 17.41748
205.3394 20.36108
205.8215 25.31567
206.3036 29.97632
206.7857 32.59863
207.2679 33.15186
207.7500 32.21997
208.2321 27.87988
208.7142 23.72290
209.1963 20.41821
209.6784 18.21924
210.1606 17.43823
210.6427 18.62842
211.1248 22.16650
211.6069 24.13477
212.0890 24.02173
212.5711 22.99072
213.0533 20.82129
213.5354 18.09521
214.0175 15.85303
214.4996 14.95996
214.9817 15.41382
215.4638 16.23975
215.9460 17.43237
216.4281 18.98120
216.9102 21.40942
217.3923 24.42627
217.8744 26.90625
218.3565 27.67163
218.8387 26.42041
219.3208 25.41968
219.8029 24.55640
220.2850 23.94678
220.7671 23.68042
221.2492 23.76929
221.7314 24.25195
222.2135 25.28662
222.6956 26.89697
223.1777 28.01465
223.6598 28.05591
224.1419 28.03345
224.6240 28.92432
225.1062 30.73022
225.5883 32.34424
226.0704 32.66553
226.5525 31.89355
227.0346 31.77271
227.5167 32.89844
227.9989 34.42578
228.4810 35.40454
228.9631 35.76392
229.4452 36.58716
229.9273 39.51440
230.4094 43.50366
230.8916 45.64746
231.3737 43.78687
231.8558 40.78345
232.3379 39.85986
232.8200 41.19409
233.3021 43.30615
233.7843 45.74048
234.2664 48.28784
234.7485 50.59717
235.2306 52.45581
235.7127 54.14282
236.1948 56.05371
236.6770 58.24609
237.1591 60.46533
237.6412 62.79956
238.1233 65.03296
238.6054 66.92432
239.0875 68.44336
239.5697 69.52856
240.0518 69.88623
240.5339 69.19092
241.0160 68.82959
241.4981 69.83569
241.9802 71.21680
242.4624 71.94482
242.9445 71.55371
243.4266 70.72266
243.9087 70.59155
244.3908 71.26489
244.8729 72.36670
245.3550 74.41162
245.8372 76.47852
246.3193 77.60376
246.8014 77.41382
247.2835 76.70996
247.7656 76.75708
248.2477 77.49121
248.7299 79.23438
249.2120 83.11206
249.6941 87.25439
250.1762 89.90674
250.6583 90.59448
251.1404 90.72217
251.6226 92.76025
252.1047 97.69263
252.5868 102.3801
253.0689 106.4810
253.5510 110.3970
254.0331 114.1321
254.5153 117.6897
254.9974 121.5049
255.4795 126.0808
255.9616 131.2632
256.4437 137.8164
256.9258 145.9189
257.4080 154.8337
257.8901 164.7949
258.3722 175.4675
258.8543 185.5327
259.3364 193.5198
259.8185 200.4763
260.3007 202.0598
260.7828 199.4387
261.2649 191.9419
261.7470 177.1184
262.2291 155.8721
262.7112 132.9509
263.1934 113.5642
263.6755 98.47632
264.1576 84.48535
264.6397 71.77246
265.1218 59.79224
265.6039 47.63477
266.0861 35.71704
266.5682 25.67090
267.0503 19.24609
267.5324 16.98267
268.0145 15.39014
268.4966 16.08374
268.9788 15.87305
269.4609 12.53589
269.9430 6.660400
270.4251 0.5034180
270.9072 4.282959
271.3893 7.675049
271.8715 8.947998
272.3536 6.763916
272.8357 4.271973
273.3178 2.445801
273.7999 1.375977
274.2820 1.109375
274.7642 1.825684
275.2463 3.389893
275.7284 4.066406
276.2105 3.674316
276.6926 2.854736
277.1747 1.647217
277.6568 0.1755370
278.1389 1.389404
278.6211 3.012207
279.1032 4.579834
279.5853 5.551758
280.0674 5.158203
280.5495 5.200195
281.0316 6.872559
281.5138 9.207031
281.9959 10.29639
282.4780 9.185547
282.9601 6.843750
283.4422 5.799805
283.9243 6.387451
284.4065 7.372803
284.8886 8.922119
285.3707 10.62573
285.8528 11.59888
286.3349 11.42480
286.8170 11.23145
287.2992 13.18921
287.7813 18.03516
288.2634 22.29956
288.7455 25.09985
289.2276 27.16138
289.7097 29.26855
290.1919 31.59521
290.6740 34.06152
291.1561 36.76440
291.6382 39.81787
292.1203 41.99609
292.6024 42.82861
293.0846 42.91895
293.5667 42.53467
294.0488 41.73389
294.5309 41.33276
295.0130 42.40161
295.4951 44.92798
295.9773 46.22168
296.4594 45.13477
296.9415 43.53247
297.4236 42.91040
297.9057 43.26416
298.3878 43.61743
298.8700 43.22754
299.3521 42.22559
299.8342 41.63013
300.3163 42.27515
300.7984 42.56787
301.2805 41.11499
301.7627 38.31470
302.2448 36.00928
302.7269 35.27197
303.2090 35.62085
303.6911 35.52832
304.1732 34.95410
304.6554 34.10107
305.1375 33.35840
305.6196 32.44507
306.1017 30.34253
306.5838 26.26855
307.0659 21.60400
307.5481 19.41138
308.0302 20.36865
308.5123 20.57544
308.9944 18.72095
309.4765 15.32422
309.9586 10.55859
310.4408 3.989990
310.9229 1.777588
311.4050 1.996338
311.8871 3.546387
312.3692 6.894775
312.8513 4.163574
313.3335 0.5075680
313.8156 2.031738
314.2977 0.3842770
314.7798 4.070068
315.2619 7.226563
315.7440 9.687256
316.2262 10.19873
316.7083 7.048584
317.1904 3.033447
317.6725 2.1970000E-03
318.1546 1.931396
318.6367 2.357422
319.1188 0.4704590
319.6010 3.157471
320.0831 5.539307
320.5652 5.825928
321.0473 5.771484
321.5294 6.338135
322.0115 7.405029
322.4937 8.541748
322.9758 9.707275
323.4579 10.64624
323.9400 10.53247
324.4221 8.587646
324.9042 7.258057
325.3864 8.025879
325.8685 9.968018
326.3506 11.20435
326.8327 11.02393
327.3148 10.47485
327.7969 11.47852
328.2791 14.44312
328.7612 16.27539
329.2433 16.02954
329.7254 14.61377
330.2075 12.78418
330.6896 10.65356
331.1718 8.987549
331.6539 8.824219
332.1360 10.21362
332.6181 10.65503
333.1002 8.842041
333.5823 6.960449
334.0645 6.702637
334.5466 8.032715
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335.5108 11.78491
335.9929 13.53442
336.4750 14.75000
336.9572 14.79517
337.4393 15.12109
337.9214 17.12598
338.4035 19.64990
338.8856 20.18677
339.3677 17.39087
339.8499 12.96729
340.3320 11.11792
340.8141 12.96777
341.2962 14.22583
341.7783 13.88110
342.2604 12.91382
342.7426 12.29224
343.2247 12.18286
343.7068 12.43628
344.1889 13.02441
344.6710 14.14893
345.1531 15.11377
345.6353 15.80396
346.1174 16.58203
346.5995 17.98828
347.0816 19.82837
347.5637 21.02246
348.0458 20.52954
348.5280 18.25439
349.0101 16.77100
349.4922 16.79688
349.9743 16.89868
350.4564 16.27856
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351.4207 13.88403
351.9028 13.11230
352.3849 12.71167
352.8670 12.26685
353.3491 10.99780
353.8312 10.49463
354.3134 11.42651
354.7955 13.14746
355.2776 14.92017
355.7597 16.47534
356.2418 17.75732
356.7239 18.48120
357.2061 18.18506
357.6882 18.26172
358.1703 18.16113
358.6524 18.80298
359.1345 21.36768
359.6166 25.56519
360.0987 29.63184
360.5808 31.80835
361.0630 31.89893
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362.0272 30.93042
362.5093 30.65552
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363.4735 34.37378
363.9557 36.52075
364.4378 37.67529
364.9199 38.14185
365.4020 39.20923
365.8841 41.29175
366.3662 43.48047
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367.8126 50.43506
368.2947 50.73267
368.7768 49.76025
369.2589 47.55957
369.7411 43.94336
370.2232 39.78394
370.7053 34.77856
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371.6695 23.56055
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372.6338 12.69653
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374.5622 8.248779
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375.5265 6.134033
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376.9728 8.693848
377.4549 7.928955
377.9370 6.310791
378.4192 3.331543
378.9013 0.9589840
379.3834 5.6150001E-03
379.8655 0.3195800
380.3476 0.6010740
380.8297 0.9636230
381.3119 0.8945310
381.7940 0.3449710
382.2761 2.731689
382.7582 5.007080
383.2403 7.666260
383.7224 9.305908
384.2046 8.501709
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385.1688 3.691162
385.6509 3.209961
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387.5794 9.417236
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390.9542 6.017822
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391.9184 3.814941
392.4005 3.723145
392.8827 5.045898
393.3648 8.067383
393.8469 9.304199
394.3290 5.504883
394.8111 0.2998050
395.2932 2.796143
395.7754 0.9968260
396.2575 1.354492
396.7396 0.6071780
397.2217 2.855225
397.7038 4.394287
398.1859 1.673584
398.6681 1.139648
399.1501 0.8210450
399.6323 1.869629
400.1144 3.996094
400.5965 4.064453
401.0786 2.683594
401.5607 1.496582
402.0428 0.2507320
402.5250 0.3886720
403.0071 0.4040530
403.4892 1.558105
403.9713 1.771484
404.4534 0.7707520
404.9355 0.8037110
405.4177 2.367676
405.8998 4.156006
406.3819 4.482910
406.8640 1.785889
407.3461 0.6872560
407.8282 1.020508
408.3104 0.2128910
408.7925 1.266846
409.2746 1.013184
409.7567 0.1916500
410.2388 0.7165530
410.7209 0.3410640
411.2031 0.9316410
411.6852 0.1206050
412.1673 1.160645
412.6494 0.1186520
413.1315 3.323730
413.6136 7.166992
414.0958 8.646973
414.5779 7.167969
415.0600 5.728271
415.5421 3.380127
416.0242 1.997803
416.5063 2.674316
416.9885 4.955566
417.4706 7.742676
417.9527 10.48340
418.4348 13.09399
418.9169 15.09497
419.3990 15.74365
419.8812 17.46387
420.3633 22.22485
420.8454 27.65942
421.3275 31.70068
421.8096 33.85352
422.2917 34.64795
422.7739 33.88818
423.2560 31.70117
423.7381 30.90820
424.2202 32.38745
424.7023 34.75537
425.1844 37.80298
425.6666 40.99487
426.1487 42.31592
426.6308 38.79468
427.1129 33.87158
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