#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-04-26 14:03:32 +0300 (Thu, 26 Apr 2018) $
#$Revision: 639 $
#$URL: svn://172.16.1.111/rod/cif/1/00/01/1000173.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000173
loop_
_publ_author_name
'Zoppi, M.'
'Pratesi, G.'
_publ_section_title
;
 The dual behavior of the beta-As4S4 altered by light
;
_journal_name_full               'American Mineralogist'
_journal_page_first              890
_journal_page_last               896
_journal_paper_doi               10.2138/am.2012.3968
_journal_volume                  97
_journal_year                    2012
_chemical_compound_source        Synthetic
_chemical_formula_sum            'As8 S9'
_chemical_name_mineral           Alacranite
_space_group_IT_number           13
_symmetry_space_group_name_Hall  '-P 2yc'
_symmetry_space_group_name_H-M   'P 1 2/c 1'
_cell_angle_alpha                90
_cell_angle_beta                 102.397
_cell_angle_gamma                90
_cell_length_a                   9.9342
_cell_length_b                   9.5566
_cell_length_c                   9.1104
_cell_volume                     844.749
_exptl_crystal_density_diffrn    3.491
_cod_database_code               9016439
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type helium-neon
_raman_measurement_device.excitation_laser_wavelength 780
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 12
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R150030.rod
_rod_data_source.block           3500000
_rod_database.code               1000173
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9016439 COD http://www.crystallography.net/cod/9016439.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
107.4698 0.0000000E+00
107.9519 2.080078
108.4340 6.113281
108.9161 5.429688
109.3982 1.085938
109.8804 4.470703
110.3625 8.7890998E-02
110.8446 13.76172
111.3267 21.66602
111.8088 16.14844
112.2909 10.61719
112.7731 12.63672
113.2552 22.26562
113.7373 33.16211
114.2194 35.76562
114.7015 20.59180
115.1836 13.79688
115.6658 21.21484
116.1479 33.73047
116.6300 42.72656
117.1121 45.09570
117.5942 42.98438
118.0763 41.19141
118.5584 40.99414
119.0406 38.53711
119.5227 29.70508
120.0048 17.13672
120.4869 8.275391
120.9690 7.173828
121.4511 11.38281
121.9333 14.53906
122.4154 15.11523
122.8975 16.75781
123.3796 24.02148
123.8617 37.71680
124.3438 49.17578
124.8260 50.59766
125.3081 48.59375
125.7902 48.72461
126.2723 52.67773
126.7544 59.92969
127.2365 69.90820
127.7187 85.44727
128.2008 98.97266
128.6829 103.1934
129.1650 105.4395
129.6471 116.1445
130.1292 143.1191
130.6114 185.0449
131.0935 221.7598
131.5756 251.9863
132.0577 278.3477
132.5398 299.4473
133.0219 316.8691
133.5041 334.0117
133.9862 354.4297
134.4683 379.7324
134.9504 396.7637
135.4325 404.8496
135.9146 407.1660
136.3968 402.5371
136.8789 391.9180
137.3610 381.1914
137.8431 377.3789
138.3252 381.9746
138.8073 386.7148
139.2895 393.9395
139.7716 399.9492
140.2537 397.1621
140.7358 381.3145
141.2179 366.8887
141.7000 376.6582
142.1821 408.1562
142.6643 439.3027
143.1464 463.7832
143.6285 481.3379
144.1106 490.6367
144.5927 488.5996
145.0748 480.4551
145.5570 471.6172
146.0391 462.1816
146.5212 451.0996
147.0033 436.6484
147.4854 418.3672
147.9675 401.0820
148.4497 382.4141
148.9318 367.1191
149.4139 359.8711
149.8960 361.2969
150.3781 365.6699
150.8602 364.0625
151.3424 352.6016
151.8245 343.4668
152.3066 336.4590
152.7887 332.4902
153.2708 334.6211
153.7529 343.6016
154.2351 354.4062
154.7172 354.2930
155.1993 329.8477
155.6814 309.8008
156.1635 298.3711
156.6456 291.0977
157.1278 282.7852
157.6099 270.7891
158.0920 255.9902
158.5741 242.2676
159.0562 225.6055
159.5383 213.8828
160.0205 208.1211
160.5026 208.6562
160.9847 217.1797
161.4668 236.2832
161.9489 263.4531
162.4310 286.1094
162.9131 298.7734
163.3953 312.4355
163.8774 333.6465
164.3595 361.9570
164.8416 392.9492
165.3237 424.8555
165.8058 456.8945
166.2880 482.7969
166.7701 499.9004
167.2522 512.2441
167.7343 524.5508
168.2164 537.4961
168.6985 547.8652
169.1807 550.5391
169.6628 550.1992
170.1449 552.7246
170.6270 561.4121
171.1091 573.6172
171.5912 583.7852
172.0734 592.8965
172.5555 597.6328
173.0376 594.2070
173.5197 586.9961
174.0018 582.2773
174.4839 584.2871
174.9661 591.8555
175.4482 597.8223
175.9303 603.2734
176.4124 605.6387
176.8945 600.9883
177.3766 593.0781
177.8588 587.8477
178.3409 589.1895
178.8230 597.1465
179.3051 612.3145
179.7872 635.6133
180.2693 664.9824
180.7515 701.8613
181.2336 744.6797
181.7157 790.5039
182.1978 837.7949
182.6799 887.4883
183.1620 926.6191
183.6441 959.1035
184.1263 980.4355
184.6084 986.7676
185.0905 978.8750
185.5726 960.1953
186.0547 931.3242
186.5368 890.0137
187.0190 863.0410
187.5011 855.7910
187.9832 858.5703
188.4653 866.0742
188.9474 877.4668
189.4296 891.5117
189.9117 908.0938
190.3938 927.2480
190.8759 945.6641
191.3580 964.6758
191.8401 981.9023
192.3223 997.3965
192.8044 1012.531
193.2865 1016.852
193.7686 993.5918
194.2507 949.9707
194.7328 903.4961
195.2150 857.7168
195.6971 813.7285
196.1792 771.5039
196.6613 728.9551
197.1434 690.1172
197.6255 654.9727
198.1077 624.7871
198.5898 605.4512
199.0719 603.9980
199.5540 615.0645
200.0361 620.0020
200.5182 615.4160
201.0004 610.8984
201.4825 614.5332
201.9646 623.0840
202.4467 628.4473
202.9288 622.1230
203.4109 604.1562
203.8930 589.4102
204.3752 578.8535
204.8573 570.9141
205.3394 565.9062
205.8215 564.0195
206.3036 565.2910
206.7857 569.0684
207.2679 575.0332
207.7500 579.6328
208.2321 577.6387
208.7142 577.9062
209.1963 584.4023
209.6784 596.8789
210.1606 611.6133
210.6427 624.5938
211.1248 634.5234
211.6069 653.8535
212.0890 689.7949
212.5711 727.2988
213.0533 762.8594
213.5354 795.0879
214.0175 822.8262
214.4996 844.2793
214.9817 858.0449
215.4638 875.6973
215.9460 893.5117
216.4281 917.4043
216.9102 952.9648
217.3923 998.5156
217.8744 1047.254
218.3565 1093.412
218.8387 1136.838
219.3208 1176.088
219.8029 1210.133
220.2850 1241.553
220.7671 1277.627
221.2492 1316.012
221.7314 1340.656
222.2135 1335.549
222.6956 1297.662
223.1777 1261.586
223.6598 1227.188
224.1419 1194.557
224.6240 1162.361
225.1062 1130.818
225.5883 1104.691
226.0704 1088.191
226.5525 1081.605
227.0346 1080.205
227.5167 1083.564
227.9989 1092.215
228.4810 1109.682
228.9631 1136.436
229.4452 1161.682
229.9273 1178.162
230.4094 1186.674
230.8916 1189.643
231.3737 1189.785
231.8558 1183.119
232.3379 1164.170
232.8200 1132.102
233.3021 1093.385
233.7843 1047.070
234.2664 997.2441
234.7485 950.3359
235.2306 910.7109
235.7127 872.3359
236.1948 825.9277
236.6770 769.3574
237.1591 712.2695
237.6412 661.9961
238.1233 613.0645
238.6054 557.9238
239.0875 491.8262
239.5697 422.0586
240.0518 359.4746
240.5339 303.4512
241.0160 256.3457
241.4981 224.9277
241.9802 199.9277
242.4624 172.5684
242.9445 139.2910
243.4266 104.4570
243.9087 74.87305
244.3908 50.12305
244.8729 32.12305
245.3550 24.22070
245.8372 21.09570
246.3193 19.22656
246.8014 17.56250
247.2835 15.05273
247.7656 9.476563
248.2477 0.9238280
248.7299 10.36523
249.2120 19.08008
249.6941 25.88086
250.1762 28.84766
250.6583 27.52148
251.1404 24.63477
251.6226 24.28320
252.1047 25.59375
252.5868 31.67578
253.0689 49.17383
253.5510 66.47070
254.0331 74.11719
254.5153 70.19141
254.9974 61.22852
255.4795 58.01758
255.9616 66.76758
256.4437 67.22656
256.9258 50.41211
257.4080 32.87695
257.8901 25.12891
258.3722 29.15430
258.8543 40.28516
259.3364 53.53711
259.8185 73.60742
260.3007 83.12500
260.7828 78.93750
261.2649 69.25977
261.7470 55.74609
262.2291 40.44336
262.7112 28.64648
263.1934 27.31250
263.6755 41.33984
264.1576 48.08789
264.6397 47.29297
265.1218 41.19141
265.6039 28.35938
266.0861 10.44141
266.5682 7.492188
267.0503 20.49805
267.5324 27.76758
268.0145 34.31836
268.4966 37.33594
268.9788 42.23633
269.4609 53.04492
269.9430 68.58203
270.4251 84.02148
270.9072 95.14062
271.3893 101.5840
271.8715 111.9785
272.3536 129.4668
272.8357 146.8613
273.3178 163.8262
273.7999 178.5059
274.2820 186.5762
274.7642 184.6934
275.2463 173.4590
275.7284 159.9102
276.2105 139.3359
276.6926 121.8965
277.1747 112.2773
277.6568 108.3281
278.1389 104.7734
278.6211 98.48242
279.1032 90.88086
279.5853 88.64844
280.0674 93.00391
280.5495 100.0312
281.0316 112.2812
281.5138 126.2305
281.9959 134.9023
282.4780 134.8203
282.9601 129.5723
283.4422 128.1758
283.9243 131.2559
284.4065 136.3125
284.8886 142.9785
285.3707 151.3457
285.8528 161.2051
286.3349 172.3672
286.8170 185.9434
287.2992 204.5098
287.7813 228.7598
288.2634 254.7246
288.7455 285.9492
289.2276 316.7773
289.7097 338.4180
290.1919 348.6133
290.6740 355.4648
291.1561 368.0469
291.6382 386.4727
292.1203 410.6348
292.6024 445.1387
293.0846 482.7578
293.5667 515.7051
294.0488 543.1836
294.5309 570.5957
295.0130 603.3457
295.4951 641.5586
295.9773 678.3711
296.4594 708.9824
296.9415 741.2734
297.4236 784.0547
297.9057 836.3398
298.3878 886.7734
298.8700 926.5898
299.3521 957.1426
299.8342 991.0098
300.3163 1028.307
300.7984 1068.271
301.2805 1111.570
301.7627 1157.617
302.2448 1204.846
302.7269 1253.566
303.2090 1302.396
303.6911 1347.738
304.1732 1388.889
304.6554 1428.811
305.1375 1468.719
305.6196 1508.396
306.1017 1547.332
306.5838 1585.895
307.0659 1623.287
307.5481 1656.453
308.0302 1683.693
308.5123 1715.297
308.9944 1759.029
309.4765 1808.250
309.9586 1850.594
310.4408 1881.752
310.9229 1907.475
311.4050 1934.256
311.8871 1962.193
312.3692 1996.305
312.8513 2043.328
313.3335 2094.186
313.8156 2138.455
314.2977 2175.006
314.7798 2208.156
315.2619 2240.277
315.7440 2270.734
316.2262 2299.523
316.7083 2319.615
317.1904 2342.070
317.6725 2380.035
318.1546 2433.189
318.6367 2483.008
319.1188 2515.484
319.6010 2534.436
320.0831 2561.125
320.5652 2602.484
321.0473 2643.605
321.5294 2673.229
322.0115 2694.947
322.4937 2721.541
322.9758 2760.186
323.4579 2806.441
323.9400 2846.748
324.4221 2878.023
324.9042 2910.734
325.3864 2951.562
325.8685 2996.137
326.3506 3036.809
326.8327 3071.406
327.3148 3101.135
327.7969 3127.160
328.2791 3149.363
328.7612 3170.240
329.2433 3192.445
329.7254 3212.527
330.2075 3224.125
330.6896 3226.123
331.1718 3228.154
331.6539 3239.777
332.1360 3261.975
332.6181 3286.363
333.1002 3317.166
333.5823 3346.535
334.0645 3364.783
334.5466 3373.701
335.0287 3388.717
335.5108 3422.223
335.9929 3471.195
336.4750 3510.977
336.9572 3536.748
337.4393 3559.863
337.9214 3583.162
338.4035 3607.377
338.8856 3634.912
339.3677 3667.775
339.8499 3702.357
340.3320 3728.381
340.8141 3743.355
341.2962 3755.689
341.7783 3769.193
342.2604 3780.113
342.7426 3783.586
343.2247 3778.268
343.7068 3765.719
344.1889 3748.361
344.6710 3726.887
345.1531 3695.818
345.6353 3650.162
346.1174 3598.736
346.5995 3547.580
347.0816 3497.775
347.5637 3446.832
348.0458 3392.209
348.5280 3333.316
349.0101 3283.225
349.4922 3240.094
349.9743 3205.916
350.4564 3185.807
350.9385 3175.832
351.4207 3167.266
351.9028 3155.094
352.3849 3140.650
352.8670 3129.529
353.3491 3125.256
353.8312 3120.744
354.3134 3119.400
354.7955 3114.820
355.2776 3101.484
355.7597 3077.799
356.2418 3043.145
356.7239 2993.814
357.2061 2916.355
357.6882 2847.857
358.1703 2786.305
358.6524 2735.211
359.1345 2701.318
359.6166 2682.092
360.0987 2665.854
360.5808 2640.363
361.0630 2603.535
361.5451 2575.908
362.0272 2575.672
362.5093 2563.857
362.9914 2519.236
363.4735 2454.131
363.9557 2393.430
364.4378 2352.500
364.9199 2327.184
365.4020 2299.146
365.8841 2266.896
366.3662 2233.340
366.8484 2194.830
367.3305 2158.297
367.8126 2132.643
368.2947 2119.828
368.7768 2109.861
369.2589 2086.475
369.7411 2044.328
370.2232 2003.100
370.7053 1961.441
371.1874 1922.252
371.6695 1886.094
372.1516 1853.520
372.6338 1825.043
373.1159 1802.791
373.5980 1786.449
374.0801 1765.131
374.5622 1735.494
375.0443 1704.398
375.5265 1673.197
376.0086 1642.279
376.4907 1612.387
376.9728 1583.736
377.4549 1556.152
377.9370 1528.477
378.4192 1499.186
378.9013 1474.285
379.3834 1460.143
379.8655 1448.133
380.3476 1432.699
380.8297 1412.688
381.3119 1387.734
381.7940 1353.506
382.2761 1310.328
382.7582 1278.176
383.2403 1267.133
383.7224 1259.225
384.2046 1242.074
384.6867 1217.553
385.1688 1192.264
385.6509 1171.230
386.1330 1151.836
386.6151 1126.818
387.0973 1094.443
387.5794 1062.729
388.0615 1037.904
388.5436 1015.838
389.0257 990.4492
389.5078 959.1270
389.9900 926.6035
390.4721 896.5625
390.9542 868.7129
391.4363 841.9785
391.9184 814.9609
392.4005 790.3301
392.8827 773.8105
393.3648 766.4863
393.8469 753.9883
394.3290 729.5664
394.8111 697.0684
395.2932 660.6504
395.7754 620.0625
396.2575 582.6270
396.7396 556.5664
397.2217 540.8691
397.7038 520.1445
398.1859 489.4355
398.6681 457.1602
399.1501 427.9082
399.6323 401.5508
400.1144 376.6523
400.5965 352.0898
401.0786 329.1621
401.5607 312.9980
402.0428 309.3438
402.5250 301.0645
403.0071 283.3379
403.4892 260.1445
403.9713 235.0391
404.4534 209.2012
404.9355 183.7637
405.4177 160.1973
405.8998 139.0762
406.3819 117.8340
406.8640 94.95508
407.3461 73.54883
407.8282 53.28125
408.3104 35.65625
408.7925 24.98047
409.2746 24.70898
409.7567 31.26953
410.2388 27.90625
410.7209 1.277344
411.2031 18.18164
411.6852 20.71875
412.1673 19.08398
412.6494 27.82031
413.1315 49.65625
413.6136 72.99609
414.0958 80.82031
414.5779 67.63477
415.0600 61.09961
415.5421 66.92578
416.0242 74.21484
416.5063 79.56445
416.9885 82.96289
417.4706 85.68945
417.9527 89.39062
418.4348 92.25000
418.9169 87.22266
419.3990 70.66406
419.8812 54.19336
420.3633 38.93750
420.8454 26.73633
421.3275 20.97461
421.8096 22.73828
422.2917 25.48828
422.7739 21.11523
423.2560 10.23047
423.7381 4.527344
424.2202 10.08398
424.7023 15.44141
425.1844 10.78516
425.6666 1.468750
426.1487 12.70117
426.6308 18.19141
427.1129 21.09766
427.5950 25.48633
428.0771 31.36328
428.5593 40.04492
429.0414 55.95117
429.5235 73.12305
430.0056 78.54883
430.4877 66.88086
430.9698 55.85547
431.4520 56.59375
431.9341 63.94922
432.4162 67.12891
432.8983 63.22461
433.3804 56.95117
433.8625 53.28711
434.3447 52.47656
434.8268 53.29688
435.3089 54.49219
435.7910 58.24023
436.2731 69.63281
436.7552 85.49805
437.2374 95.20117
437.7195 91.82812
438.2016 79.05859
438.6837 71.05078
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1284.798 0.0000000E+00
