#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-04-26 14:07:27 +0300 (Thu, 26 Apr 2018) $
#$Revision: 650 $
#$URL: svn://172.16.1.111/rod/cif/1/00/01/1000183.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000183
loop_
_publ_author_name
'Andrade, M. B.'
'Atencio, D.'
'Menezes, L. A. D.'
'Ellena, J.'
_publ_section_title
;
 The crystal structure of a microlite-group mineral with a formula near
 NaCaTa2O6F from the Morro Redondo mine, Coronel Murta, Minas Gerias,
 Brazil
;
_journal_name_full               'The Canadian Mineralogist'
_journal_page_first              615
_journal_page_last               621
_journal_paper_doi               10.3749/canmin.49.2.615
_journal_volume                  49
_journal_year                    2011
_chemical_compound_source        R130019
_chemical_formula_sum
'As0.04 Ca0.88 F0.73 H0.24 Na0.88 Nb0.14 O6 Pb0.02 Si0.12 Ta1.7'
_chemical_name_mineral           Fluornatromicrolite
_space_group_IT_number           227
_symmetry_space_group_name_Hall  '-F 4vw 2vw 3'
_symmetry_space_group_name_H-M   'F d -3 m :2'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_length_a                   10.4396
_cell_length_b                   10.4396
_cell_length_c                   10.4396
_cell_volume                     1137.762
_exptl_crystal_density_diffrn    5.800
_cod_original_sg_symbol_H-M      'F d 3 m'
_cod_original_formula_sum
'Na.88 Ca.88 Pb.02 (Ta1.7 Nb.14 Si.12 As.04) O6 F.73 H.24'
_cod_database_code               9014190
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type helium-neon
_raman_measurement_device.excitation_laser_wavelength 780
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 12
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R130019.rod
_rod_data_source.block           3500000
_rod_database.code               1000183
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9014190 COD http://www.crystallography.net/cod/9014190.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
96.98498 0.0000000E+00
97.46709 1.152832
97.94921 2.344238
98.43133 1.216797
98.91344 0.1074220
99.39556 0.7041020
99.87768 0.7355960
100.3598 0.1679690
100.8419 1.932373
101.3240 4.798584
101.8061 9.059082
102.2883 15.63501
102.7704 22.59155
103.2525 27.82959
103.7346 30.90405
104.2167 33.89624
104.6988 37.69922
105.1810 41.69678
105.6631 45.05298
106.1452 46.88354
106.6273 47.60352
107.1094 49.13281
107.5915 51.85352
108.0737 54.77246
108.5558 57.28784
109.0379 59.56714
109.5200 62.10327
110.0021 65.49854
110.4842 70.04565
110.9664 73.87012
111.4485 76.19165
111.9306 78.51172
112.4127 81.82007
112.8948 86.09326
113.3769 90.38574
113.8591 93.31812
114.3412 93.87744
114.8233 94.64258
115.3054 95.54688
115.7875 96.61670
116.2696 98.00098
116.7517 99.75415
117.2339 101.5322
117.7160 102.3774
118.1981 101.6038
118.6802 101.3667
119.1623 102.7378
119.6444 105.1753
120.1266 107.2065
120.6087 108.1787
121.0908 108.2375
121.5729 107.9683
122.0550 107.2500
122.5371 106.3926
123.0193 105.6384
123.5014 104.9585
123.9835 104.4224
124.4656 104.3008
124.9477 104.3232
125.4298 104.0784
125.9120 103.2170
126.3941 102.3228
126.8762 103.0886
127.3583 107.0303
127.8404 110.1077
128.3225 111.1316
128.8047 110.7312
129.2868 109.6956
129.7689 108.4558
130.2510 107.0156
130.7331 105.5161
131.2152 103.6230
131.6974 101.9585
132.1795 100.5208
132.6616 99.41724
133.1437 98.88208
133.6258 99.10938
134.1079 100.1611
134.5901 101.6748
135.0722 104.4968
135.5543 107.0266
136.0364 107.9868
136.5185 107.4094
137.0006 106.6785
137.4828 107.5254
137.9649 110.3787
138.4470 112.6689
138.9291 114.0452
139.4112 114.8796
139.8933 115.4753
140.3755 115.8667
140.8576 116.4128
141.3397 117.4248
141.8218 118.7886
142.3039 120.8079
142.7860 123.8628
143.2681 127.6729
143.7503 131.4561
144.2324 135.6177
144.7145 139.1946
145.1966 140.8755
145.6787 140.7329
146.1608 140.8950
146.6430 143.7983
147.1251 150.0576
147.6072 155.6606
148.0893 158.4595
148.5714 160.5703
149.0535 163.3792
149.5357 167.0444
150.0178 170.8340
150.4999 173.5891
150.9820 174.5024
151.4641 175.9321
151.9462 179.3435
152.4284 183.8267
152.9105 187.5979
153.3926 190.1033
153.8747 192.3843
154.3568 195.3762
154.8389 197.9966
155.3211 200.4934
155.8032 203.4275
156.2853 206.1965
156.7674 207.9165
157.2495 208.0583
157.7316 207.0183
158.2138 206.3884
158.6959 206.6628
159.1780 206.6335
159.6601 205.6658
160.1422 204.1017
160.6243 202.7482
161.1065 202.1147
161.5886 202.0511
162.0707 202.0232
162.5528 203.2599
163.0349 203.4298
163.5170 200.7313
163.9991 195.4492
164.4813 190.0441
164.9634 186.1528
165.4455 183.1339
165.9276 179.5026
166.4097 174.5684
166.8918 169.3182
167.3740 165.1674
167.8561 162.4481
168.3382 159.3214
168.8203 153.7202
169.3024 147.3284
169.7845 142.3162
170.2667 140.1912
170.7488 139.5708
171.2309 137.2450
171.7130 132.5704
172.1951 127.2405
172.6772 121.2467
173.1594 115.2118
173.6415 109.9839
174.1236 106.1451
174.6057 103.5593
175.0878 101.4669
175.5699 100.5544
176.0521 99.40039
176.5342 98.09009
177.0163 96.27319
177.4984 93.28479
177.9805 88.35095
178.4626 81.42639
178.9448 76.48425
179.4269 75.05725
179.9090 74.06555
180.3911 72.76270
180.8732 71.14478
181.3553 69.60669
181.8375 68.54236
182.3196 68.07654
182.8017 66.66516
183.2838 63.82288
183.7659 60.67358
184.2480 57.42615
184.7301 54.26318
185.2123 51.72766
185.6944 50.55554
186.1765 51.03052
186.6586 50.14648
187.1407 46.77344
187.6228 42.93811
188.1050 39.84949
188.5871 37.70557
189.0692 36.60327
189.5513 37.43359
190.0334 40.05872
190.5155 40.37878
190.9977 36.02148
191.4798 30.05725
191.9619 26.03076
192.4440 24.55945
192.9261 23.82849
193.4082 21.88281
193.8904 19.16980
194.3725 17.23291
194.8546 17.49866
195.3367 18.69250
195.8188 18.07129
196.3009 14.78540
196.7831 11.05347
197.2652 8.138428
197.7473 5.982788
198.2294 4.738525
198.7115 4.952637
199.1936 6.242798
199.6758 6.953613
200.1579 6.661255
200.6400 6.285889
201.1221 6.413086
201.6042 6.869385
202.0863 7.256470
202.5685 7.337036
203.0506 7.108398
203.5327 6.591797
204.0148 5.200684
204.4969 4.162720
204.9790 4.636353
205.4612 5.930664
205.9433 6.345215
206.4254 4.136963
206.9075 0.9024660
207.3896 4.507813
207.8717 5.659668
208.3539 6.217407
208.8360 6.126587
209.3181 5.808960
209.8002 6.162598
210.2823 8.267334
210.7644 12.53406
211.2466 14.56335
211.7287 12.04968
212.2108 9.657471
212.6929 9.410278
213.1750 11.03479
213.6571 13.03284
214.1393 14.01428
214.6214 13.76331
215.1035 13.99902
215.5856 15.33521
216.0677 16.51086
216.5498 16.85132
217.0320 16.40076
217.5141 15.72241
217.9962 15.39612
218.4783 15.52954
218.9604 14.58679
219.4425 11.71191
219.9247 8.604248
220.4068 6.022095
220.8889 4.099976
221.3710 3.047485
221.8531 3.366211
222.3352 5.129883
222.8174 5.481079
223.2995 3.984253
223.7816 1.442139
224.2637 2.203613
224.7458 6.816528
225.2279 10.71912
225.7100 12.24988
226.1922 11.63965
226.6743 11.43030
227.1564 11.56470
227.6385 12.29602
228.1206 14.06543
228.6027 16.91821
229.0849 20.06616
229.5670 23.11072
230.0491 26.01428
230.5312 28.66956
231.0133 30.56824
231.4954 32.48389
231.9776 35.46045
232.4597 39.64343
232.9418 43.86902
233.4239 47.43103
233.9060 50.55225
234.3881 53.47827
234.8703 55.91296
235.3524 58.47388
235.8345 62.22766
236.3166 67.50659
236.7987 72.62878
237.2808 77.41711
237.7630 81.35706
238.2451 83.53748
238.7272 83.21643
239.2093 81.68396
239.6914 80.77112
240.1735 80.34216
240.6557 80.99609
241.1378 83.58325
241.6199 87.03894
242.1020 90.47998
242.5841 93.62488
243.0662 96.58545
243.5484 99.53430
244.0305 102.4794
244.5126 105.4255
244.9947 108.2590
245.4768 111.1315
245.9589 114.2988
246.4410 117.8832
246.9232 121.4583
247.4053 124.2677
247.8874 126.0139
248.3695 127.6768
248.8516 129.2181
249.3337 130.8271
249.8159 132.6901
250.2980 134.8662
250.7801 137.2201
251.2622 139.6537
251.7443 142.6259
252.2264 144.5065
252.7086 144.1233
253.1907 143.4966
253.6728 144.0275
254.1549 146.0353
254.6370 148.8580
255.1191 151.4875
255.6013 153.4631
256.0834 156.3618
256.5655 160.7721
257.0476 165.6545
257.5297 170.6385
258.0118 175.4535
258.4940 179.6599
258.9761 182.5299
259.4582 183.1798
259.9403 184.7791
260.4224 187.9912
260.9045 191.4174
261.3867 193.9089
261.8688 195.4911
262.3509 197.3007
262.8330 200.8657
263.3151 207.0780
263.7972 211.8596
264.2794 214.0522
264.7615 215.7096
265.2436 218.1450
265.7257 221.5022
266.2078 224.9902
266.6899 227.7494
267.1721 229.4994
267.6542 232.4801
268.1363 237.6823
268.6184 242.6060
269.1005 246.2661
269.5826 248.9933
270.0648 251.3535
270.5469 253.6436
271.0290 255.7307
271.5111 257.6508
271.9932 259.1169
272.4753 260.8942
272.9575 263.1096
273.4396 265.7555
273.9217 269.0872
274.4038 273.5142
274.8859 278.9001
275.3680 282.7494
275.8501 283.5833
276.3322 284.8252
276.8144 287.9514
277.2965 292.5707
277.7786 297.6760
278.2607 302.8707
278.7428 307.7917
279.2249 310.8311
279.7071 309.5482
280.1892 309.3755
280.6713 312.6317
281.1534 318.0316
281.6355 323.2157
282.1176 327.0977
282.5998 329.9991
283.0819 332.8225
283.5640 335.5286
284.0461 338.2325
284.5282 340.7830
285.0103 343.4025
285.4925 346.4508
285.9746 350.0760
286.4567 354.0674
286.9388 358.1473
287.4209 362.3873
287.9030 366.4574
288.3852 370.0988
288.8673 373.6057
289.3494 377.6615
289.8315 382.4642
290.3136 386.7200
290.7957 388.5754
291.2779 387.6738
291.7600 386.9965
292.2421 387.0156
292.7242 387.2731
293.2063 387.2709
293.6884 386.9429
294.1706 386.7037
294.6527 387.1250
295.1348 388.1768
295.6169 388.3130
296.0990 386.6516
296.5811 384.6635
297.0633 383.8181
297.5454 384.0378
298.0275 383.6796
298.5096 381.5216
298.9917 377.7026
299.4738 373.8929
299.9560 369.7471
300.4381 365.9583
300.9202 363.0591
301.4023 360.9080
301.8844 358.8469
302.3665 356.6836
302.8487 354.2065
303.3308 350.8613
303.8129 346.3347
304.2950 341.5253
304.7771 336.4806
305.2592 331.4259
305.7414 327.2786
306.2235 324.8646
306.7056 322.6282
307.1877 317.2362
307.6698 308.1298
308.1519 299.0778
308.6341 291.2203
309.1162 284.2333
309.5983 277.8979
310.0804 272.3434
310.5625 266.7533
311.0446 259.6239
311.5268 250.7911
312.0089 243.4452
312.4910 239.0494
312.9731 236.0865
313.4552 232.8448
313.9373 229.0966
314.4195 225.1274
314.9016 221.3984
315.3837 217.7668
315.8658 212.8865
316.3479 205.4833
316.8300 197.6078
317.3121 190.8108
317.7943 185.1127
318.2764 180.1558
318.7585 175.7852
319.2406 172.0240
319.7227 168.5619
320.2048 165.8126
320.6870 162.9290
321.1691 158.8912
321.6512 154.2026
322.1333 150.7683
322.6154 149.9510
323.0975 150.4207
323.5797 148.7413
324.0618 144.0114
324.5439 139.5186
325.0260 136.3910
325.5081 134.2833
325.9902 132.5730
326.4724 131.1160
326.9545 129.8104
327.4366 128.3608
327.9187 126.5702
328.4008 125.6208
328.8829 126.9628
329.3651 128.6957
329.8472 128.1152
330.3293 124.7476
330.8114 121.2197
331.2935 120.3076
331.7756 122.2706
332.2578 123.4160
332.7399 123.0073
333.2220 122.2222
333.7041 121.3777
334.1862 120.7218
334.6683 121.5009
335.1505 125.2152
335.6326 131.1201
336.1147 133.8993
336.5968 131.8851
337.0789 128.9406
337.5610 126.3987
338.0432 124.1993
338.5253 122.1296
339.0074 120.0554
339.4895 117.8948
339.9716 115.5580
340.4537 112.7288
340.9359 110.3374
341.4180 108.7277
341.9001 107.6028
342.3822 106.7783
342.8643 106.2184
343.3464 105.5415
343.8286 104.2227
344.3107 102.0979
344.7928 99.62927
345.2749 96.08447
345.7570 92.71143
346.2391 90.62683
346.7213 89.83728
347.2034 89.44006
347.6855 88.78210
348.1676 87.84192
348.6497 86.13538
349.1318 83.20129
349.6140 80.30566
350.0961 77.94458
350.5782 76.02319
351.0603 74.27124
351.5424 72.56848
352.0245 70.91443
352.5067 69.28894
352.9888 67.76514
353.4709 66.14502
353.9530 63.63330
354.4351 61.38599
354.9172 61.20325
355.3994 63.63660
355.8815 66.86023
356.3636 67.69055
356.8457 64.48962
357.3278 61.91248
357.8099 60.34814
358.2920 59.08337
358.7741 57.77283
359.2563 56.33691
359.7384 54.81702
360.2205 53.19360
360.7026 51.43518
361.1847 49.68311
361.6668 47.66235
362.1490 45.97607
362.6311 45.00098
363.1132 44.39917
363.5953 43.64941
364.0774 42.42566
364.5595 40.89636
365.0417 39.72095
365.5238 39.41821
366.0059 38.77405
366.4880 36.91626
366.9701 34.86365
367.4522 33.81323
367.9344 34.17786
368.4165 35.26477
368.8986 36.02759
369.3807 36.50610
369.8628 36.43140
370.3449 36.09656
370.8271 35.06995
371.3092 32.56311
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372.2734 25.22546
372.7555 22.55847
373.2376 20.88062
373.7198 19.68274
374.2019 19.26074
374.6840 19.03174
375.1661 19.03430
375.6482 19.06116
376.1303 18.88647
376.6125 18.46216
377.0946 17.70215
377.5767 16.08679
378.0588 12.89612
378.5409 10.94714
379.0230 11.92700
379.5052 13.91235
379.9873 15.78760
380.4694 17.30713
380.9515 18.01697
381.4336 17.19824
381.9157 14.85461
382.3979 12.50366
382.8800 9.928345
383.3621 7.885864
383.8442 7.021729
384.3263 7.102783
384.8084 7.168213
385.2906 6.556396
385.7727 5.635254
386.2548 5.331177
386.7369 5.846069
387.2190 6.268799
387.7011 6.064209
388.1833 5.439819
388.6654 4.594360
389.1475 3.409424
389.6296 2.305298
390.1117 1.606628
390.5938 1.303589
391.0760 1.361633
391.5581 1.785034
392.0402 2.535034
392.5223 3.902710
393.0044 6.055908
393.4865 7.083679
393.9687 5.818665
394.4508 3.129089
394.9329 2.2887999E-02
395.4150 3.531738
395.8971 6.339355
396.3792 7.146667
396.8614 6.008667
397.3435 4.829712
397.8256 3.582275
398.3077 2.370361
398.7898 1.098755
399.2719 4.6997000E-02
399.7540 0.5026860
400.2361 4.6875000E-02
400.7183 1.318848
401.2004 2.586853
401.6825 3.987671
402.1646 5.038025
402.6467 5.636108
403.1288 5.864685
403.6110 5.769592
404.0931 5.372620
404.5752 4.720093
405.0573 3.693787
405.5394 1.905640
406.0215 1.608337
406.5037 4.012390
406.9858 6.487915
407.4679 7.917725
407.9500 8.396057
408.4321 8.410156
408.9142 8.251892
409.3964 7.877991
409.8785 7.251526
410.3606 5.979431
410.8427 5.088135
411.3248 4.930115
411.8069 5.122314
412.2891 5.430603
412.7712 5.731628
413.2533 5.798401
413.7354 5.230225
414.2175 3.766357
414.6996 2.596497
415.1818 1.701416
415.6639 1.173401
416.1460 1.245178
416.6281 1.715881
417.1102 2.108765
417.5923 2.101624
418.0745 1.773804
418.5566 1.604065
419.0387 1.907837
419.5208 1.818298
420.0029 0.5429080
420.4850 0.9431150
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