#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-05-24 15:07:55 +0300 (Thu, 24 May 2018) $
#$Revision: 652 $
#$URL: svn://172.16.1.111/rod/cif/1/00/01/1000184.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000184
loop_
_publ_author_name
'Ghose, S.'
'Sen Gupta, P. K.'
'Schlemper, E. O.'
_publ_section_title
;
 Leiteite, ZnAs2O4: A novel type of tetrahedral layer structure with
 arsenite chains
;
_journal_name_full               'American Mineralogist'
_journal_page_first              629
_journal_page_last               632
_journal_volume                  72
_journal_year                    1987
_chemical_compound_source        R040011
_chemical_formula_sum            'As2 O4 Zn'
_chemical_name_mineral           Leiteite
_space_group_IT_number           14
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90
_cell_angle_beta                 90.81
_cell_angle_gamma                90
_cell_length_a                   4.542
_cell_length_b                   5.022
_cell_length_c                   17.597
_cell_volume                     401.346
_exptl_crystal_density_diffrn    4.621
_cod_original_formula_sum        'As2 Zn O4'
_cod_database_code               9001071
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 15
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R040011.rod
_rod_data_source.block           3500000
_rod_database.code               1000184
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9001071 COD http://www.crystallography.net/cod/9001071.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
118.9584 0.0000000E+00
119.4405 0.9224850
119.9227 11.54602
120.4048 22.31006
120.8869 30.30542
121.3690 39.85266
121.8511 51.23993
122.3332 65.53998
122.8154 85.49811
123.2975 119.6083
123.7796 156.6512
124.2617 187.5533
124.7438 212.3287
125.2259 224.7547
125.7081 213.6777
126.1902 182.3079
126.6723 142.2065
127.1544 99.59656
127.6365 61.04803
128.1186 31.50098
128.6008 12.94647
129.0829 2.637085
129.5650 1.204773
130.0471 1.055847
130.5292 4.577637
131.0113 5.554077
131.4935 4.461182
131.9756 3.132385
132.4577 1.444336
132.9398 4.9805000E-02
133.4219 0.4619140
133.9040 2.526550
134.3862 7.028259
134.8683 15.41229
135.3504 27.61267
135.8325 40.41278
136.3146 53.27051
136.7967 66.01678
137.2789 77.28522
137.7610 87.07196
138.2431 97.01929
138.7252 106.9470
139.2073 116.0377
139.6894 126.5863
140.1716 138.6738
140.6537 151.9756
141.1358 169.9515
141.6179 192.6719
142.1000 220.2053
142.5821 251.6767
143.0643 285.8093
143.5464 326.9208
144.0285 376.5939
144.5106 432.5640
144.9927 502.2703
145.4748 587.3640
145.9570 685.2801
146.4391 785.9388
146.9212 896.7119
147.4033 1002.618
147.8854 1100.221
148.3675 1212.187
148.8497 1280.071
149.3318 1304.360
149.8139 1284.554
150.2960 1212.398
150.7781 1049.105
151.2602 862.4250
151.7424 690.3966
152.2245 522.4407
152.7066 380.1851
153.1887 268.7094
153.6708 187.7857
154.1529 122.8196
154.6351 76.65643
155.1172 43.16663
155.5993 18.12939
156.0814 4.342468
156.5635 4.871948
157.0456 10.24866
157.5278 11.79102
158.0099 11.00732
158.4920 7.680725
158.9741 2.392883
159.4562 4.338684
159.9383 13.68207
160.4205 23.28522
160.9026 31.99506
161.3847 39.65625
161.8668 48.48468
162.3489 56.10370
162.8310 66.20062
163.3132 83.07318
163.7953 111.8931
164.2774 144.9225
164.7595 179.0219
165.2416 214.2661
165.7237 248.9088
166.2059 288.7853
166.6880 326.8703
167.1701 352.4596
167.6522 361.5876
168.1343 356.2926
168.6164 335.5434
169.0985 296.9531
169.5807 253.1656
170.0628 207.4249
170.5449 162.4640
171.0270 124.0911
171.5091 96.17810
171.9912 75.70569
172.4734 59.99115
172.9555 48.93726
173.4376 44.47815
173.9197 46.09930
174.4018 52.27136
174.8839 61.74738
175.3661 75.21765
175.8482 90.61963
176.3303 106.7275
176.8124 124.2270
177.2945 142.4994
177.7766 162.7264
178.2588 183.4794
178.7409 198.0155
179.2230 203.4528
179.7051 199.7489
180.1872 185.4193
180.6693 157.1746
181.1515 123.6891
181.6336 94.75043
182.1157 70.49152
182.5978 52.03296
183.0799 40.66077
183.5620 35.54968
184.0442 34.95215
184.5263 39.32391
185.0084 46.88110
185.4905 54.21228
185.9726 61.40051
186.4547 71.18567
186.9369 87.53741
187.4190 108.9204
187.9011 128.4377
188.3832 145.2514
188.8653 159.1241
189.3474 171.1308
189.8296 181.5656
190.3117 185.4807
190.7938 176.2378
191.2759 155.3073
191.7580 133.7499
192.2401 112.4960
192.7223 92.83765
193.2044 77.80743
193.6865 67.15558
194.1686 61.86713
194.6507 62.63037
195.1328 69.35706
195.6150 82.28760
196.0971 101.5298
196.5792 126.9336
197.0613 158.1807
197.5434 195.2252
198.0255 237.7528
198.5077 287.9667
198.9898 346.6702
199.4719 398.4727
199.9540 440.4294
200.4361 472.4916
200.9182 493.5401
201.4004 501.5889
201.8825 504.2802
202.3646 508.0306
202.8467 512.5974
203.3288 520.2717
203.8109 532.8043
204.2931 549.3682
204.7752 562.9935
205.2573 573.6021
205.7394 581.5051
206.2215 586.3297
206.7036 587.3810
207.1858 588.6241
207.6679 590.0209
208.1500 591.8711
208.6321 598.5595
209.1142 609.6065
209.5963 626.3427
210.0785 650.0632
210.5606 680.4963
211.0427 718.2247
211.5248 762.5902
212.0069 813.7083
212.4890 877.2860
212.9712 953.7155
213.4533 1042.383
213.9354 1139.756
214.4175 1243.115
214.8996 1365.532
215.3817 1511.499
215.8639 1679.773
216.3460 1875.385
216.8281 2122.872
217.3102 2365.928
217.7923 2548.345
218.2744 2684.015
218.7565 2726.357
219.2387 2657.461
219.7208 2476.321
220.2029 2231.448
220.6850 1897.294
221.1671 1532.190
221.6492 1199.291
222.1314 887.1693
222.6135 626.8228
223.0956 434.9130
223.5777 310.4620
224.0598 213.5422
224.5419 149.5880
225.0241 106.0988
225.5062 69.85071
225.9883 42.30334
226.4704 19.52997
226.9525 1.497253
227.4346 11.99054
227.9168 22.29443
228.3989 29.15466
228.8810 33.13574
229.3631 34.51471
229.8452 32.50311
230.3273 29.49866
230.8095 26.14117
231.2916 22.49329
231.7737 17.08319
232.2558 10.01312
232.7379 1.083496
233.2200 9.400696
233.7022 19.47382
234.1843 34.95148
234.6664 57.62408
235.1485 87.35052
235.6306 119.6251
236.1127 156.8655
236.5949 194.5897
237.0770 229.0214
237.5591 260.4976
238.0412 287.8593
238.5233 310.0370
239.0054 327.1066
239.4876 342.8234
239.9697 355.3879
240.4518 368.6785
240.9339 386.4766
241.4160 411.3483
241.8981 435.5380
242.3803 457.0519
242.8624 476.1146
243.3445 497.2645
243.8266 520.4528
244.3087 545.9358
244.7908 573.9925
245.2730 605.0153
245.7551 637.7445
246.2372 671.6228
246.7193 706.7883
247.2014 745.0967
247.6835 784.4650
248.1657 829.0710
248.6478 881.3146
249.1299 941.7380
249.6120 1008.754
250.0941 1079.850
250.5762 1156.391
251.0584 1250.022
251.5405 1360.986
252.0226 1487.629
252.5047 1628.002
252.9868 1785.934
253.4689 1952.597
253.9511 2139.457
254.4332 2337.610
254.9153 2497.740
255.3974 2638.905
255.8795 2713.535
256.3616 2685.188
256.8438 2527.716
257.3259 2332.708
257.8080 2088.375
258.2901 1813.612
258.7722 1571.987
259.2543 1363.615
259.7365 1187.022
260.2186 1039.249
260.7007 926.4142
261.1828 828.5629
261.6649 746.1376
262.1470 677.9387
262.6292 617.9767
263.1113 566.7444
263.5934 523.4711
264.0755 488.3153
264.5576 461.7217
265.0397 440.4979
265.5219 424.4440
266.0040 413.4993
266.4861 407.8923
266.9682 409.5111
267.4503 412.3036
267.9324 415.4788
268.4146 421.4236
268.8967 416.1243
269.3788 397.3405
269.8609 369.2992
270.3430 339.4287
270.8251 307.3134
271.3073 275.0884
271.7894 242.9498
272.2715 210.2748
272.7536 184.4079
273.2357 167.0792
273.7178 154.7512
274.2000 142.2704
274.6821 129.6321
275.1642 116.8331
275.6463 103.4828
276.1284 89.55786
276.6105 77.14044
277.0927 65.97882
277.5748 56.73090
278.0569 50.65063
278.5390 48.08179
279.0211 46.45471
279.5032 44.77826
279.9854 43.22229
280.4675 43.27576
280.9496 45.34137
281.4317 47.98163
281.9138 49.52570
282.3959 49.90820
282.8781 50.59326
283.3602 52.27466
283.8423 54.65125
284.3244 56.23364
284.8065 56.57874
285.2886 56.48242
285.7708 57.44977
286.2529 59.58417
286.7350 61.23486
287.2171 61.95129
287.6992 62.41699
288.1813 64.46204
288.6635 68.07751
289.1456 72.00531
289.6277 75.56458
290.1098 78.80328
290.5919 81.15894
291.0740 81.97168
291.5562 82.21082
292.0383 84.62787
292.5204 89.14349
293.0025 93.69843
293.4846 96.72247
293.9667 98.68640
294.4489 101.2048
294.9310 104.4500
295.4131 108.3014
295.8952 112.5275
296.3773 117.1635
296.8594 122.4608
297.3416 129.2600
297.8237 136.8265
298.3058 143.0689
298.7879 147.6292
299.2700 152.1982
299.7521 159.1194
300.2343 167.7626
300.7164 175.7747
301.1985 182.8452
301.6806 188.4113
302.1627 190.8394
302.6448 189.9183
303.1270 188.4937
303.6091 189.5028
304.0912 191.9282
304.5733 193.7075
305.0554 194.9307
305.5375 194.5544
306.0197 191.3660
306.5018 185.4241
306.9839 177.2805
307.4660 166.9625
307.9481 154.8466
308.4302 141.4315
308.9124 125.6660
309.3945 109.6860
309.8766 94.20825
310.3587 79.48199
310.8408 67.59503
311.3229 62.41821
311.8051 59.47382
312.2872 54.00049
312.7693 42.64288
313.2514 32.27209
313.7335 27.66693
314.2156 27.37250
314.6978 27.04889
315.1799 24.30115
315.6620 20.99597
316.1441 18.47504
316.6262 17.02197
317.1083 16.11414
317.5905 16.33246
318.0726 16.85822
318.5547 16.26642
319.0368 12.75354
319.5189 9.020874
320.0010 6.396423
320.4832 5.113770
320.9653 4.271606
321.4474 3.387390
321.9295 2.887451
322.4116 3.272095
322.8937 6.693298
323.3759 9.056152
323.8580 8.774536
324.3401 5.670410
324.8222 2.712524
325.3043 0.3510130
325.7864 2.737366
326.2686 3.843201
326.7507 2.125671
327.2328 0.7708130
327.7149 0.4414670
328.1970 1.028564
328.6791 1.161438
329.1613 0.1337890
329.6434 1.192993
330.1255 1.156372
330.6076 1.372803
331.0897 3.191284
331.5718 4.071777
332.0540 4.218445
332.5361 4.249512
333.0182 4.238953
333.5003 4.008606
333.9824 3.260437
334.4645 1.274414
334.9467 0.9379270
335.4288 3.244629
335.9109 6.504333
336.3930 7.782715
336.8751 6.209656
337.3572 4.838074
337.8394 4.876404
338.3215 6.453613
338.8036 6.193726
339.2857 3.223633
339.7678 0.1145020
340.2499 0.9734500
340.7320 1.201111
341.2141 2.818176
341.6963 2.924805
342.1784 1.866272
342.6605 1.083008
343.1426 0.5249630
343.6247 0.5444340
344.1068 2.372986
344.5890 5.836365
345.0711 6.442932
345.5532 2.789856
346.0353 2.993286
346.5174 6.156433
346.9995 6.775513
347.4817 7.474670
347.9638 10.08533
348.4459 14.11731
348.9280 17.93347
349.4101 21.46741
349.8922 24.49554
350.3744 26.14484
350.8565 26.80194
351.3386 28.04578
351.8207 31.39429
352.3028 35.51190
352.7849 38.02637
353.2671 38.92413
353.7492 39.69812
354.2313 41.29663
354.7134 43.70410
355.1955 46.99487
355.6776 51.69092
356.1598 56.76746
356.6419 61.02344
357.1240 64.71399
357.6061 69.18982
358.0882 75.69684
358.5703 83.21191
359.0525 90.60333
359.5346 97.42163
360.0167 104.5475
360.4988 111.8363
360.9809 119.7336
361.4630 129.1631
361.9452 141.9482
362.4273 155.2702
362.9094 166.8108
363.3915 175.3305
363.8736 186.7689
364.3557 206.0737
364.8379 228.2169
365.3200 247.2267
365.8021 262.6873
366.2842 273.9970
366.7663 280.5396
367.2484 282.3735
367.7306 281.0840
368.2127 277.1772
368.6948 270.0349
369.1769 259.2319
369.6590 242.0856
370.1411 224.5176
370.6233 205.5808
371.1054 186.0986
371.5875 169.2751
372.0696 155.3304
372.5517 144.0762
373.0338 135.5472
373.5160 130.4041
373.9981 125.9334
374.4802 121.7249
374.9623 118.5251
375.4444 118.2034
375.9265 122.4863
376.4087 124.7889
376.8908 122.4398
377.3729 115.6082
377.8550 110.7361
378.3371 108.7025
378.8192 106.5215
379.3014 101.1370
379.7835 92.43079
380.2656 82.76263
380.7477 72.20251
381.2298 61.48456
381.7119 52.70538
382.1941 45.85522
382.6762 38.95148
383.1583 29.84143
383.6404 19.40460
384.1225 11.44159
384.6046 6.677856
385.0868 3.869385
385.5689 2.259277
386.0510 1.394043
386.5331 0.1712650
387.0152 4.310242
387.4973 8.953369
387.9795 10.95740
388.4616 10.43921
388.9437 9.208191
389.4258 8.333374
389.9079 7.598694
390.3900 6.758789
390.8722 5.202637
391.3543 4.115906
391.8364 4.741394
392.3185 6.608215
392.8006 8.307617
393.2827 9.712769
393.7649 10.64563
394.2470 10.72711
394.7291 9.492798
395.2112 7.964966
395.6933 6.333862
396.1754 4.880859
396.6576 3.762878
397.1397 3.973877
397.6218 3.309692
398.1039 0.5279540
398.5860 4.554321
399.0681 7.608032
399.5503 5.176147
400.0324 2.630737
400.5145 3.888733
400.9966 12.60699
401.4787 20.02051
401.9608 25.57208
402.4430 29.20850
402.9251 31.01428
403.4072 29.76208
403.8893 29.35077
404.3714 31.29193
404.8535 35.98700
405.3357 40.96381
405.8178 46.17487
406.2999 51.65814
406.7820 57.40613
407.2641 63.40295
407.7462 69.61664
408.2284 75.78571
408.7105 82.09625
409.1926 90.96204
409.6747 102.8217
410.1568 114.0261
410.6389 120.0637
411.1211 122.0753
411.6032 127.1160
412.0853 136.8755
412.5674 149.1740
413.0495 161.9800
413.5316 175.1220
414.0138 187.3083
414.4959 196.5750
414.9780 205.0863
415.4601 216.1412
415.9422 230.1208
416.4243 245.0631
416.9065 260.2313
417.3886 275.2205
417.8707 289.0304
418.3528 299.1354
418.8349 310.2136
419.3170 325.7117
419.7992 345.1632
420.2813 365.3690
420.7634 385.8361
421.2455 406.4215
421.7276 426.9224
422.2097 447.2520
422.6919 468.0870
423.1740 489.2588
423.6561 511.1781
424.1382 535.0462
424.6203 561.2063
425.1024 588.5113
425.5846 616.9741
426.0667 646.4930
426.5488 676.7678
427.0309 706.1588
427.5130 738.1121
427.9951 775.4624
428.4773 820.8774
428.9594 865.5839
429.4415 907.3157
429.9236 948.5577
430.4057 996.0966
430.8878 1049.501
431.3700 1109.931
431.8521 1179.539
432.3342 1258.336
432.8163 1334.411
433.2984 1405.420
433.7805 1481.905
434.2627 1576.157
434.7448 1687.357
435.2269 1806.382
435.7090 1930.773
436.1911 2064.165
436.6732 2210.682
437.1554 2371.137
437.6375 2548.029
438.1196 2744.343
438.6017 2957.741
439.0838 3185.213
439.5659 3427.844
440.0480 3680.927
440.5302 3946.953
441.0123 4222.239
441.4944 4500.631
441.9765 4784.668
442.4586 5066.806
442.9407 5339.095
443.4229 5601.416
443.9050 5873.696
444.3871 6164.607
444.8692 6464.342
445.3513 6765.555
445.8334 7064.338
446.3156 7371.072
446.7977 7671.818
447.2798 7982.229
447.7619 8329.439
448.2440 8726.998
448.7261 9146.111
449.2083 9573.063
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