#\#CIF_2.0 #------------------------------------------------------------------------------ #$Date: 2018-05-24 15:20:34 +0300 (Thu, 24 May 2018) $ #$Revision: 656 $ #$URL: svn://172.16.1.111/rod/cif/1/00/01/1000188.rod $ #------------------------------------------------------------------------------ # # This file is available in the Raman Open Database (ROD), # http://solsa.crystallography.net/rod/ # # All data on this site have been placed in the public domain by the # contributors. # data_1000188 loop_ _publ_author_name 'Cruciani, G.' 'Gualtieri, A.' _publ_section_title ; Dehydration dynamics of analcime by in situ synchrotron powder diffraction Sample at T = 298 K ; _journal_name_full 'American Mineralogist' _journal_page_first 112 _journal_page_last 119 _journal_volume 84 _journal_year 1999 _chemical_compound_source R050094 _chemical_formula_sum 'Al1.9 H4 Na1.95 O14 Si4.1' _chemical_name_mineral Analcime _space_group_IT_number 142 _symmetry_space_group_name_Hall '-I 4bd 2c' _symmetry_space_group_name_H-M 'I 41/a c d :2' _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 13.7295 _cell_length_b 13.7295 _cell_length_c 13.7036 _cell_volume 2583.117 _diffrn_ambient_temperature 298 _exptl_crystal_density_diffrn 2.259 _cod_original_sg_symbol_H-M 'I 41/a c d' _cod_original_formula_sum '(Si4.1 Al1.9) Na1.95 O14 H4' _cod_database_code 9002000 _raman_determination_method experimental _raman_measurement_device.location 'Arizona University' _raman_measurement_device.company 'Thermo Scientific' _raman_measurement_device.model 'Nicolet Almega XR' _raman_measurement_device.optics_type microscope _raman_measurement_device.microscope_system dispersive _raman_measurement_device.microscope_objective_magnification 50 _raman_measurement_device.microscope_numerical_aperture 0.5 _raman_measurement_device.excitation_laser_type other _raman_measurement_device.excitation_laser_wavelength 532 _raman_measurement_device.configuration simple _raman_measurement_device.resolution 4 _raman_measurement_device.power_on_sample 15 _raman_measurement_device.direction_polarization unoriented _raman_measurement_device.spot_size 1 _raman_measurement_device.diffraction_grating 400 _raman_measurement.environment Air _raman_measurement.environment_details ; The sample was measured in air. ; _raman_measurement.temperature 300 _raman_measurement.pressure 100 _raman_measurement.background_subtraction no _raman_measurement.background_subtraction_details ; No background subtraction method was applied. ; _raman_measurement.baseline_correction no _raman_measurement.baseline_correction_details ; No baseline correction method was applied. ; _raman_measurement.integration_time 10 _rod_data_source.file R050094.rod _rod_data_source.block 3500000 _rod_database.code 1000188 loop_ _raman_complementary.id _raman_complementary.method 1 XRD loop_ _raman_measurement_device_calibration.id _raman_measurement_device_calibration.standard 1 neon_lamp loop_ _rod_related_entry.id _rod_related_entry.code _rod_related_entry.database _rod_related_entry.uri _rod_related_entry.description 1 9002000 COD http://www.crystallography.net/cod/9002000.html ; XRD analysis data was done. ; loop_ _raman_spectrum.raman_shift _raman_spectrum.intensity 126.3948 0.0000000E+00 126.8769 39.77466 127.3591 90.54443 127.8412 109.1001 128.3233 103.0945 128.8054 95.07690 129.2875 84.67920 129.7696 74.74878 130.2518 74.79419 130.7339 87.56226 131.2160 102.8398 131.6981 102.9412 132.1802 89.66846 132.6623 77.79590 133.1445 71.58691 133.6266 70.51611 134.1087 72.13892 134.5908 75.36401 135.0729 82.84424 135.5550 100.1519 136.0372 127.8989 136.5193 158.8223 137.0014 192.1687 137.4835 228.7024 137.9656 257.8757 138.4477 280.5269 138.9299 294.6746 139.4120 292.5435 139.8941 266.5171 140.3762 240.2808 140.8583 233.6328 141.3404 254.0366 141.8226 271.1438 142.3047 281.1299 142.7868 284.2263 143.2689 275.4114 143.7510 246.2197 144.2331 212.6836 144.7152 196.6345 145.1974 210.0918 145.6795 221.9463 146.1616 222.4893 146.6437 205.6255 147.1258 192.9904 147.6079 190.2421 148.0901 192.5638 148.5722 186.2659 149.0543 171.7555 149.5364 171.3538 150.0185 178.2988 150.5006 206.2773 150.9828 219.6171 151.4649 217.6689 151.9470 207.2120 152.4291 197.9104 152.9112 200.0286 153.3933 205.1309 153.8755 206.0918 154.3576 201.8257 154.8397 193.4755 155.3218 180.1626 155.8039 161.0244 156.2860 141.6511 156.7682 120.2396 157.2503 100.0366 157.7324 84.95984 158.2145 83.40369 158.6966 81.51624 159.1787 71.36792 159.6609 44.07544 160.1430 26.50952 160.6251 37.47876 161.1072 65.08521 161.5893 81.76074 162.0714 68.49939 162.5536 46.00916 163.0357 28.21362 163.5178 20.16284 163.9999 15.47278 164.4820 11.91968 164.9641 9.474731 165.4463 8.221436 165.9284 9.766846 166.4105 11.98035 166.8926 12.56714 167.3747 10.29272 167.8568 6.318237 168.3390 1.309937 168.8211 13.03577 169.3032 19.04663 169.7853 2.481323 170.2674 23.63354 170.7495 36.54675 171.2317 11.66516 171.7138 24.98389 172.1959 46.96533 172.6780 49.34473 173.1601 44.09082 173.6422 39.58362 174.1244 35.21130 174.6065 28.94824 175.0886 15.79028 175.5707 1.393921 176.0528 5.069458 176.5349 2.833862 177.0171 12.68970 177.4992 6.943115 177.9813 12.39526 178.4634 29.55664 178.9455 29.48865 179.4276 18.18298 179.9098 8.994751 180.3919 2.765259 180.8740 3.004761 181.3561 20.77979 181.8382 56.77710 182.3203 91.02112 182.8025 100.3311 183.2846 88.85620 183.7667 74.63782 184.2488 63.04138 184.7309 54.52905 185.2130 50.85364 185.6951 52.54871 186.1773 56.88879 186.6594 58.01074 187.1415 56.70410 187.6236 61.50916 188.1057 84.89221 188.5878 120.8896 189.0700 139.7185 189.5521 134.7650 190.0342 117.6676 190.5163 107.1772 190.9984 103.3503 191.4805 105.5066 191.9627 117.4993 192.4448 138.0559 192.9269 150.5472 193.4090 149.1768 193.8911 140.4292 194.3732 143.7935 194.8554 160.3105 195.3375 179.3567 195.8196 193.6677 196.3017 204.6217 196.7838 204.9396 197.2659 186.9584 197.7481 155.4861 198.2302 145.3676 198.7123 162.1136 199.1944 186.1426 199.6765 191.7936 200.1586 176.1749 200.6408 162.8604 201.1229 161.1853 201.6050 171.4541 202.0871 177.9788 202.5692 179.4213 203.0513 179.5476 203.5335 186.6807 204.0156 203.4918 204.4977 215.4592 204.9798 213.2966 205.4619 194.5925 205.9440 182.4470 206.4262 180.0486 206.9083 183.0684 207.3904 179.3453 207.8725 166.2743 208.3546 154.9636 208.8367 154.7310 209.3189 170.6791 209.8010 174.8545 210.2831 159.9821 210.7652 132.1414 211.2473 118.8552 211.7294 123.8420 212.2116 136.0619 212.6937 149.5763 213.1758 168.2299 213.6579 175.8126 214.1400 165.7838 214.6221 139.8811 215.1043 125.9176 215.5864 127.5684 216.0685 135.5845 216.5506 141.8263 217.0327 147.5892 217.5148 148.2662 217.9970 139.3820 218.4791 119.5559 218.9612 114.7466 219.4433 132.7784 219.9254 158.0750 220.4075 170.5836 220.8897 166.9683 221.3718 157.2780 221.8539 141.6057 222.3360 116.8198 222.8181 103.2965 223.3002 104.9933 223.7824 115.7845 224.2645 125.1930 224.7466 133.9810 225.2287 140.2615 225.7108 143.2506 226.1929 142.2396 226.6750 138.3140 227.1572 130.4017 227.6393 121.9344 228.1214 116.7279 228.6035 113.5480 229.0856 114.8307 229.5677 121.8141 230.0499 141.9452 230.5320 152.3644 231.0141 149.0504 231.4962 135.4894 231.9783 126.5035 232.4604 126.0260 232.9426 125.8297 233.4247 120.2943 233.9068 105.2109 234.3889 90.93835 234.8710 77.35596 235.3531 65.69739 235.8353 60.40393 236.3174 65.48279 236.7995 71.02173 237.2816 68.46155 237.7637 50.03271 238.2458 38.69116 238.7280 40.27148 239.2101 54.67188 239.6922 63.97852 240.1743 65.62183 240.6564 64.55933 241.1385 65.85022 241.6207 73.25159 242.1028 76.06946 242.5849 70.46838 243.0670 55.36707 243.5491 45.60486 244.0313 43.13818 244.5134 44.36206 244.9955 45.42896 245.4776 47.07727 245.9597 47.20251 246.4418 44.31812 246.9240 37.15613 247.4061 34.79956 247.8882 40.08142 248.3703 48.16785 248.8524 52.55188 249.3345 54.15881 249.8167 50.31970 250.2988 38.49426 250.7809 15.06946 251.2630 2.611084 251.7451 15.96814 252.2272 22.66882 252.7094 16.01855 253.1915 14.90344 253.6736 40.55103 254.1557 49.30408 254.6378 35.90637 255.1199 21.67981 255.6021 4.661743 256.0842 12.13110 256.5663 21.57751 257.0484 21.37292 257.5305 17.81433 258.0126 13.16968 258.4948 6.610474 258.9769 1.012817 259.4590 3.966064 259.9411 7.910156 260.4232 9.930420 260.9053 6.760254 261.3875 4.352051 261.8696 8.372925 262.3517 23.38879 262.8338 29.91467 263.3159 22.00562 263.7980 4.098999 264.2802 0.1665040 264.7623 15.40112 265.2444 33.11914 265.7265 42.51367 266.2086 41.39026 266.6907 39.18884 267.1729 36.57629 267.6550 33.43958 268.1371 28.85217 268.6192 21.53882 269.1013 15.30017 269.5834 13.62512 270.0656 17.98376 270.5477 19.82483 271.0298 16.97632 271.5119 11.01208 271.9940 8.810913 272.4761 11.16431 272.9583 15.36389 273.4404 20.26733 273.9225 26.47290 274.4046 29.72131 274.8867 28.11865 275.3688 23.28613 275.8510 24.35388 276.3331 34.04761 276.8152 41.33374 277.2973 33.15686 277.7794 6.860107 278.2615 9.720581 278.7437 9.566040 279.2258 4.091431 279.7079 18.21143 280.1900 33.54688 280.6721 46.23083 281.1542 52.55078 281.6364 52.41260 282.1185 48.66101 282.6006 38.41919 283.0827 25.66150 283.5648 28.50549 284.0469 48.90393 284.5291 74.80237 285.0112 95.97351 285.4933 112.4551 285.9754 126.2397 286.4575 135.9978 286.9396 143.7484 287.4217 156.0046 287.9038 172.8066 288.3860 193.6010 288.8681 221.4180 289.3502 254.7247 289.8323 281.4413 290.3144 291.9990 290.7965 295.2969 291.2787 320.2731 291.7608 368.8519 292.2429 418.4371 292.7250 443.2184 293.2071 448.5139 293.6892 461.0583 294.1714 492.7793 294.6535 535.7056 295.1356 574.2628 295.6177 608.5308 296.0998 638.4673 296.5819 669.1755 297.0641 697.3159 297.5462 710.4141 298.0283 698.7466 298.5104 672.6235 298.9925 647.8064 299.4746 624.2229 299.9568 600.5730 300.4389 575.1710 300.9210 548.5616 301.4031 521.6707 301.8852 498.4720 302.3673 473.4353 302.8495 435.4193 303.3316 385.0056 303.8137 336.3051 304.2958 301.6541 304.7779 276.8492 305.2600 255.2383 305.7422 232.9352 306.2243 213.7003 306.7064 204.2651 307.1885 203.9681 307.6706 201.1698 308.1527 184.2010 308.6349 160.0001 309.1170 138.5269 309.5991 126.7047 310.0812 116.8641 310.5633 103.6550 311.0454 88.40552 311.5276 73.50391 312.0097 54.79443 312.4918 39.02795 312.9739 33.77002 313.4560 59.29309 313.9381 80.66443 314.4203 73.27209 314.9024 40.15088 315.3845 13.03198 315.8666 15.12903 316.3487 26.85974 316.8308 29.54602 317.3130 0.7613530 317.7951 22.75195 318.2772 19.48865 318.7593 7.399292 319.2414 23.69080 319.7235 4.427002 320.2057 22.43408 320.6878 35.18030 321.1699 12.63989 321.6520 7.219116 322.1341 12.98926 322.6162 7.025146 323.0984 4.241821 323.5805 12.96582 324.0626 22.22363 324.5447 24.68250 325.0268 6.826050 325.5089 4.085205 325.9911 0.2846680 326.4732 17.94702 326.9553 28.61511 327.4374 23.18628 327.9195 15.97449 328.4016 15.18225 328.8838 31.43250 329.3659 40.32776 329.8480 37.27576 330.3301 24.50623 330.8122 15.19592 331.2943 8.545776 331.7765 6.001587 332.2586 8.851563 332.7407 21.44690 333.2228 31.39795 333.7049 37.66492 334.1870 40.99683 334.6692 44.19360 335.1513 47.60742 335.6334 49.82581 336.1155 49.18469 336.5976 45.06543 337.0797 45.22998 337.5619 50.89172 338.0440 59.83337 338.5261 65.82068 339.0082 68.16931 339.4903 69.37915 339.9724 70.73926 340.4546 72.33130 340.9367 73.63550 341.4188 75.74500 341.9009 76.50403 342.3830 66.85486 342.8651 44.66553 343.3473 31.69934 343.8294 49.20129 344.3115 93.57666 344.7936 112.1875 345.2757 97.30884 345.7578 69.01965 346.2400 56.76086 346.7221 60.17310 347.2042 69.99915 347.6863 85.77869 348.1684 104.7179 348.6505 117.1067 349.1327 121.7974 349.6148 123.6678 350.0969 127.5420 350.5790 133.3090 351.0611 140.6938 351.5432 152.2050 352.0254 164.2743 352.5075 170.3130 352.9896 169.4900 353.4717 168.0759 353.9538 174.6655 354.4359 184.7915 354.9181 189.4038 355.4002 174.6102 355.8823 158.7855 356.3644 162.8669 356.8465 187.3616 357.3286 209.9813 357.8108 212.5154 358.2929 205.7468 358.7750 203.8833 359.2571 217.4620 359.7392 232.8811 360.2213 241.6050 360.7035 244.1155 361.1856 248.7125 361.6677 263.0955 362.1498 279.3417 362.6319 290.4789 363.1140 289.0635 363.5962 288.1992 364.0783 290.9514 364.5604 297.1252 365.0425 305.7958 365.5246 320.9153 366.0067 335.9647 366.4889 346.9728 366.9710 346.8596 367.4531 351.7596 367.9352 361.1687 368.4173 375.2604 368.8994 394.4095 369.3815 431.3628 369.8636 462.5533 370.3458 477.2246 370.8279 458.3257 371.3100 451.8455 371.7921 461.3282 372.2742 482.5728 372.7563 510.2324 373.2385 553.2007 373.7206 587.3145 374.2027 598.7612 374.6848 578.5151 375.1669 571.4028 375.6490 578.8354 376.1312 597.4374 376.6133 623.8535 377.0954 659.6692 377.5775 691.6429 378.0596 713.6775 378.5417 725.6812 379.0239 740.1935 379.5060 757.2201 379.9881 773.3645 380.4702 783.1711 380.9523 786.9902 381.4344 792.1399 381.9166 800.8949 382.3987 812.7686 382.8808 829.3018 383.3629 850.7532 383.8450 869.0524 384.3271 870.3208 384.8093 860.8972 385.2914 861.2749 385.7735 884.1055 386.2556 913.2604 386.7377 926.0242 387.2198 923.7234 387.7020 916.6465 388.1841 907.0626 388.6662 898.7485 389.1483 897.9564 389.6304 911.9414 390.1125 924.6157 390.5947 923.7627 391.0768 911.8151 391.5589 896.1667 392.0410 874.2938 392.5231 854.1709 393.0052 843.0122 393.4874 847.0911 393.9695 847.7568 394.4516 838.5453 394.9337 820.8987 395.4158 797.4794 395.8979 761.7935 396.3801 726.4633 396.8622 696.6235 397.3443 673.3585 397.8264 652.8943 398.3085 638.5081 398.7906 625.4962 399.2728 608.2216 399.7549 580.8684 400.2370 555.6577 400.7191 536.6525 401.2012 524.7058 401.6833 505.9514 402.1655 475.2998 402.6476 443.2126 403.1297 419.4741 403.6118 408.4912 404.0939 394.9872 404.5760 375.8055 405.0582 352.3026 405.5403 331.9584 406.0224 315.1318 406.5045 300.9083 406.9866 291.7606 407.4688 288.4446 407.9509 273.2454 408.4330 240.3094 408.9151 199.9121 409.3972 174.0668 409.8793 162.9115 410.3615 155.1281 410.8436 143.8325 411.3257 130.5881 411.8078 121.6798 412.2899 118.1945 412.7720 115.7140 413.2542 108.6036 413.7363 98.19336 414.2184 88.23120 414.7005 79.86011 415.1826 73.28516 415.6647 70.15417 416.1469 70.59021 416.6290 69.27161 417.1111 62.13904 417.5932 50.92969 418.0753 38.20117 418.5574 20.13013 419.0396 4.669800 419.5217 2.737061 420.0038 3.141602 420.4859 3.996460 420.9680 9.884277 421.4501 16.17334 421.9323 19.45618 422.4144 16.49194 422.8965 14.14648 423.3786 11.90698 423.8607 10.86633 424.3428 14.17358 424.8250 34.58374 425.3071 23.81079 425.7892 17.22278 426.2713 14.59314 426.7534 27.78943 427.2355 20.54236 427.7177 21.48364 428.1998 22.75769 428.6819 12.62329 429.1640 23.50122 429.6461 13.53796 430.1282 11.88745 430.6104 6.423462 431.0925 9.193604 431.5746 9.411377 432.0567 1.373901 432.5388 2.108643 433.0209 1.572388 433.5031 4.194458 433.9852 6.880859 434.4673 3.155518 434.9494 6.963379 435.4315 3.354370 435.9136 3.056885 436.3958 0.7099610 436.8779 9.760620 437.3600 26.00867 437.8421 42.70703 438.3242 50.55664 438.8063 52.48254 439.2885 56.64587 439.7706 73.05579 440.2527 90.18506 440.7348 94.54407 441.2169 83.56641 441.6990 76.38904 442.1812 88.31946 442.6633 108.4856 443.1454 124.0819 443.6275 125.4408 444.1096 126.9850 444.5917 134.0927 445.0739 146.5209 445.5560 159.0184 446.0381 169.4303 446.5202 180.3049 447.0023 193.1161 447.4844 207.8197 447.9666 224.8175 448.4487 246.0198 448.9308 269.4790 449.4129 289.3466 449.8950 300.8883 450.3771 316.0923 450.8593 342.0984 451.3413 382.3586 451.8235 410.3197 452.3056 421.0031 452.7877 427.3645 453.2698 446.8939 453.7519 480.1925 454.2340 519.3938 454.7162 565.1425 455.1983 614.4489 455.6804 658.5345 456.1625 697.4930 456.6446 732.0566 457.1267 753.4154 457.6089 770.4260 458.0910 811.7319 458.5731 890.7546 459.0552 981.7284 459.5373 1054.027 460.0194 1111.590 460.5016 1168.927 460.9837 1223.617 461.4658 1287.319 461.9479 1376.346 462.4300 1497.817 462.9121 1613.049 463.3943 1685.489 463.8764 1744.218 464.3585 1825.758 464.8406 1958.092 465.3227 2098.226 465.8048 2233.143 466.2870 2362.433 466.7691 2493.679 467.2512 2618.262 467.7333 2753.102 468.2154 2909.195 468.6975 3101.325 469.1797 3290.494 469.6618 3468.227 470.1439 3641.591 470.6260 3826.188 471.1081 4020.895 471.5902 4229.404 472.0724 4455.612 472.5545 4702.620 473.0366 4945.883 473.5187 5180.945 474.0008 5417.926 474.4829 5667.594 474.9651 5929.554 475.4472 6199.812 475.9293 6480.635 476.4114 6766.759 476.8935 7049.899 477.3756 7327.696 477.8578 7601.320 478.3399 7890.472 478.8220 8169.688 479.3041 8396.798 479.7862 8551.914 480.2683 8685.024 480.7505 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507.7490 874.5580 508.2311 816.6532 508.7132 767.3641 509.1953 751.5728 509.6775 765.6174 510.1596 761.6455 510.6417 713.3174 511.1238 643.1382 511.6059 593.9769 512.0880 565.0696 512.5701 546.8550 513.0522 540.5603 513.5344 537.7736 514.0165 525.4915 514.4986 495.4775 514.9807 468.1095 515.4628 464.5662 515.9449 472.5060 516.4271 470.6727 516.9092 446.5164 517.3913 416.5695 517.8734 383.8013 518.3555 348.1805 518.8376 320.4091 519.3198 305.6195 519.8019 296.3286 520.2840 288.1216 520.7661 281.1541 521.2482 275.4856 521.7303 272.1746 522.2125 269.4430 522.6946 262.6918 523.1767 250.5526 523.6588 239.9362 524.1409 235.5360 524.6230 235.9502 525.1052 227.5796 525.5873 209.2129 526.0694 191.4536 526.5515 185.8154 527.0336 189.2198 527.5157 194.1594 527.9979 201.3920 528.4800 204.8512 528.9621 195.8444 529.4442 177.3420 529.9263 157.7595 530.4084 138.7325 530.8906 122.2942 531.3727 110.8671 531.8548 105.0149 532.3369 99.66479 532.8190 90.10168 533.3011 81.61902 533.7833 79.20886 534.2654 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