#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-05-24 15:20:34 +0300 (Thu, 24 May 2018) $
#$Revision: 656 $
#$URL: svn://172.16.1.111/rod/cif/1/00/01/1000188.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000188
loop_
_publ_author_name
'Cruciani, G.'
'Gualtieri, A.'
_publ_section_title
;
 Dehydration dynamics of analcime by in situ synchrotron powder
 diffraction Sample at T = 298 K
;
_journal_name_full               'American Mineralogist'
_journal_page_first              112
_journal_page_last               119
_journal_volume                  84
_journal_year                    1999
_chemical_compound_source        R050094
_chemical_formula_sum            'Al1.9 H4 Na1.95 O14 Si4.1'
_chemical_name_mineral           Analcime
_space_group_IT_number           142
_symmetry_space_group_name_Hall  '-I 4bd 2c'
_symmetry_space_group_name_H-M   'I 41/a c d :2'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            8
_cell_length_a                   13.7295
_cell_length_b                   13.7295
_cell_length_c                   13.7036
_cell_volume                     2583.117
_diffrn_ambient_temperature      298
_exptl_crystal_density_diffrn    2.259
_cod_original_sg_symbol_H-M      'I 41/a c d'
_cod_original_formula_sum        '(Si4.1 Al1.9) Na1.95 O14 H4'
_cod_database_code               9002000
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 15
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R050094.rod
_rod_data_source.block           3500000
_rod_database.code               1000188
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9002000 COD http://www.crystallography.net/cod/9002000.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
126.3948 0.0000000E+00
126.8769 39.77466
127.3591 90.54443
127.8412 109.1001
128.3233 103.0945
128.8054 95.07690
129.2875 84.67920
129.7696 74.74878
130.2518 74.79419
130.7339 87.56226
131.2160 102.8398
131.6981 102.9412
132.1802 89.66846
132.6623 77.79590
133.1445 71.58691
133.6266 70.51611
134.1087 72.13892
134.5908 75.36401
135.0729 82.84424
135.5550 100.1519
136.0372 127.8989
136.5193 158.8223
137.0014 192.1687
137.4835 228.7024
137.9656 257.8757
138.4477 280.5269
138.9299 294.6746
139.4120 292.5435
139.8941 266.5171
140.3762 240.2808
140.8583 233.6328
141.3404 254.0366
141.8226 271.1438
142.3047 281.1299
142.7868 284.2263
143.2689 275.4114
143.7510 246.2197
144.2331 212.6836
144.7152 196.6345
145.1974 210.0918
145.6795 221.9463
146.1616 222.4893
146.6437 205.6255
147.1258 192.9904
147.6079 190.2421
148.0901 192.5638
148.5722 186.2659
149.0543 171.7555
149.5364 171.3538
150.0185 178.2988
150.5006 206.2773
150.9828 219.6171
151.4649 217.6689
151.9470 207.2120
152.4291 197.9104
152.9112 200.0286
153.3933 205.1309
153.8755 206.0918
154.3576 201.8257
154.8397 193.4755
155.3218 180.1626
155.8039 161.0244
156.2860 141.6511
156.7682 120.2396
157.2503 100.0366
157.7324 84.95984
158.2145 83.40369
158.6966 81.51624
159.1787 71.36792
159.6609 44.07544
160.1430 26.50952
160.6251 37.47876
161.1072 65.08521
161.5893 81.76074
162.0714 68.49939
162.5536 46.00916
163.0357 28.21362
163.5178 20.16284
163.9999 15.47278
164.4820 11.91968
164.9641 9.474731
165.4463 8.221436
165.9284 9.766846
166.4105 11.98035
166.8926 12.56714
167.3747 10.29272
167.8568 6.318237
168.3390 1.309937
168.8211 13.03577
169.3032 19.04663
169.7853 2.481323
170.2674 23.63354
170.7495 36.54675
171.2317 11.66516
171.7138 24.98389
172.1959 46.96533
172.6780 49.34473
173.1601 44.09082
173.6422 39.58362
174.1244 35.21130
174.6065 28.94824
175.0886 15.79028
175.5707 1.393921
176.0528 5.069458
176.5349 2.833862
177.0171 12.68970
177.4992 6.943115
177.9813 12.39526
178.4634 29.55664
178.9455 29.48865
179.4276 18.18298
179.9098 8.994751
180.3919 2.765259
180.8740 3.004761
181.3561 20.77979
181.8382 56.77710
182.3203 91.02112
182.8025 100.3311
183.2846 88.85620
183.7667 74.63782
184.2488 63.04138
184.7309 54.52905
185.2130 50.85364
185.6951 52.54871
186.1773 56.88879
186.6594 58.01074
187.1415 56.70410
187.6236 61.50916
188.1057 84.89221
188.5878 120.8896
189.0700 139.7185
189.5521 134.7650
190.0342 117.6676
190.5163 107.1772
190.9984 103.3503
191.4805 105.5066
191.9627 117.4993
192.4448 138.0559
192.9269 150.5472
193.4090 149.1768
193.8911 140.4292
194.3732 143.7935
194.8554 160.3105
195.3375 179.3567
195.8196 193.6677
196.3017 204.6217
196.7838 204.9396
197.2659 186.9584
197.7481 155.4861
198.2302 145.3676
198.7123 162.1136
199.1944 186.1426
199.6765 191.7936
200.1586 176.1749
200.6408 162.8604
201.1229 161.1853
201.6050 171.4541
202.0871 177.9788
202.5692 179.4213
203.0513 179.5476
203.5335 186.6807
204.0156 203.4918
204.4977 215.4592
204.9798 213.2966
205.4619 194.5925
205.9440 182.4470
206.4262 180.0486
206.9083 183.0684
207.3904 179.3453
207.8725 166.2743
208.3546 154.9636
208.8367 154.7310
209.3189 170.6791
209.8010 174.8545
210.2831 159.9821
210.7652 132.1414
211.2473 118.8552
211.7294 123.8420
212.2116 136.0619
212.6937 149.5763
213.1758 168.2299
213.6579 175.8126
214.1400 165.7838
214.6221 139.8811
215.1043 125.9176
215.5864 127.5684
216.0685 135.5845
216.5506 141.8263
217.0327 147.5892
217.5148 148.2662
217.9970 139.3820
218.4791 119.5559
218.9612 114.7466
219.4433 132.7784
219.9254 158.0750
220.4075 170.5836
220.8897 166.9683
221.3718 157.2780
221.8539 141.6057
222.3360 116.8198
222.8181 103.2965
223.3002 104.9933
223.7824 115.7845
224.2645 125.1930
224.7466 133.9810
225.2287 140.2615
225.7108 143.2506
226.1929 142.2396
226.6750 138.3140
227.1572 130.4017
227.6393 121.9344
228.1214 116.7279
228.6035 113.5480
229.0856 114.8307
229.5677 121.8141
230.0499 141.9452
230.5320 152.3644
231.0141 149.0504
231.4962 135.4894
231.9783 126.5035
232.4604 126.0260
232.9426 125.8297
233.4247 120.2943
233.9068 105.2109
234.3889 90.93835
234.8710 77.35596
235.3531 65.69739
235.8353 60.40393
236.3174 65.48279
236.7995 71.02173
237.2816 68.46155
237.7637 50.03271
238.2458 38.69116
238.7280 40.27148
239.2101 54.67188
239.6922 63.97852
240.1743 65.62183
240.6564 64.55933
241.1385 65.85022
241.6207 73.25159
242.1028 76.06946
242.5849 70.46838
243.0670 55.36707
243.5491 45.60486
244.0313 43.13818
244.5134 44.36206
244.9955 45.42896
245.4776 47.07727
245.9597 47.20251
246.4418 44.31812
246.9240 37.15613
247.4061 34.79956
247.8882 40.08142
248.3703 48.16785
248.8524 52.55188
249.3345 54.15881
249.8167 50.31970
250.2988 38.49426
250.7809 15.06946
251.2630 2.611084
251.7451 15.96814
252.2272 22.66882
252.7094 16.01855
253.1915 14.90344
253.6736 40.55103
254.1557 49.30408
254.6378 35.90637
255.1199 21.67981
255.6021 4.661743
256.0842 12.13110
256.5663 21.57751
257.0484 21.37292
257.5305 17.81433
258.0126 13.16968
258.4948 6.610474
258.9769 1.012817
259.4590 3.966064
259.9411 7.910156
260.4232 9.930420
260.9053 6.760254
261.3875 4.352051
261.8696 8.372925
262.3517 23.38879
262.8338 29.91467
263.3159 22.00562
263.7980 4.098999
264.2802 0.1665040
264.7623 15.40112
265.2444 33.11914
265.7265 42.51367
266.2086 41.39026
266.6907 39.18884
267.1729 36.57629
267.6550 33.43958
268.1371 28.85217
268.6192 21.53882
269.1013 15.30017
269.5834 13.62512
270.0656 17.98376
270.5477 19.82483
271.0298 16.97632
271.5119 11.01208
271.9940 8.810913
272.4761 11.16431
272.9583 15.36389
273.4404 20.26733
273.9225 26.47290
274.4046 29.72131
274.8867 28.11865
275.3688 23.28613
275.8510 24.35388
276.3331 34.04761
276.8152 41.33374
277.2973 33.15686
277.7794 6.860107
278.2615 9.720581
278.7437 9.566040
279.2258 4.091431
279.7079 18.21143
280.1900 33.54688
280.6721 46.23083
281.1542 52.55078
281.6364 52.41260
282.1185 48.66101
282.6006 38.41919
283.0827 25.66150
283.5648 28.50549
284.0469 48.90393
284.5291 74.80237
285.0112 95.97351
285.4933 112.4551
285.9754 126.2397
286.4575 135.9978
286.9396 143.7484
287.4217 156.0046
287.9038 172.8066
288.3860 193.6010
288.8681 221.4180
289.3502 254.7247
289.8323 281.4413
290.3144 291.9990
290.7965 295.2969
291.2787 320.2731
291.7608 368.8519
292.2429 418.4371
292.7250 443.2184
293.2071 448.5139
293.6892 461.0583
294.1714 492.7793
294.6535 535.7056
295.1356 574.2628
295.6177 608.5308
296.0998 638.4673
296.5819 669.1755
297.0641 697.3159
297.5462 710.4141
298.0283 698.7466
298.5104 672.6235
298.9925 647.8064
299.4746 624.2229
299.9568 600.5730
300.4389 575.1710
300.9210 548.5616
301.4031 521.6707
301.8852 498.4720
302.3673 473.4353
302.8495 435.4193
303.3316 385.0056
303.8137 336.3051
304.2958 301.6541
304.7779 276.8492
305.2600 255.2383
305.7422 232.9352
306.2243 213.7003
306.7064 204.2651
307.1885 203.9681
307.6706 201.1698
308.1527 184.2010
308.6349 160.0001
309.1170 138.5269
309.5991 126.7047
310.0812 116.8641
310.5633 103.6550
311.0454 88.40552
311.5276 73.50391
312.0097 54.79443
312.4918 39.02795
312.9739 33.77002
313.4560 59.29309
313.9381 80.66443
314.4203 73.27209
314.9024 40.15088
315.3845 13.03198
315.8666 15.12903
316.3487 26.85974
316.8308 29.54602
317.3130 0.7613530
317.7951 22.75195
318.2772 19.48865
318.7593 7.399292
319.2414 23.69080
319.7235 4.427002
320.2057 22.43408
320.6878 35.18030
321.1699 12.63989
321.6520 7.219116
322.1341 12.98926
322.6162 7.025146
323.0984 4.241821
323.5805 12.96582
324.0626 22.22363
324.5447 24.68250
325.0268 6.826050
325.5089 4.085205
325.9911 0.2846680
326.4732 17.94702
326.9553 28.61511
327.4374 23.18628
327.9195 15.97449
328.4016 15.18225
328.8838 31.43250
329.3659 40.32776
329.8480 37.27576
330.3301 24.50623
330.8122 15.19592
331.2943 8.545776
331.7765 6.001587
332.2586 8.851563
332.7407 21.44690
333.2228 31.39795
333.7049 37.66492
334.1870 40.99683
334.6692 44.19360
335.1513 47.60742
335.6334 49.82581
336.1155 49.18469
336.5976 45.06543
337.0797 45.22998
337.5619 50.89172
338.0440 59.83337
338.5261 65.82068
339.0082 68.16931
339.4903 69.37915
339.9724 70.73926
340.4546 72.33130
340.9367 73.63550
341.4188 75.74500
341.9009 76.50403
342.3830 66.85486
342.8651 44.66553
343.3473 31.69934
343.8294 49.20129
344.3115 93.57666
344.7936 112.1875
345.2757 97.30884
345.7578 69.01965
346.2400 56.76086
346.7221 60.17310
347.2042 69.99915
347.6863 85.77869
348.1684 104.7179
348.6505 117.1067
349.1327 121.7974
349.6148 123.6678
350.0969 127.5420
350.5790 133.3090
351.0611 140.6938
351.5432 152.2050
352.0254 164.2743
352.5075 170.3130
352.9896 169.4900
353.4717 168.0759
353.9538 174.6655
354.4359 184.7915
354.9181 189.4038
355.4002 174.6102
355.8823 158.7855
356.3644 162.8669
356.8465 187.3616
357.3286 209.9813
357.8108 212.5154
358.2929 205.7468
358.7750 203.8833
359.2571 217.4620
359.7392 232.8811
360.2213 241.6050
360.7035 244.1155
361.1856 248.7125
361.6677 263.0955
362.1498 279.3417
362.6319 290.4789
363.1140 289.0635
363.5962 288.1992
364.0783 290.9514
364.5604 297.1252
365.0425 305.7958
365.5246 320.9153
366.0067 335.9647
366.4889 346.9728
366.9710 346.8596
367.4531 351.7596
367.9352 361.1687
368.4173 375.2604
368.8994 394.4095
369.3815 431.3628
369.8636 462.5533
370.3458 477.2246
370.8279 458.3257
371.3100 451.8455
371.7921 461.3282
372.2742 482.5728
372.7563 510.2324
373.2385 553.2007
373.7206 587.3145
374.2027 598.7612
374.6848 578.5151
375.1669 571.4028
375.6490 578.8354
376.1312 597.4374
376.6133 623.8535
377.0954 659.6692
377.5775 691.6429
378.0596 713.6775
378.5417 725.6812
379.0239 740.1935
379.5060 757.2201
379.9881 773.3645
380.4702 783.1711
380.9523 786.9902
381.4344 792.1399
381.9166 800.8949
382.3987 812.7686
382.8808 829.3018
383.3629 850.7532
383.8450 869.0524
384.3271 870.3208
384.8093 860.8972
385.2914 861.2749
385.7735 884.1055
386.2556 913.2604
386.7377 926.0242
387.2198 923.7234
387.7020 916.6465
388.1841 907.0626
388.6662 898.7485
389.1483 897.9564
389.6304 911.9414
390.1125 924.6157
390.5947 923.7627
391.0768 911.8151
391.5589 896.1667
392.0410 874.2938
392.5231 854.1709
393.0052 843.0122
393.4874 847.0911
393.9695 847.7568
394.4516 838.5453
394.9337 820.8987
395.4158 797.4794
395.8979 761.7935
396.3801 726.4633
396.8622 696.6235
397.3443 673.3585
397.8264 652.8943
398.3085 638.5081
398.7906 625.4962
399.2728 608.2216
399.7549 580.8684
400.2370 555.6577
400.7191 536.6525
401.2012 524.7058
401.6833 505.9514
402.1655 475.2998
402.6476 443.2126
403.1297 419.4741
403.6118 408.4912
404.0939 394.9872
404.5760 375.8055
405.0582 352.3026
405.5403 331.9584
406.0224 315.1318
406.5045 300.9083
406.9866 291.7606
407.4688 288.4446
407.9509 273.2454
408.4330 240.3094
408.9151 199.9121
409.3972 174.0668
409.8793 162.9115
410.3615 155.1281
410.8436 143.8325
411.3257 130.5881
411.8078 121.6798
412.2899 118.1945
412.7720 115.7140
413.2542 108.6036
413.7363 98.19336
414.2184 88.23120
414.7005 79.86011
415.1826 73.28516
415.6647 70.15417
416.1469 70.59021
416.6290 69.27161
417.1111 62.13904
417.5932 50.92969
418.0753 38.20117
418.5574 20.13013
419.0396 4.669800
419.5217 2.737061
420.0038 3.141602
420.4859 3.996460
420.9680 9.884277
421.4501 16.17334
421.9323 19.45618
422.4144 16.49194
422.8965 14.14648
423.3786 11.90698
423.8607 10.86633
424.3428 14.17358
424.8250 34.58374
425.3071 23.81079
425.7892 17.22278
426.2713 14.59314
426.7534 27.78943
427.2355 20.54236
427.7177 21.48364
428.1998 22.75769
428.6819 12.62329
429.1640 23.50122
429.6461 13.53796
430.1282 11.88745
430.6104 6.423462
431.0925 9.193604
431.5746 9.411377
432.0567 1.373901
432.5388 2.108643
433.0209 1.572388
433.5031 4.194458
433.9852 6.880859
434.4673 3.155518
434.9494 6.963379
435.4315 3.354370
435.9136 3.056885
436.3958 0.7099610
436.8779 9.760620
437.3600 26.00867
437.8421 42.70703
438.3242 50.55664
438.8063 52.48254
439.2885 56.64587
439.7706 73.05579
440.2527 90.18506
440.7348 94.54407
441.2169 83.56641
441.6990 76.38904
442.1812 88.31946
442.6633 108.4856
443.1454 124.0819
443.6275 125.4408
444.1096 126.9850
444.5917 134.0927
445.0739 146.5209
445.5560 159.0184
446.0381 169.4303
446.5202 180.3049
447.0023 193.1161
447.4844 207.8197
447.9666 224.8175
448.4487 246.0198
448.9308 269.4790
449.4129 289.3466
449.8950 300.8883
450.3771 316.0923
450.8593 342.0984
451.3413 382.3586
451.8235 410.3197
452.3056 421.0031
452.7877 427.3645
453.2698 446.8939
453.7519 480.1925
454.2340 519.3938
454.7162 565.1425
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