#\#CIF_2.0 #------------------------------------------------------------------------------ #$Date: 2018-05-24 15:22:18 +0300 (Thu, 24 May 2018) $ #$Revision: 684 $ #$URL: svn://172.16.1.111/rod/cif/1/00/02/1000202.rod $ #------------------------------------------------------------------------------ # # This file is available in the Raman Open Database (ROD), # http://solsa.crystallography.net/rod/ # # All data on this site have been placed in the public domain by the # contributors. # data_1000202 loop_ _publ_author_name 'Cruciani, G.' 'Gualtieri, A.' _publ_section_title ; Dehydration dynamics of analcime by in situ synchrotron powder diffraction Sample at T = 298 K ; _journal_name_full 'American Mineralogist' _journal_page_first 112 _journal_page_last 119 _journal_volume 84 _journal_year 1999 _chemical_compound_source R060023 _chemical_formula_sum 'Al1.9 H4 Na1.95 O14 Si4.1' _chemical_name_mineral Analcime _space_group_IT_number 142 _symmetry_space_group_name_Hall '-I 4bd 2c' _symmetry_space_group_name_H-M 'I 41/a c d :2' _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 13.7295 _cell_length_b 13.7295 _cell_length_c 13.7036 _cell_volume 2583.117 _diffrn_ambient_temperature 298 _exptl_crystal_density_diffrn 2.259 _cod_original_sg_symbol_H-M 'I 41/a c d' _cod_original_formula_sum '(Si4.1 Al1.9) Na1.95 O14 H4' _cod_database_code 9002000 _raman_determination_method experimental _raman_measurement_device.location 'Arizona University' _raman_measurement_device.company 'Thermo Scientific' _raman_measurement_device.model 'Nicolet Almega XR' _raman_measurement_device.optics_type microscope _raman_measurement_device.microscope_system dispersive _raman_measurement_device.microscope_objective_magnification 50 _raman_measurement_device.microscope_numerical_aperture 0.5 _raman_measurement_device.excitation_laser_type other _raman_measurement_device.excitation_laser_wavelength 532 _raman_measurement_device.configuration simple _raman_measurement_device.resolution 4 _raman_measurement_device.power_on_sample 15 _raman_measurement_device.direction_polarization unoriented _raman_measurement_device.spot_size 1 _raman_measurement_device.diffraction_grating 400 _raman_measurement.environment Air _raman_measurement.environment_details ; The sample was measured in air. ; _raman_measurement.temperature 300 _raman_measurement.pressure 100 _raman_measurement.background_subtraction no _raman_measurement.background_subtraction_details ; No background subtraction method was applied. ; _raman_measurement.baseline_correction no _raman_measurement.baseline_correction_details ; No baseline correction method was applied. ; _raman_measurement.integration_time 10 _rod_data_source.file R060023.rod _rod_data_source.block 3500000 _rod_database.code 1000202 loop_ _raman_complementary.id _raman_complementary.method 1 XRD loop_ _raman_measurement_device_calibration.id _raman_measurement_device_calibration.standard 1 neon_lamp loop_ _rod_related_entry.id _rod_related_entry.code _rod_related_entry.database _rod_related_entry.uri _rod_related_entry.description 1 9002000 COD http://www.crystallography.net/cod/9002000.html ; XRD analysis data was done. ; loop_ _raman_spectrum.raman_shift _raman_spectrum.intensity 166.0323 0.0000000E+00 166.5145 0.7153930 166.9966 0.4946290 167.4787 8.1179999E-03 167.9608 0.1086880 168.4429 0.9488220 168.9250 1.817078 169.4071 2.450150 169.8893 2.860405 170.3714 3.051018 170.8535 3.699852 171.3356 3.316536 171.8177 2.692207 172.2998 1.871681 172.7820 1.044548 173.2641 0.8193210 173.7462 1.017029 174.2283 1.123924 174.7104 0.4593350 175.1925 0.3288730 175.6747 0.3658750 176.1568 0.5850370 176.6389 1.562744 177.1210 1.528366 177.6031 0.7823100 178.0852 0.2711870 178.5674 0.8263780 179.0495 1.873711 179.5316 2.506065 180.0137 2.567253 180.4958 2.319641 180.9779 1.885071 181.4601 1.330780 181.9422 1.002747 182.4243 1.254623 182.9064 1.880753 183.3885 2.474968 183.8706 3.046127 184.3528 3.430267 184.8349 3.073334 185.3170 2.079765 185.7991 1.474442 186.2812 2.407188 186.7633 4.406731 187.2455 5.776917 187.7276 6.125893 188.2097 5.885307 188.6918 5.831085 189.1739 5.965050 189.6560 6.089775 190.1382 5.951660 190.6203 5.620186 191.1024 5.592484 191.5845 6.108276 192.0666 6.853729 192.5487 6.984482 193.0309 6.451096 193.5130 5.900620 193.9951 5.921227 194.4772 6.480186 194.9593 6.935745 195.4414 7.208519 195.9236 7.276955 196.4057 6.941833 196.8878 6.124550 197.3699 5.353973 197.8520 5.116730 198.3341 5.418739 198.8163 5.874474 199.2984 6.501785 199.7805 7.205864 200.2626 7.477394 200.7447 7.215645 201.2268 6.901115 201.7090 7.143524 202.1911 8.045380 202.6732 8.496445 203.1553 8.090981 203.6374 6.996796 204.1195 6.311073 204.6017 6.079521 205.0838 6.134804 205.5659 6.393135 206.0480 6.910088 206.5301 7.304665 207.0122 7.464050 207.4944 7.398323 207.9765 7.557739 208.4586 8.069183 208.9407 8.605736 209.4228 8.686417 209.9049 8.164215 210.3871 7.788589 210.8692 7.718620 211.3513 7.964149 211.8334 8.586929 212.3155 9.701073 212.7976 10.86445 213.2798 11.80331 213.7619 12.27274 214.2440 12.56123 214.7261 12.77631 215.2082 12.88256 215.6903 13.16943 216.1725 13.75935 216.6546 14.45961 217.1367 14.89877 217.6188 15.09218 218.1009 15.41288 218.5830 15.93388 219.0651 16.30253 219.5473 16.60393 220.0294 16.87179 220.5115 17.06326 220.9936 17.04982 221.4757 16.87840 221.9578 17.05159 222.4400 17.84593 222.9221 19.41953 223.4042 20.32715 223.8863 20.48872 224.3684 20.29073 224.8505 20.30458 225.3327 20.74387 225.8148 20.93148 226.2969 20.57850 226.7790 19.58762 227.2611 19.13268 227.7432 19.38016 228.2254 19.98598 228.7075 20.61942 229.1896 21.49500 229.6717 21.98756 230.1538 21.84598 230.6359 20.98785 231.1181 20.37600 231.6002 20.10052 232.0823 19.98789 232.5644 19.84988 233.0465 19.66018 233.5286 19.44258 234.0108 19.23392 234.4929 19.00593 234.9750 18.73111 235.4571 18.44752 235.9392 18.07866 236.4213 17.51065 236.9035 16.53868 237.3856 15.75739 237.8677 15.35985 238.3498 15.38222 238.8319 15.22885 239.3140 14.81700 239.7962 14.30761 240.2783 13.88220 240.7604 13.68151 241.2425 13.29652 241.7246 12.56963 242.2067 11.46301 242.6889 10.59207 243.1710 10.05728 243.6531 9.655273 244.1352 9.156700 244.6173 8.375999 245.0994 7.866379 245.5816 7.941422 246.0637 8.625000 246.5458 8.452026 247.0279 6.893379 247.5100 5.017227 247.9921 3.865715 248.4743 3.785217 248.9564 3.718002 249.4385 3.493782 249.9206 3.115685 250.4027 2.686035 250.8848 2.083389 251.3670 1.567192 251.8491 1.398384 252.3312 1.752701 252.8133 2.074257 253.2954 2.288040 253.7775 2.396713 254.2597 2.450768 254.7418 2.457916 255.2239 2.397537 255.7060 2.252594 256.1881 2.010674 256.6702 1.690285 257.1523 1.199867 257.6345 0.5926210 258.1166 0.3939360 258.5987 0.8700640 259.0808 1.361748 259.5629 1.281639 260.0450 0.2368090 260.5272 0.2564320 261.0093 0.2203140 261.4914 1.426552 261.9735 1.986870 262.4556 1.658089 262.9377 1.145706 263.4199 0.8850400 263.9020 0.9566730 264.3841 0.9318620 264.8662 0.7667470 265.3483 0.4940950 265.8304 0.1929320 266.3126 0.1932600 266.7947 0.4415440 267.2768 0.4110110 267.7589 5.0415002E-02 268.2410 0.3070680 268.7231 0.3118210 269.2053 9.2735000E-02 269.6874 0.3694690 270.1695 1.266556 270.6516 1.909538 271.1337 1.742340 271.6158 0.4709320 272.0980 0.1182630 272.5801 0.2703400 273.0622 1.219162 273.5443 1.883354 274.0264 2.287544 274.5085 2.329124 274.9907 1.794479 275.4728 0.5730130 275.9549 0.2232740 276.4370 0.4605710 276.9191 0.4187240 277.4012 0.6643140 277.8834 1.279495 278.3655 1.728180 278.8476 1.557442 279.3297 0.7229540 279.8118 0.7999340 280.2939 2.033424 280.7761 3.673523 281.2582 4.531937 281.7403 4.537773 282.2224 4.585800 282.7045 5.018936 283.1866 5.811699 283.6688 6.647018 284.1509 7.503586 284.6330 8.476006 285.1151 9.746117 285.5972 11.31151 286.0793 12.89011 286.5615 14.38542 287.0436 15.81387 287.5257 17.19154 288.0078 18.48626 288.4899 19.93706 288.9720 21.81013 289.4542 24.09067 289.9363 26.62539 290.4184 29.39232 290.9005 32.36800 291.3826 35.62833 291.8647 39.20198 292.3469 42.82713 292.8290 46.15481 293.3111 49.29671 293.7932 52.95158 294.2753 57.41530 294.7574 62.36165 295.2396 67.28905 295.7217 72.19718 296.2038 76.66917 296.6859 80.48709 297.1680 83.58592 297.6501 85.90713 298.1323 87.59254 298.6144 88.22093 299.0965 86.99887 299.5786 84.04346 300.0607 80.29185 300.5428 76.07269 301.0250 71.47972 301.5071 66.48023 301.9892 60.89156 302.4713 55.39384 302.9534 50.78404 303.4355 46.89417 303.9177 42.98822 304.3998 38.42583 304.8819 33.75887 305.3640 29.85860 305.8461 26.82268 306.3282 24.20141 306.8104 21.57771 307.2925 19.04752 307.7746 16.86745 308.2567 15.43315 308.7388 14.23922 309.2209 12.66165 309.7031 10.65528 310.1852 9.015450 310.6673 8.645859 311.1494 8.891701 311.6315 8.817764 312.1136 7.669769 312.5958 6.379341 313.0779 5.611572 313.5600 5.333961 314.0421 5.037628 314.5242 4.325745 315.0063 3.500847 315.4885 2.865463 315.9706 2.668816 316.4527 2.545708 316.9348 2.319557 317.4169 1.997910 317.8990 1.646484 318.3812 1.402992 318.8633 1.140251 319.3454 0.6963960 319.8275 0.3154450 320.3096 1.029228 320.7917 1.037979 321.2739 0.5413440 321.7560 4.4280998E-02 322.2381 0.5769880 322.7202 0.9629290 323.2023 0.8228450 323.6844 0.3051910 324.1666 0.9344410 324.6487 0.3172230 325.1308 0.8930970 325.6129 1.674095 326.0950 1.366859 326.5771 1.048058 327.0593 1.129547 327.5414 1.819649 328.0235 1.971565 328.5056 0.7221980 328.9877 0.6868670 329.4698 0.9286270 329.9520 1.437050 330.4341 3.116302 330.9162 3.238243 331.3983 1.751984 331.8804 0.9519650 332.3625 1.301025 332.8447 2.020882 333.3268 2.549095 333.8089 2.608742 334.2910 2.882843 334.7731 3.597878 335.2552 4.623711 335.7374 5.152107 336.2195 4.919884 336.7016 4.596397 337.1837 4.551910 337.6658 4.877060 338.1479 5.267609 338.6301 5.697906 339.1122 6.163330 339.5943 6.671448 340.0764 7.229927 340.5585 7.787170 341.0406 8.284256 341.5227 8.718689 342.0049 9.234200 342.4870 9.839561 342.9691 10.51641 343.4512 11.26804 343.9333 12.11306 344.4154 12.87148 344.8976 13.44102 345.3797 13.87128 345.8618 14.40617 346.3439 15.08479 346.8260 15.64925 347.3081 15.62615 347.7903 15.15012 348.2724 15.18096 348.7545 16.14237 349.2366 17.56837 349.7187 18.51884 350.2008 19.02943 350.6830 19.49111 351.1651 20.31171 351.6472 21.29773 352.1293 21.94319 352.6114 22.08759 353.0935 22.05771 353.5757 22.09930 354.0578 22.25125 354.5399 22.64637 355.0220 23.54995 355.5041 24.65585 355.9862 25.53551 356.4684 26.10618 356.9505 26.72856 357.4326 27.83755 357.9147 29.15906 358.3968 30.24579 358.8789 30.60777 359.3611 30.91180 359.8432 31.66307 360.3253 32.85670 360.8074 34.07343 361.2895 35.13362 361.7716 36.11038 362.2538 37.07043 362.7359 38.02132 363.2180 38.97345 363.7001 39.93539 364.1822 40.90991 364.6643 41.89938 365.1465 42.77123 365.6286 43.75551 366.1107 44.99957 366.5928 46.67261 367.0749 48.28017 367.5570 49.77818 368.0392 51.19913 368.5213 52.56055 369.0034 53.42982 369.4855 54.60268 369.9676 56.53349 370.4497 59.52336 370.9319 61.69531 371.4140 62.36902 371.8961 62.60573 372.3782 63.47881 372.8603 65.44504 373.3424 67.27197 373.8246 68.75193 374.3067 69.89113 374.7888 70.97029 375.2709 72.02074 375.7530 73.00809 376.2351 73.96611 376.7173 74.98860 377.1994 75.57574 377.6815 75.53890 378.1636 75.17594 378.6457 75.35880 379.1278 76.26242 379.6100 76.92197 380.0921 76.61224 380.5742 75.39951 381.0563 75.16724 381.5384 76.10503 382.0205 77.25337 382.5027 77.38503 382.9848 76.58975 383.4669 75.85839 383.9490 75.53742 384.4311 75.47403 384.9132 75.41496 385.3954 75.35216 385.8775 75.06286 386.3596 73.96680 386.8417 72.53409 387.3238 71.90823 387.8059 72.68568 388.2881 73.67749 388.7702 73.64801 389.2523 72.77484 389.7344 71.60647 390.2165 70.13442 390.6986 68.66766 391.1808 67.56279 391.6629 66.88654 392.1450 66.22503 392.6271 65.40845 393.1092 64.42827 393.5913 63.28143 394.0735 61.79610 394.5556 60.28610 395.0377 58.87370 395.5198 57.56161 396.0019 56.32741 396.4840 55.26059 396.9662 54.21053 397.4483 53.06822 397.9304 51.60457 398.4125 50.33769 398.8946 49.67767 399.3767 49.27493 399.8589 48.26864 400.3410 45.79105 400.8231 43.45442 401.3052 41.79318 401.7873 41.03992 402.2694 40.04667 402.7516 38.65709 403.2337 37.14214 403.7158 35.81148 404.1979 34.75571 404.6800 33.70334 405.1621 32.68048 405.6443 31.63223 406.1264 30.07480 406.6085 27.75026 407.0906 25.57775 407.5727 24.34798 408.0548 24.16290 408.5370 23.62865 409.0191 22.59700 409.5012 21.24830 409.9833 19.82771 410.4654 18.33616 410.9475 16.95793 411.4297 15.90324 411.9118 15.04607 412.3939 13.86962 412.8760 12.36481 413.3581 10.93275 413.8402 10.02100 414.3224 9.499405 414.8045 9.028152 415.2866 8.545914 415.7687 8.027733 416.2508 7.426880 416.7329 6.755371 417.2151 6.055206 417.6972 5.305573 418.1793 4.560287 418.6614 3.852936 419.1435 3.192528 419.6256 2.588966 420.1078 2.123039 420.5899 1.706558 421.0720 1.189621 421.5541 0.3238370 422.0362 0.4626310 422.5183 1.011505 423.0005 1.312965 423.4826 1.478752 423.9647 1.347313 424.4468 1.203606 424.9289 1.233780 425.4110 1.716934 425.8932 2.051582 426.3753 2.100220 426.8574 1.995590 427.3395 2.070862 427.8216 2.562645 428.3037 2.916733 428.7859 2.906998 429.2680 2.464508 429.7501 2.163193 430.2322 2.090240 430.7143 2.036301 431.1964 1.731483 431.6786 1.104149 432.1607 0.6155780 432.6428 0.4155730 433.1249 0.3780750 433.6070 3.9145999E-02 434.0891 0.6347500 434.5713 1.253815 435.0534 1.557709 435.5355 1.591339 436.0176 1.468185 436.4997 1.127258 436.9818 0.9416350 437.4640 1.540062 437.9461 2.700806 438.4282 3.718567 438.9103 4.241219 439.3924 4.509628 439.8745 4.743980 440.3566 4.956512 440.8387 5.264786 441.3209 5.719513 441.8030 6.319702 442.2851 7.090462 442.7672 8.113022 443.2493 9.131432 443.7314 9.864357 444.2136 10.51122 444.6957 11.41905 445.1778 13.10117 445.6599 14.70800 446.1420 15.86420 446.6241 16.51701 447.1063 17.14803 447.5884 17.50429 448.0705 18.06577 448.5526 19.19279 449.0347 21.30319 449.5168 23.38984 449.9990 25.38913 450.4811 27.34961 450.9632 29.38000 451.4453 31.53494 451.9274 33.67263 452.4095 35.66670 452.8917 37.43554 453.3738 39.74355 453.8559 42.69100 454.3380 45.88782 454.8201 48.84248 455.3022 51.52612 455.7844 54.53149 456.2665 57.98100 456.7486 61.79153 457.2307 65.83117 457.7128 70.07564 458.1949 74.66776 458.6771 79.54826 459.1592 84.84365 459.6413 90.75031 460.1234 97.30471 460.6055 104.2486 461.0876 111.4213 461.5698 118.8742 462.0519 126.7082 462.5340 135.0572 463.0161 143.7806 463.4982 152.8557 463.9803 162.3247 464.4625 172.2290 464.9446 182.7092 465.4267 193.7581 465.9088 205.3867 466.3909 217.8047 466.8730 230.5513 467.3552 243.0947 467.8373 256.0750 468.3194 270.3108 468.8015 286.4008 469.2836 303.0949 469.7657 320.1816 470.2479 337.7956 470.7300 355.7589 471.2121 373.7066 471.6942 392.5524 472.1763 412.9733 472.6584 434.8862 473.1406 457.5281 473.6227 480.9361 474.1048 504.7125 474.5869 527.8976 475.0690 550.4608 475.5511 574.4452 476.0333 601.1899 476.5154 629.3944 476.9975 656.7004 477.4796 683.1057 477.9617 708.3719 478.4438 733.0034 478.9260 756.2373 479.4081 776.5850 479.8902 793.7515 480.3723 808.4999 480.8544 822.5322 481.3365 834.6631 481.8187 842.8582 482.3008 846.6365 482.7829 845.8951 483.2650 840.3724 483.7471 830.1450 484.2292 816.1098 484.7114 797.5817 485.1935 775.8939 485.6756 751.8354 486.1577 724.4771 486.6398 696.6115 487.1219 668.6598 487.6041 640.0184 488.0862 610.6069 488.5683 578.9741 489.0504 548.1799 489.5325 519.0215 490.0146 491.3317 490.4968 464.7923 490.9789 439.6419 491.4610 415.6748 491.9431 392.4461 492.4252 370.2999 492.9073 350.3463 493.3895 332.9290 493.8716 316.7490 494.3537 299.3221 494.8358 281.1671 495.3179 264.4227 495.8000 250.2569 496.2822 237.7619 496.7643 225.7426 497.2464 214.1149 497.7285 203.0760 498.2106 192.5891 498.6927 182.7300 499.1749 173.4655 499.6570 164.9057 500.1391 156.6591 500.6212 148.4406 501.1033 140.4570 501.5854 132.8500 502.0676 125.5916 502.5497 118.9172 503.0318 113.0166 503.5139 107.7681 503.9960 102.5625 504.4781 96.89272 504.9603 91.60206 505.4424 87.05319 505.9245 83.33868 506.4066 79.58794 506.8887 75.71045 507.3708 71.95532 507.8530 68.53717 508.3351 65.56798 508.8172 62.95612 509.2993 60.80222 509.7814 58.76683 510.2635 55.84927 510.7457 52.05775 511.2278 48.81122 511.7099 47.27090 512.1920 46.77046 512.6741 45.68034 513.1563 43.95909 513.6384 42.11832 514.1205 40.67970 514.6026 39.38350 515.0847 37.76609 515.5668 35.42777 516.0490 33.18451 516.5311 31.73756 517.0132 30.78757 517.4953 29.71222 517.9774 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