#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-05-24 15:22:18 +0300 (Thu, 24 May 2018) $
#$Revision: 684 $
#$URL: svn://172.16.1.111/rod/cif/1/00/02/1000202.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000202
loop_
_publ_author_name
'Cruciani, G.'
'Gualtieri, A.'
_publ_section_title
;
 Dehydration dynamics of analcime by in situ synchrotron powder
 diffraction Sample at T = 298 K
;
_journal_name_full               'American Mineralogist'
_journal_page_first              112
_journal_page_last               119
_journal_volume                  84
_journal_year                    1999
_chemical_compound_source        R060023
_chemical_formula_sum            'Al1.9 H4 Na1.95 O14 Si4.1'
_chemical_name_mineral           Analcime
_space_group_IT_number           142
_symmetry_space_group_name_Hall  '-I 4bd 2c'
_symmetry_space_group_name_H-M   'I 41/a c d :2'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            8
_cell_length_a                   13.7295
_cell_length_b                   13.7295
_cell_length_c                   13.7036
_cell_volume                     2583.117
_diffrn_ambient_temperature      298
_exptl_crystal_density_diffrn    2.259
_cod_original_sg_symbol_H-M      'I 41/a c d'
_cod_original_formula_sum        '(Si4.1 Al1.9) Na1.95 O14 H4'
_cod_database_code               9002000
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 15
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R060023.rod
_rod_data_source.block           3500000
_rod_database.code               1000202
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9002000 COD http://www.crystallography.net/cod/9002000.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
166.0323 0.0000000E+00
166.5145 0.7153930
166.9966 0.4946290
167.4787 8.1179999E-03
167.9608 0.1086880
168.4429 0.9488220
168.9250 1.817078
169.4071 2.450150
169.8893 2.860405
170.3714 3.051018
170.8535 3.699852
171.3356 3.316536
171.8177 2.692207
172.2998 1.871681
172.7820 1.044548
173.2641 0.8193210
173.7462 1.017029
174.2283 1.123924
174.7104 0.4593350
175.1925 0.3288730
175.6747 0.3658750
176.1568 0.5850370
176.6389 1.562744
177.1210 1.528366
177.6031 0.7823100
178.0852 0.2711870
178.5674 0.8263780
179.0495 1.873711
179.5316 2.506065
180.0137 2.567253
180.4958 2.319641
180.9779 1.885071
181.4601 1.330780
181.9422 1.002747
182.4243 1.254623
182.9064 1.880753
183.3885 2.474968
183.8706 3.046127
184.3528 3.430267
184.8349 3.073334
185.3170 2.079765
185.7991 1.474442
186.2812 2.407188
186.7633 4.406731
187.2455 5.776917
187.7276 6.125893
188.2097 5.885307
188.6918 5.831085
189.1739 5.965050
189.6560 6.089775
190.1382 5.951660
190.6203 5.620186
191.1024 5.592484
191.5845 6.108276
192.0666 6.853729
192.5487 6.984482
193.0309 6.451096
193.5130 5.900620
193.9951 5.921227
194.4772 6.480186
194.9593 6.935745
195.4414 7.208519
195.9236 7.276955
196.4057 6.941833
196.8878 6.124550
197.3699 5.353973
197.8520 5.116730
198.3341 5.418739
198.8163 5.874474
199.2984 6.501785
199.7805 7.205864
200.2626 7.477394
200.7447 7.215645
201.2268 6.901115
201.7090 7.143524
202.1911 8.045380
202.6732 8.496445
203.1553 8.090981
203.6374 6.996796
204.1195 6.311073
204.6017 6.079521
205.0838 6.134804
205.5659 6.393135
206.0480 6.910088
206.5301 7.304665
207.0122 7.464050
207.4944 7.398323
207.9765 7.557739
208.4586 8.069183
208.9407 8.605736
209.4228 8.686417
209.9049 8.164215
210.3871 7.788589
210.8692 7.718620
211.3513 7.964149
211.8334 8.586929
212.3155 9.701073
212.7976 10.86445
213.2798 11.80331
213.7619 12.27274
214.2440 12.56123
214.7261 12.77631
215.2082 12.88256
215.6903 13.16943
216.1725 13.75935
216.6546 14.45961
217.1367 14.89877
217.6188 15.09218
218.1009 15.41288
218.5830 15.93388
219.0651 16.30253
219.5473 16.60393
220.0294 16.87179
220.5115 17.06326
220.9936 17.04982
221.4757 16.87840
221.9578 17.05159
222.4400 17.84593
222.9221 19.41953
223.4042 20.32715
223.8863 20.48872
224.3684 20.29073
224.8505 20.30458
225.3327 20.74387
225.8148 20.93148
226.2969 20.57850
226.7790 19.58762
227.2611 19.13268
227.7432 19.38016
228.2254 19.98598
228.7075 20.61942
229.1896 21.49500
229.6717 21.98756
230.1538 21.84598
230.6359 20.98785
231.1181 20.37600
231.6002 20.10052
232.0823 19.98789
232.5644 19.84988
233.0465 19.66018
233.5286 19.44258
234.0108 19.23392
234.4929 19.00593
234.9750 18.73111
235.4571 18.44752
235.9392 18.07866
236.4213 17.51065
236.9035 16.53868
237.3856 15.75739
237.8677 15.35985
238.3498 15.38222
238.8319 15.22885
239.3140 14.81700
239.7962 14.30761
240.2783 13.88220
240.7604 13.68151
241.2425 13.29652
241.7246 12.56963
242.2067 11.46301
242.6889 10.59207
243.1710 10.05728
243.6531 9.655273
244.1352 9.156700
244.6173 8.375999
245.0994 7.866379
245.5816 7.941422
246.0637 8.625000
246.5458 8.452026
247.0279 6.893379
247.5100 5.017227
247.9921 3.865715
248.4743 3.785217
248.9564 3.718002
249.4385 3.493782
249.9206 3.115685
250.4027 2.686035
250.8848 2.083389
251.3670 1.567192
251.8491 1.398384
252.3312 1.752701
252.8133 2.074257
253.2954 2.288040
253.7775 2.396713
254.2597 2.450768
254.7418 2.457916
255.2239 2.397537
255.7060 2.252594
256.1881 2.010674
256.6702 1.690285
257.1523 1.199867
257.6345 0.5926210
258.1166 0.3939360
258.5987 0.8700640
259.0808 1.361748
259.5629 1.281639
260.0450 0.2368090
260.5272 0.2564320
261.0093 0.2203140
261.4914 1.426552
261.9735 1.986870
262.4556 1.658089
262.9377 1.145706
263.4199 0.8850400
263.9020 0.9566730
264.3841 0.9318620
264.8662 0.7667470
265.3483 0.4940950
265.8304 0.1929320
266.3126 0.1932600
266.7947 0.4415440
267.2768 0.4110110
267.7589 5.0415002E-02
268.2410 0.3070680
268.7231 0.3118210
269.2053 9.2735000E-02
269.6874 0.3694690
270.1695 1.266556
270.6516 1.909538
271.1337 1.742340
271.6158 0.4709320
272.0980 0.1182630
272.5801 0.2703400
273.0622 1.219162
273.5443 1.883354
274.0264 2.287544
274.5085 2.329124
274.9907 1.794479
275.4728 0.5730130
275.9549 0.2232740
276.4370 0.4605710
276.9191 0.4187240
277.4012 0.6643140
277.8834 1.279495
278.3655 1.728180
278.8476 1.557442
279.3297 0.7229540
279.8118 0.7999340
280.2939 2.033424
280.7761 3.673523
281.2582 4.531937
281.7403 4.537773
282.2224 4.585800
282.7045 5.018936
283.1866 5.811699
283.6688 6.647018
284.1509 7.503586
284.6330 8.476006
285.1151 9.746117
285.5972 11.31151
286.0793 12.89011
286.5615 14.38542
287.0436 15.81387
287.5257 17.19154
288.0078 18.48626
288.4899 19.93706
288.9720 21.81013
289.4542 24.09067
289.9363 26.62539
290.4184 29.39232
290.9005 32.36800
291.3826 35.62833
291.8647 39.20198
292.3469 42.82713
292.8290 46.15481
293.3111 49.29671
293.7932 52.95158
294.2753 57.41530
294.7574 62.36165
295.2396 67.28905
295.7217 72.19718
296.2038 76.66917
296.6859 80.48709
297.1680 83.58592
297.6501 85.90713
298.1323 87.59254
298.6144 88.22093
299.0965 86.99887
299.5786 84.04346
300.0607 80.29185
300.5428 76.07269
301.0250 71.47972
301.5071 66.48023
301.9892 60.89156
302.4713 55.39384
302.9534 50.78404
303.4355 46.89417
303.9177 42.98822
304.3998 38.42583
304.8819 33.75887
305.3640 29.85860
305.8461 26.82268
306.3282 24.20141
306.8104 21.57771
307.2925 19.04752
307.7746 16.86745
308.2567 15.43315
308.7388 14.23922
309.2209 12.66165
309.7031 10.65528
310.1852 9.015450
310.6673 8.645859
311.1494 8.891701
311.6315 8.817764
312.1136 7.669769
312.5958 6.379341
313.0779 5.611572
313.5600 5.333961
314.0421 5.037628
314.5242 4.325745
315.0063 3.500847
315.4885 2.865463
315.9706 2.668816
316.4527 2.545708
316.9348 2.319557
317.4169 1.997910
317.8990 1.646484
318.3812 1.402992
318.8633 1.140251
319.3454 0.6963960
319.8275 0.3154450
320.3096 1.029228
320.7917 1.037979
321.2739 0.5413440
321.7560 4.4280998E-02
322.2381 0.5769880
322.7202 0.9629290
323.2023 0.8228450
323.6844 0.3051910
324.1666 0.9344410
324.6487 0.3172230
325.1308 0.8930970
325.6129 1.674095
326.0950 1.366859
326.5771 1.048058
327.0593 1.129547
327.5414 1.819649
328.0235 1.971565
328.5056 0.7221980
328.9877 0.6868670
329.4698 0.9286270
329.9520 1.437050
330.4341 3.116302
330.9162 3.238243
331.3983 1.751984
331.8804 0.9519650
332.3625 1.301025
332.8447 2.020882
333.3268 2.549095
333.8089 2.608742
334.2910 2.882843
334.7731 3.597878
335.2552 4.623711
335.7374 5.152107
336.2195 4.919884
336.7016 4.596397
337.1837 4.551910
337.6658 4.877060
338.1479 5.267609
338.6301 5.697906
339.1122 6.163330
339.5943 6.671448
340.0764 7.229927
340.5585 7.787170
341.0406 8.284256
341.5227 8.718689
342.0049 9.234200
342.4870 9.839561
342.9691 10.51641
343.4512 11.26804
343.9333 12.11306
344.4154 12.87148
344.8976 13.44102
345.3797 13.87128
345.8618 14.40617
346.3439 15.08479
346.8260 15.64925
347.3081 15.62615
347.7903 15.15012
348.2724 15.18096
348.7545 16.14237
349.2366 17.56837
349.7187 18.51884
350.2008 19.02943
350.6830 19.49111
351.1651 20.31171
351.6472 21.29773
352.1293 21.94319
352.6114 22.08759
353.0935 22.05771
353.5757 22.09930
354.0578 22.25125
354.5399 22.64637
355.0220 23.54995
355.5041 24.65585
355.9862 25.53551
356.4684 26.10618
356.9505 26.72856
357.4326 27.83755
357.9147 29.15906
358.3968 30.24579
358.8789 30.60777
359.3611 30.91180
359.8432 31.66307
360.3253 32.85670
360.8074 34.07343
361.2895 35.13362
361.7716 36.11038
362.2538 37.07043
362.7359 38.02132
363.2180 38.97345
363.7001 39.93539
364.1822 40.90991
364.6643 41.89938
365.1465 42.77123
365.6286 43.75551
366.1107 44.99957
366.5928 46.67261
367.0749 48.28017
367.5570 49.77818
368.0392 51.19913
368.5213 52.56055
369.0034 53.42982
369.4855 54.60268
369.9676 56.53349
370.4497 59.52336
370.9319 61.69531
371.4140 62.36902
371.8961 62.60573
372.3782 63.47881
372.8603 65.44504
373.3424 67.27197
373.8246 68.75193
374.3067 69.89113
374.7888 70.97029
375.2709 72.02074
375.7530 73.00809
376.2351 73.96611
376.7173 74.98860
377.1994 75.57574
377.6815 75.53890
378.1636 75.17594
378.6457 75.35880
379.1278 76.26242
379.6100 76.92197
380.0921 76.61224
380.5742 75.39951
381.0563 75.16724
381.5384 76.10503
382.0205 77.25337
382.5027 77.38503
382.9848 76.58975
383.4669 75.85839
383.9490 75.53742
384.4311 75.47403
384.9132 75.41496
385.3954 75.35216
385.8775 75.06286
386.3596 73.96680
386.8417 72.53409
387.3238 71.90823
387.8059 72.68568
388.2881 73.67749
388.7702 73.64801
389.2523 72.77484
389.7344 71.60647
390.2165 70.13442
390.6986 68.66766
391.1808 67.56279
391.6629 66.88654
392.1450 66.22503
392.6271 65.40845
393.1092 64.42827
393.5913 63.28143
394.0735 61.79610
394.5556 60.28610
395.0377 58.87370
395.5198 57.56161
396.0019 56.32741
396.4840 55.26059
396.9662 54.21053
397.4483 53.06822
397.9304 51.60457
398.4125 50.33769
398.8946 49.67767
399.3767 49.27493
399.8589 48.26864
400.3410 45.79105
400.8231 43.45442
401.3052 41.79318
401.7873 41.03992
402.2694 40.04667
402.7516 38.65709
403.2337 37.14214
403.7158 35.81148
404.1979 34.75571
404.6800 33.70334
405.1621 32.68048
405.6443 31.63223
406.1264 30.07480
406.6085 27.75026
407.0906 25.57775
407.5727 24.34798
408.0548 24.16290
408.5370 23.62865
409.0191 22.59700
409.5012 21.24830
409.9833 19.82771
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410.9475 16.95793
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411.9118 15.04607
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413.3581 10.93275
413.8402 10.02100
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414.8045 9.028152
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415.7687 8.027733
416.2508 7.426880
416.7329 6.755371
417.2151 6.055206
417.6972 5.305573
418.1793 4.560287
418.6614 3.852936
419.1435 3.192528
419.6256 2.588966
420.1078 2.123039
420.5899 1.706558
421.0720 1.189621
421.5541 0.3238370
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422.5183 1.011505
423.0005 1.312965
423.4826 1.478752
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424.4468 1.203606
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425.8932 2.051582
426.3753 2.100220
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430.2322 2.090240
430.7143 2.036301
431.1964 1.731483
431.6786 1.104149
432.1607 0.6155780
432.6428 0.4155730
433.1249 0.3780750
433.6070 3.9145999E-02
434.0891 0.6347500
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435.0534 1.557709
435.5355 1.591339
436.0176 1.468185
436.4997 1.127258
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437.4640 1.540062
437.9461 2.700806
438.4282 3.718567
438.9103 4.241219
439.3924 4.509628
439.8745 4.743980
440.3566 4.956512
440.8387 5.264786
441.3209 5.719513
441.8030 6.319702
442.2851 7.090462
442.7672 8.113022
443.2493 9.131432
443.7314 9.864357
444.2136 10.51122
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445.1778 13.10117
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448.0705 18.06577
448.5526 19.19279
449.0347 21.30319
449.5168 23.38984
449.9990 25.38913
450.4811 27.34961
450.9632 29.38000
451.4453 31.53494
451.9274 33.67263
452.4095 35.66670
452.8917 37.43554
453.3738 39.74355
453.8559 42.69100
454.3380 45.88782
454.8201 48.84248
455.3022 51.52612
455.7844 54.53149
456.2665 57.98100
456.7486 61.79153
457.2307 65.83117
457.7128 70.07564
458.1949 74.66776
458.6771 79.54826
459.1592 84.84365
459.6413 90.75031
460.1234 97.30471
460.6055 104.2486
461.0876 111.4213
461.5698 118.8742
462.0519 126.7082
462.5340 135.0572
463.0161 143.7806
463.4982 152.8557
463.9803 162.3247
464.4625 172.2290
464.9446 182.7092
465.4267 193.7581
465.9088 205.3867
466.3909 217.8047
466.8730 230.5513
467.3552 243.0947
467.8373 256.0750
468.3194 270.3108
468.8015 286.4008
469.2836 303.0949
469.7657 320.1816
470.2479 337.7956
470.7300 355.7589
471.2121 373.7066
471.6942 392.5524
472.1763 412.9733
472.6584 434.8862
473.1406 457.5281
473.6227 480.9361
474.1048 504.7125
474.5869 527.8976
475.0690 550.4608
475.5511 574.4452
476.0333 601.1899
476.5154 629.3944
476.9975 656.7004
477.4796 683.1057
477.9617 708.3719
478.4438 733.0034
478.9260 756.2373
479.4081 776.5850
479.8902 793.7515
480.3723 808.4999
480.8544 822.5322
481.3365 834.6631
481.8187 842.8582
482.3008 846.6365
482.7829 845.8951
483.2650 840.3724
483.7471 830.1450
484.2292 816.1098
484.7114 797.5817
485.1935 775.8939
485.6756 751.8354
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