#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-05-24 15:22:59 +0300 (Thu, 24 May 2018) $
#$Revision: 695 $
#$URL: svn://172.16.1.111/rod/cif/1/00/02/1000207.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000207
loop_
_publ_author_name
'Morgenstern-Badarau I'
_publ_section_title
;
 Effet Jahn-Teller et structure cristalline de l'hydroxyde CuSn(OH)6
;
_journal_name_full               'Journal of Solid State Chemistry'
_journal_page_first              399
_journal_page_last               406
_journal_paper_doi               10.1016/S0022-4596(76)80010-2
_journal_volume                  17
_journal_year                    1976
_chemical_compound_source        R060153
_chemical_formula_sum            'Cu H6 O6 Sn'
_chemical_name_mineral           Mushistonite
_space_group_IT_number           134
_symmetry_space_group_name_Hall  '-P 4ac 2bc'
_symmetry_space_group_name_H-M   'P 42/n n m :2'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_length_a                   7.586
_cell_length_b                   7.586
_cell_length_c                   8.103
_cell_volume                     466.307
_exptl_crystal_density_diffrn    4.050
_cod_original_sg_symbol_H-M      'P 42/n n m'
_cod_original_formula_sum        'Cu Sn (O6 H6)'
_cod_database_code               9009750
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 15
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R060153.rod
_rod_data_source.block           3500000
_rod_database.code               1000207
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9009750 COD http://www.crystallography.net/cod/9009750.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
164.912 0.000
165.394 32.884
165.876 60.252
166.359 61.366
166.841 46.615
167.323 39.779
167.805 44.810
168.287 48.871
168.769 41.450
169.251 17.462
169.734 2.393
170.216 1.096
170.698 19.163
171.180 35.164
171.662 34.111
172.144 26.688
172.626 25.879
173.108 34.581
173.590 47.084
174.072 61.900
174.555 75.681
175.037 83.927
175.519 78.646
176.001 63.815
176.483 48.667
176.965 35.978
177.447 26.670
177.930 21.724
178.412 21.986
178.894 25.017
179.376 29.866
179.858 35.610
180.340 48.497
180.822 71.886
181.304 94.803
181.786 100.301
182.268 87.456
182.751 70.739
183.233 68.310
183.715 78.008
184.197 85.565
184.679 77.460
185.161 59.668
185.643 53.896
186.125 61.677
186.608 75.562
187.090 91.310
187.572 108.730
188.054 117.881
188.536 100.708
189.018 65.792
189.500 59.676
189.982 92.795
190.464 145.222
190.947 182.097
191.429 190.568
191.911 182.080
192.393 157.267
192.875 126.708
193.357 125.006
193.839 136.213
194.321 149.090
194.804 151.375
195.286 127.191
195.768 109.927
196.250 126.141
196.732 166.463
197.214 184.241
197.696 179.995
198.178 161.382
198.661 148.440
199.143 141.521
199.625 144.131
200.107 164.150
200.589 198.012
201.071 216.271
201.553 209.073
202.035 181.597
202.517 153.524
202.999 125.776
203.482 105.698
203.964 104.802
204.446 127.137
204.928 146.219
205.410 154.133
205.892 150.732
206.374 145.492
206.857 137.765
207.339 128.864
207.821 121.141
208.303 115.490
208.785 107.541
209.267 94.420
209.749 74.920
210.231 60.971
210.713 53.356
211.195 50.929
211.678 53.729
212.160 65.755
212.642 73.196
213.124 69.303
213.606 50.707
214.088 34.242
214.570 20.638
215.053 9.152
215.535 2.854
216.017 18.700
216.499 28.363
216.981 25.107
217.463 2.915
217.945 13.763
218.427 24.603
218.909 28.942
219.391 24.525
219.874 8.828
220.356 11.731
220.838 36.542
221.320 75.231
221.802 91.733
222.284 72.219
222.766 23.641
223.249 2.364
223.731 21.504
224.213 48.842
224.695 60.950
225.177 48.327
225.659 42.130
226.141 49.590
226.623 68.627
227.105 76.777
227.587 72.405
228.070 59.437
228.552 38.997
229.034 1.772
229.516 22.266
229.998 23.762
230.480 2.540
230.962 9.126
231.445 7.622
231.927 0.762
232.409 4.965
232.891 12.536
233.373 12.758
233.855 0.629
234.337 29.772
234.819 41.613
235.301 28.623
235.783 5.400
236.266 13.063
236.748 30.886
237.230 36.119
237.712 20.376
238.194 22.177
238.676 42.766
239.158 32.981
239.640 7.744
240.123 15.615
240.605 41.520
241.087 57.615
241.569 57.606
242.051 36.500
242.533 24.103
243.015 20.884
243.497 26.261
243.980 41.466
244.462 76.155
244.944 104.221
245.426 115.788
245.908 105.264
246.390 98.429
246.872 93.777
247.354 93.310
247.836 102.275
248.319 129.211
248.801 150.284
249.283 155.754
249.765 139.313
250.247 127.577
250.729 119.499
251.211 116.604
251.693 123.319
252.176 146.659
252.658 167.958
253.140 180.430
253.622 183.124
254.104 179.011
254.586 162.365
255.068 142.123
255.550 141.010
256.032 170.876
256.515 197.753
256.997 204.271
257.479 178.014
257.961 169.380
258.443 185.125
258.925 215.445
259.407 234.833
259.889 235.521
260.371 239.938
260.854 261.234
261.336 309.064
261.818 342.101
262.300 354.552
262.782 353.701
263.264 356.881
263.746 361.398
264.228 375.348
264.711 408.009
265.193 469.236
265.675 509.341
266.157 519.839
266.639 511.569
267.121 512.329
267.603 524.090
268.085 539.543
268.568 555.654
269.050 573.372
269.532 588.759
270.014 600.067
270.496 610.089
270.978 628.508
271.460 658.967
271.942 685.251
272.424 695.334
272.906 685.944
273.389 681.459
273.871 681.116
274.353 688.344
274.835 716.895
275.317 774.486
275.799 828.850
276.281 855.638
276.763 850.894
277.246 860.549
277.728 891.307
278.210 933.292
278.692 964.134
279.174 981.858
279.656 996.407
280.138 1014.906
280.620 1039.073
281.103 1066.062
281.585 1094.462
282.067 1120.881
282.549 1135.739
283.031 1138.586
283.513 1149.772
283.995 1187.188
284.477 1247.887
284.959 1296.728
285.442 1329.841
285.924 1353.516
286.406 1379.469
286.888 1408.688
287.370 1434.875
287.852 1455.444
288.334 1470.545
288.816 1478.779
289.298 1478.633
289.781 1475.997
290.263 1479.894
290.745 1490.191
291.227 1504.808
291.709 1526.474
292.191 1551.000
292.673 1566.180
293.155 1570.497
293.638 1570.602
294.120 1575.514
294.602 1584.581
295.084 1593.966
295.566 1605.425
296.048 1614.883
296.530 1611.373
297.012 1592.759
297.495 1571.057
297.977 1562.248
298.459 1563.612
298.941 1562.718
299.423 1550.824
299.905 1532.620
300.387 1516.690
300.869 1504.945
301.351 1491.683
301.834 1467.954
302.316 1436.804
302.798 1408.705
303.280 1390.617
303.762 1377.714
304.244 1363.602
304.726 1347.765
305.208 1329.900
305.690 1307.991
306.173 1283.589
306.655 1261.033
307.137 1245.745
307.619 1231.237
308.101 1210.211
308.583 1181.259
309.065 1151.117
309.547 1124.816
310.030 1100.675
310.512 1076.245
310.994 1055.101
311.476 1030.229
311.958 993.271
312.440 941.997
312.922 896.561
313.404 871.589
313.887 857.979
314.369 843.042
314.851 823.364
315.333 799.908
315.815 768.614
316.297 728.282
316.779 700.464
317.261 710.679
317.743 731.927
318.225 735.335
318.708 693.940
319.190 650.379
319.672 618.830
320.154 600.321
320.636 588.981
321.118 587.966
321.600 591.297
322.082 593.809
322.565 590.738
323.047 590.449
323.529 597.887
324.011 612.564
324.493 620.356
324.975 615.739
325.457 605.577
325.939 594.605
326.422 572.157
326.904 561.119
327.386 571.346
327.868 600.092
328.350 617.242
328.832 612.023
329.314 603.490
329.796 602.729
330.278 623.137
330.761 631.595
331.243 617.168
331.725 587.644
332.207 580.781
332.689 614.379
333.171 648.511
333.653 661.799
334.135 642.722
334.617 628.481
335.100 618.760
335.582 615.003
336.064 622.749
336.546 646.713
337.028 672.180
337.510 693.200
337.992 710.626
338.474 719.483
338.957 717.480
339.439 708.950
339.921 700.422
340.403 690.448
340.885 687.631
341.367 699.938
341.849 727.586
342.331 744.916
342.814 750.711
343.296 748.973
343.778 743.656
344.260 734.816
344.742 726.333
345.224 718.015
345.706 711.185
346.188 712.036
346.670 721.218
347.153 734.596
347.635 752.565
348.117 772.872
348.599 783.093
349.081 774.663
349.563 755.323
350.045 737.298
350.527 720.558
351.009 711.479
351.492 723.281
351.974 746.551
352.456 761.487
352.938 759.413
353.420 748.864
353.902 737.729
354.384 726.293
354.866 715.643
355.349 711.726
355.831 707.483
356.313 692.607
356.795 656.906
357.277 623.144
357.759 613.332
358.241 620.180
358.723 621.126
359.206 595.932
359.688 565.619
360.170 548.548
360.652 554.393
361.134 556.749
361.616 535.897
362.098 504.605
362.580 486.844
363.062 512.600
363.544 533.793
364.027 522.665
364.509 463.919
364.991 421.802
365.473 421.623
365.955 441.456
366.437 453.042
366.919 447.311
367.401 436.635
367.884 425.357
368.366 415.471
368.848 399.815
369.330 369.218
369.812 338.117
370.294 318.371
370.776 314.182
371.258 310.102
371.741 306.357
372.223 303.709
372.705 297.027
373.187 282.205
373.669 268.648
374.151 263.726
374.633 271.099
375.115 276.934
375.598 280.033
376.080 279.083
376.562 270.456
377.044 252.989
377.526 237.499
378.008 230.562
378.490 231.859
378.972 229.916
379.454 224.258
379.936 215.607
380.419 204.262
380.901 189.533
381.383 176.076
381.865 170.224
382.347 169.993
382.829 159.459
383.311 134.971
383.793 109.812
384.276 104.885
384.758 115.246
385.240 122.302
385.722 111.553
386.204 96.819
386.686 104.331
387.168 132.791
387.650 156.755
388.133 144.670
388.615 117.632
389.097 107.589
389.579 138.169
390.061 170.856
390.543 172.414
391.025 149.368
391.507 127.884
391.989 121.483
392.472 122.415
392.954 125.257
393.436 130.732
393.918 134.671
394.400 136.126
394.882 135.075
395.364 131.371
395.846 114.956
396.328 104.637
396.811 111.957
397.293 146.688
397.775 166.809
398.257 151.954
398.739 125.302
399.221 114.319
399.703 132.888
400.185 152.172
400.668 170.820
401.150 189.044
401.632 191.942
402.114 168.413
402.596 141.303
403.078 127.788
403.560 131.010
404.042 141.221
404.525 161.746
405.007 187.396
405.489 197.835
405.971 189.768
406.453 177.326
406.935 168.222
407.417 162.654
407.899 155.972
408.381 146.495
408.864 138.918
409.346 145.272
409.828 164.571
410.310 177.807
410.792 173.668
411.274 156.620
411.756 139.267
412.238 121.285
412.720 105.597
413.203 96.183
413.685 91.236
414.167 86.672
414.649 81.476
415.131 75.699
415.613 69.447
416.095 62.716
416.577 55.402
417.060 47.378
417.542 38.750
418.024 29.820
418.506 20.784
418.988 10.884
419.470 4.281
419.952 20.792
420.434 29.865
420.917 19.516
421.399 8.167
421.881 4.678
422.363 11.280
422.845 19.776
423.327 31.840
423.809 43.814
424.291 51.199
424.773 43.586
425.255 42.617
425.738 54.081
426.220 77.756
426.702 98.409
427.184 122.085
427.666 135.973
428.148 128.271
428.630 87.289
429.112 58.066
429.595 46.155
430.077 46.792
430.559 47.621
431.041 48.660
431.523 50.091
432.005 53.615
432.487 59.013
432.969 56.384
433.452 43.373
433.934 30.026
434.416 32.819
434.898 48.883
435.380 59.480
435.862 55.635
436.344 43.117
436.826 32.545
437.308 23.724
437.791 13.789
438.273 5.406
438.755 25.736
439.237 32.421
439.719 13.211
440.201 4.588
440.683 5.853
441.165 35.206
441.647 58.006
442.130 56.723
442.612 49.510
443.094 45.959
443.576 46.430
444.058 53.733
444.540 75.848
445.022 103.011
445.504 123.501
445.987 133.947
446.469 139.316
446.951 137.383
447.433 128.699
447.915 126.849
448.397 134.518
448.879 146.469
449.361 160.776
449.844 181.902
450.326 194.282
450.808 193.613
451.290 185.968
451.772 184.377
452.254 188.820
452.736 199.284
453.218 218.329
453.700 245.497
454.183 267.074
454.665 283.031
455.147 295.029
455.629 302.908
456.111 307.530
456.593 314.720
457.075 326.138
457.557 341.277
458.039 359.604
458.522 380.927
459.004 402.625
459.486 424.834
459.968 445.859
460.450 464.070
460.932 478.457
461.414 491.977
461.896 505.881
462.379 520.185
462.861 535.145
463.343 546.664
463.825 562.227
464.307 588.490
464.789 625.773
465.271 659.132
465.753 679.452
466.236 698.072
466.718 723.345
467.200 771.655
467.682 807.436
468.164 819.286
468.646 817.086
469.128 830.574
469.610 870.750
470.092 909.578
470.574 933.275
471.057 937.183
471.539 958.912
472.021 1003.510
472.503 1055.313
472.985 1097.340
473.467 1128.997
473.949 1154.263
474.431 1170.048
474.914 1182.765
475.396 1210.919
475.878 1254.444
476.360 1302.262
476.842 1351.805
477.324 1399.445
477.806 1437.471
478.288 1464.499
478.771 1488.069
479.253 1507.792
479.735 1528.423
480.217 1560.382
480.699 1617.882
481.181 1679.953
481.663 1731.747
482.145 1773.800
482.627 1820.661
483.110 1879.242
483.592 1942.737
484.074 2003.830
484.556 2053.084
485.038 2112.584
485.520 2192.258
486.002 2286.212
486.484 2377.229
486.966 2463.847
487.449 2547.160
487.931 2623.089
488.413 2691.040
488.895 2767.708
489.377 2856.383
489.859 2949.020
490.341 3037.618
490.823 3120.407
491.306 3216.710
491.788 3333.985
492.270 3459.891
492.752 3566.081
493.234 3652.888
493.716 3744.806
494.198 3858.136
494.680 3986.274
495.163 4121.635
495.645 4262.218
496.127 4399.683
496.609 4509.683
497.091 4611.072
497.573 4733.697
498.055 4911.208
498.537 5092.164
499.019 5235.176
499.502 5349.109
499.984 5472.844
500.466 5633.278
500.948 5800.851
501.430 5958.501
501.912 6102.041
502.394 6246.799
502.876 6397.566
503.358 6550.775
503.841 6697.646
504.323 6836.486
504.805 6973.069
505.287 7111.895
505.769 7250.474
506.251 7372.864
506.733 7471.812
507.215 7572.123
507.698 7696.299
508.180 7845.104
508.662 7966.075
509.144 8052.340
509.626 8121.548
510.108 8199.891
510.590 8284.923
511.072 8358.274
511.555 8411.538
512.037 8449.638
512.519 8478.991
513.001 8499.568
513.483 8509.956
513.965 8515.584
514.447 8507.587
514.929 8478.112
515.411 8428.022
515.894 8350.167
516.376 8220.638
516.858 8065.552
517.340 7924.119
517.822 7853.312
518.304 7749.165
518.786 7570.773
519.268 7317.358
519.750 7068.711
520.233 6828.863
520.715 6587.674
521.197 6339.203
521.679 6079.900
522.161 5822.408
522.643 5568.325
523.125 5311.304
523.607 5042.017
524.089 4757.061
524.572 4476.009
525.054 4200.769
525.536 3932.390
526.018 3679.894
526.500 3442.070
526.982 3213.227
527.464 2995.963
527.946 2786.976
528.429 2582.470
528.911 2382.813
529.393 2191.445
529.875 2009.868
530.357 1839.832
530.839 1679.742
531.321 1534.262
531.803 1397.758
532.286 1268.911
532.768 1147.043
533.250 1037.438
533.732 949.845
534.214 867.358
534.696 778.720
535.178 678.411
535.660 587.275
536.143 504.532
536.625 432.313
537.107 377.955
537.589 347.488
538.071 312.333
538.553 262.000
539.035 202.564
539.517 164.763
539.999 149.456
540.482 135.562
540.964 106.340
541.446 67.300
541.928 33.101
542.410 4.300
542.892 18.085
543.374 34.471
543.856 44.068
544.338 45.545
544.821 31.559
545.303 15.814
545.785 4.304
546.267 2.732
546.749 4.632
547.231 5.035
547.713 14.921
548.195 18.897
548.677 13.804
549.160 11.524
549.642 16.552
550.124 21.216
550.606 17.670
551.088 3.022
551.570 11.953
552.052 25.164
552.534 38.187
553.016 57.206
553.499 83.101
553.981 105.574
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