#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-05-24 15:23:10 +0300 (Thu, 24 May 2018) $
#$Revision: 698 $
#$URL: svn://172.16.1.111/rod/cif/1/00/02/1000209.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000209
loop_
_publ_author_name
'Echigo, T.'
'Kimata, M.'
'Maruoka, T.'
_publ_section_title
;
 Crystal-chemical and carbon-isotopic characteristics of karpatite
 (C24H12) from the Picacho Peak Area, San Benito County, California:
 Evidences for the hydrothermal formation Locality: Picacho Peak Area, San
 Benito County, California, USA
;
_journal_name_full               'American Mineralogist'
_journal_page_first              1262
_journal_page_last               1269
_journal_paper_doi               10.2138/am.2007.2509
_journal_volume                  92
_journal_year                    2007
_chemical_compound_source        R060162
_chemical_formula_sum            'C2 H'
_chemical_name_mineral           Carpathite/Karpalite?
_space_group_IT_number           14
_symmetry_space_group_name_Hall  '-P 2yab'
_symmetry_space_group_name_H-M   'P 1 21/a 1'
_cell_angle_alpha                90
_cell_angle_beta                 110.79
_cell_angle_gamma                90
_cell_length_a                   16.094
_cell_length_b                   4.690
_cell_length_c                   10.049
_cell_volume                     709.119
_cod_data_source_file            04410.cif
_cod_data_source_block           global
_cod_original_formula_sum        'C2 H1'
_cod_database_code               9010291
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 15
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R060162.rod
_rod_data_source.block           3500000
_rod_database.code               1000209
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9010291 COD http://www.crystallography.net/cod/9010291.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
150.5283 0.0000000E+00
151.0105 390.0469
151.4926 418.3555
151.9747 394.5078
152.4568 400.4805
152.9389 455.3633
153.4210 521.7578
153.9032 553.4648
154.3853 514.7734
154.8674 462.4727
155.3495 412.2422
155.8316 364.3086
156.3138 317.7617
156.7959 269.8047
157.2780 221.5781
157.7601 176.0820
158.2422 125.7656
158.7243 82.21875
159.2065 50.38281
159.6886 30.32422
160.1707 19.82812
160.6528 15.66016
161.1349 18.83984
161.6170 33.46875
162.0992 62.66406
162.5813 101.5859
163.0634 147.7031
163.5455 206.5898
164.0276 263.4336
164.5097 309.5469
164.9919 347.3242
165.4740 386.1719
165.9561 435.9570
166.4382 486.6719
166.9203 530.2461
167.4025 561.1055
167.8846 588.2461
168.3667 615.4727
168.8488 643.4570
169.3309 676.0977
169.8130 718.2891
170.2952 765.5781
170.7773 811.5898
171.2594 858.9883
171.7415 900.4727
172.2236 926.9258
172.7057 938.8242
173.1879 949.8125
173.6700 962.6133
174.1521 981.2188
174.6342 1012.719
175.1163 1071.906
175.5984 1138.871
176.0806 1188.996
176.5627 1222.328
177.0448 1248.559
177.5269 1276.609
178.0090 1304.016
178.4911 1326.434
178.9733 1344.309
179.4554 1355.211
179.9375 1355.277
180.4196 1344.492
180.9017 1325.484
181.3839 1309.613
181.8660 1291.145
182.3481 1247.855
182.8302 1155.715
183.3123 1034.375
183.7944 926.6172
184.2766 833.7305
184.7587 753.5430
185.2408 680.8164
185.7229 617.0273
186.2050 567.0898
186.6871 538.8516
187.1693 527.2695
187.6514 512.3516
188.1335 490.4805
188.6156 472.5508
189.0977 477.1328
189.5798 502.6133
190.0620 531.4961
190.5441 554.9531
191.0262 573.1953
191.5083 594.0742
191.9904 621.7773
192.4725 643.6836
192.9547 632.4688
193.4368 587.3008
193.9189 543.4531
194.4010 520.9922
194.8831 519.1562
195.3652 521.2852
195.8474 526.2969
196.3295 535.8125
196.8116 556.9023
197.2937 591.3633
197.7758 620.4883
198.2579 629.5938
198.7401 618.0156
199.2222 609.8594
199.7043 605.8750
200.1864 605.9922
200.6685 611.2617
201.1507 621.5859
201.6328 634.4727
202.1149 652.7305
202.5970 678.2734
203.0791 684.3047
203.5612 661.7617
204.0434 623.6094
204.5255 607.0195
205.0076 617.3320
205.4897 631.9961
205.9718 637.5586
206.4539 632.9180
206.9361 628.8555
207.4182 628.2969
207.9003 628.6211
208.3824 607.0117
208.8645 573.1836
209.3466 541.5938
209.8288 520.2695
210.3109 509.2305
210.7930 508.7695
211.2751 522.7344
211.7572 546.1641
212.2393 562.2383
212.7215 569.2891
213.2036 573.1953
213.6857 577.6680
214.1678 582.5703
214.6499 588.9414
215.1321 594.1797
215.6142 599.4648
216.0963 614.0039
216.5784 640.7500
217.0605 669.6055
217.5426 694.1016
218.0248 711.6836
218.5069 736.0625
218.9890 772.9375
219.4711 817.9297
219.9532 848.1445
220.4353 854.5430
220.9175 857.4297
221.3996 871.3164
221.8817 900.5273
222.3638 934.8789
222.8459 978.1406
223.3280 1025.719
223.8102 1050.180
224.2923 1038.172
224.7744 1027.336
225.2565 1040.602
225.7386 1085.398
226.2208 1129.859
226.7029 1170.355
227.1850 1208.871
227.6671 1254.734
228.1492 1315.719
228.6313 1372.805
229.1135 1413.938
229.5956 1434.879
230.0777 1448.988
230.5598 1446.074
231.0419 1436.188
231.5240 1470.086
232.0062 1566.348
232.4883 1682.355
232.9704 1794.520
233.4525 1903.293
233.9346 2007.691
234.4167 2105.098
234.8989 2197.434
235.3810 2298.906
235.8631 2444.301
236.3452 2553.770
236.8273 2584.438
237.3095 2529.531
237.7916 2405.512
238.2737 2186.582
238.7558 1896.188
239.2379 1627.191
239.7200 1369.016
240.2022 1145.125
240.6843 968.5156
241.1664 854.6953
241.6485 755.1602
242.1306 672.2344
242.6127 602.3242
243.0949 532.6445
243.5770 459.2578
244.0591 393.6328
244.5412 343.5820
245.0233 315.9570
245.5054 291.2188
245.9876 271.7188
246.4697 255.3438
246.9518 232.9688
247.4339 198.3984
247.9160 167.1562
248.3981 145.7148
248.8803 131.9609
249.3624 132.2930
249.8445 152.3320
250.3266 183.9219
250.8087 205.2305
251.2909 209.9258
251.7730 211.7969
252.2551 216.4883
252.7372 224.9805
253.2193 232.1172
253.7014 237.7695
254.1836 241.5781
254.6657 243.2734
255.1478 244.8008
255.6299 241.0625
256.1120 228.4883
256.5941 202.6328
257.0763 184.5156
257.5584 177.8633
258.0405 177.3711
258.5226 171.3242
259.0047 156.5742
259.4868 143.8711
259.9690 139.7070
260.4511 148.7344
260.9332 143.5078
261.4153 114.4648
261.8974 79.49609
262.3795 73.07031
262.8617 108.6445
263.3438 140.5391
263.8259 149.0391
264.3080 129.0781
264.7901 120.6289
265.2722 129.3633
265.7544 143.5078
266.2365 144.4258
266.7186 127.0469
267.2007 112.8945
267.6829 112.8555
268.1650 129.3125
268.6471 116.7617
269.1292 64.30859
269.6113 0.9843750
270.0934 35.50000
270.5756 38.61328
271.0577 40.92969
271.5398 53.24219
272.0219 74.96875
272.5040 84.39453
272.9861 79.02734
273.4683 66.83594
273.9504 52.53125
274.4325 33.91016
274.9146 27.80078
275.3967 41.64844
275.8788 72.83203
276.3610 101.6953
276.8431 130.9922
277.3252 149.1055
277.8073 138.6562
278.2894 96.12109
278.7715 62.47266
279.2537 47.74219
279.7358 46.55078
280.2179 34.34766
280.7000 7.292969
281.1821 16.00781
281.6642 13.36719
282.1464 15.31641
282.6285 25.83203
283.1106 10.13672
283.5927 27.16406
284.0748 79.20312
284.5569 147.5977
285.0391 213.0625
285.5212 257.2812
286.0033 282.0664
286.4854 317.2656
286.9675 369.4297
287.4496 427.5664
287.9318 472.4141
288.4139 503.9688
288.8960 522.8398
289.3781 523.2969
289.8602 509.9961
290.3424 507.5273
290.8245 520.8906
291.3066 540.0469
291.7887 548.2109
292.2708 546.9336
292.7530 546.3320
293.2351 552.3828
293.7172 563.9102
294.1993 574.3320
294.6814 581.9648
295.1635 595.5938
295.6457 620.2266
296.1278 657.6836
296.6099 717.5742
297.0920 815.8477
297.5741 935.5625
298.0562 1044.383
298.5384 1140.531
299.0205 1228.191
299.5026 1308.027
299.9847 1381.699
300.4668 1457.461
300.9489 1571.359
301.4311 1671.551
301.9132 1673.207
302.3953 1579.168
302.8774 1449.820
303.3595 1306.535
303.8416 1165.086
304.3238 1050.980
304.8059 992.1875
305.2880 948.1953
305.7701 879.7109
306.2522 788.9531
306.7343 694.3047
307.2165 596.5898
307.6986 504.3008
308.1807 427.6641
308.6628 367.8203
309.1449 323.5742
309.6270 296.3750
310.1092 283.1992
310.5913 276.3711
311.0734 271.2422
311.5555 269.9414
312.0376 276.8984
312.5197 297.9805
313.0019 312.3828
313.4840 301.7891
313.9661 276.3398
314.4482 256.7969
314.9304 262.3516
315.4125 269.8984
315.8946 262.8672
316.3767 235.9258
316.8588 214.4844
317.3409 225.0000
317.8231 243.6016
318.3052 238.7305
318.7873 176.5898
319.2694 110.6680
319.7515 58.18750
320.2336 19.87109
320.7158 1.812500
321.1979 24.08984
321.6800 58.88672
322.1621 80.99609
322.6442 76.99609
323.1263 67.77734
323.6085 50.28516
324.0906 26.22656
324.5727 20.53516
325.0548 50.17969
325.5369 91.29688
326.0190 129.6289
326.5012 172.6641
326.9833 204.1680
327.4654 215.5039
327.9475 211.3555
328.4296 215.4531
328.9117 236.2578
329.3939 257.6641
329.8760 273.3086
330.3581 284.5820
330.8402 287.1836
331.3223 272.7070
331.8044 250.8203
332.2866 241.8477
332.7687 248.3008
333.2508 259.3906
333.7329 271.8789
334.2150 286.4844
334.6971 296.9297
335.1793 308.5352
335.6614 314.1523
336.1435 303.9922
336.6256 272.6055
337.1077 234.7188
337.5899 192.2227
338.0720 148.2852
338.5541 125.6055
339.0362 130.0469
339.5183 139.8164
340.0005 136.8828
340.4826 121.6562
340.9647 110.6914
341.4468 105.8750
341.9289 107.0078
342.4110 122.2422
342.8932 153.9688
343.3753 186.0898
343.8574 195.3242
344.3395 180.9336
344.8216 182.0469
345.3037 202.5781
345.7859 239.9336
346.2680 294.4727
346.7501 364.8984
347.2322 432.6172
347.7143 476.4414
348.1964 509.2578
348.6786 572.0039
349.1607 667.2852
349.6428 790.8086
350.1249 931.7891
350.6070 1096.496
351.0891 1308.852
351.5713 1619.945
352.0534 1961.562
352.5355 2257.746
353.0176 2503.223
353.4997 2669.777
353.9818 2680.613
354.4640 2609.957
354.9461 2572.676
355.4282 2618.266
355.9103 2688.359
356.3924 2724.457
356.8745 2738.582
357.3567 2776.828
357.8388 2866.770
358.3209 2991.246
358.8030 3134.832
359.2851 3289.176
359.7672 3476.457
360.2494 3684.504
360.7315 3936.766
361.2136 4272.160
361.6957 4679.945
362.1779 5197.016
362.6600 5868.164
363.1421 6713.043
363.6242 7574.297
364.1063 8444.695
364.5884 9294.988
365.0706 10087.92
365.5527 10649.96
366.0348 11323.50
366.5169 12258.84
366.9990 13435.59
367.4811 14496.70
367.9633 16229.97
368.4454 17275.51
368.9275 16823.24
369.4096 13703.31
369.8917 10704.70
370.3738 7628.309
370.8560 4699.883
371.3381 2616.414
371.8202 1686.125
372.3023 1157.336
372.7844 794.3633
373.2665 631.5938
373.7487 500.5664
374.2308 406.2891
374.7129 339.2109
375.1950 286.5625
375.6771 250.1758
376.1592 224.0117
376.6414 211.4844
377.1235 210.1719
377.6056 187.4219
378.0877 135.6367
378.5698 86.47266
379.0519 74.44922
379.5341 100.3516
380.0162 117.0312
380.4983 114.9297
380.9804 100.2031
381.4625 84.61328
381.9446 67.53516
382.4268 54.01172
382.9089 49.68750
383.3910 52.00391
383.8731 50.81641
384.3553 43.90625
384.8374 38.36719
385.3195 44.13281
385.8016 58.25391
386.2837 72.19922
386.7658 81.64062
387.2480 88.99609
387.7301 99.56641
388.2122 112.9531
388.6943 120.6797
389.1764 110.8555
389.6585 93.56250
390.1407 82.60156
390.6228 87.55859
391.1049 91.44141
391.5870 83.37500
392.0691 65.23828
392.5512 42.83594
393.0334 7.093750
393.5155 23.85938
393.9976 35.23828
394.4797 18.09375
394.9618 5.730469
395.4439 18.32812
395.9261 39.04297
396.4082 45.34375
396.8903 12.24219
397.3724 15.93750
397.8545 24.00781
398.3366 10.84375
398.8188 2.578125
399.3009 15.58203
399.7830 24.25000
400.2651 10.87500
400.7472 59.83203
401.2293 99.42969
401.7115 92.28516
402.1936 52.89062
402.6757 24.71094
403.1578 12.91406
403.6399 3.914063
404.1220 9.035156
404.6042 28.07812
405.0863 36.31250
405.5684 30.71875
406.0505 18.95703
406.5326 11.15625
407.0147 8.023438
407.4969 4.097656
407.9790 2.750000
408.4611 11.03125
408.9432 15.92969
409.4254 17.16406
409.9075 13.69141
410.3896 1.851563
410.8717 16.34375
411.3538 29.86719
411.8359 34.68750
412.3181 40.48438
412.8002 69.68359
413.2823 114.4258
413.7644 144.5859
414.2465 129.7695
414.7286 97.15625
415.2108 82.49609
415.6929 87.75391
416.1750 99.19922
416.6571 113.1406
417.1392 124.8750
417.6213 127.6562
418.1035 109.6484
418.5856 92.39844
419.0677 87.25391
419.5498 93.19141
420.0319 106.8828
420.5140 141.2969
420.9962 172.9961
421.4783 187.1562
421.9604 177.4648
422.4425 162.1445
422.9246 141.1406
423.4067 118.1289
423.8889 97.62891
424.3710 75.50000
424.8531 61.23047
425.3352 59.75000
425.8173 71.03516
426.2994 80.32031
426.7816 82.34375
427.2637 87.73828
427.7458 104.9883
428.2279 142.7578
428.7100 170.7422
429.1921 184.2812
429.6743 188.7852
430.1564 195.1406
430.6385 201.9883
431.1206 215.9570
431.6028 240.4609
432.0849 275.3359
432.5670 315.3320
433.0491 361.3750
433.5312 409.6992
434.0133 458.5703
434.4955 507.5742
434.9776 551.8203
435.4597 587.3750
435.9418 621.7422
436.4239 666.8594
436.9060 722.1367
437.3882 784.5586
437.8703 856.6602
438.3524 932.6914
438.8345 1000.312
439.3166 1055.141
439.7987 1119.629
440.2809 1211.383
440.7630 1324.352
441.2451 1448.336
441.7272 1588.289
442.2093 1729.137
442.6914 1858.117
443.1736 1978.266
443.6557 2109.324
444.1378 2271.625
444.6199 2439.250
445.1020 2595.406
445.5841 2734.414
446.0663 2869.555
446.5484 3008.145
447.0305 3143.777
447.5126 3267.207
447.9947 3417.441
448.4768 3507.645
448.9590 3515.262
449.4411 3439.066
449.9232 3314.160
450.4053 3123.426
450.8874 2904.254
451.3695 2672.336
451.8517 2410.070
452.3338 2211.375
452.8159 2091.297
453.2980 2030.539
453.7801 1996.633
454.2622 1991.164
454.7444 2006.555
455.2265 2042.617
455.7086 2095.195
456.1907 2151.238
456.6729 2211.801
457.1550 2272.855
457.6371 2324.020
458.1192 2372.859
458.6013 2439.930
459.0834 2543.668
459.5656 2650.121
460.0477 2706.797
460.5298 2731.867
461.0119 2777.328
461.4940 2866.355
461.9761 2990.242
462.4583 3138.754
462.9404 3310.957
463.4225 3523.992
463.9046 3757.055
464.3867 4049.668
464.8688 4433.965
465.3510 4923.211
465.8331 5501.188
466.3152 6195.008
466.7973 6981.809
467.2794 7772.434
467.7615 8640.230
468.2437 9440.938
468.7258 10122.42
469.2079 10655.98
469.6900 11159.76
470.1721 11629.65
470.6542 12074.07
471.1364 12494.18
471.6185 12879.95
472.1006 13278.21
472.5827 13672.45
473.0648 14094.59
473.5469 14636.65
474.0291 15296.00
474.5112 16113.93
474.9933 17114.67
475.4754 18294.05
475.9575 19645.96
476.4396 21175.65
476.9218 22842.86
477.4039 24587.87
477.8860 26425.21
478.3681 28371.38
478.8503 30420.33
479.3324 32593.20
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1247.827 205.5156
1248.309 214.9453
1248.792 215.6562
1249.274 209.8281
1249.756 195.8984
1250.238 191.5000
1250.720 230.8477
1251.202 249.7148
1251.684 210.9023
1252.166 142.7852
1252.649 116.2695
1253.131 122.5234
1253.613 139.2266
1254.095 165.0469
1254.577 174.4648
1255.059 146.2188
1255.541 118.3828
1256.023 101.0859
1256.505 96.14062
1256.988 119.8711
1257.470 155.7734
1257.952 167.3320
1258.434 146.0078
1258.916 118.6680
1259.398 79.25000
1259.880 61.76562
1260.362 84.26172
1260.844 122.2852
1261.327 141.6992
1261.809 146.6445
1262.291 141.0625
1262.773 124.2344
1263.255 113.1797
1263.737 111.3906
1264.219 101.6992
1264.701 72.16406
1265.184 48.50000
1265.666 69.42969
1266.148 110.0781
1266.630 140.3867
1267.112 156.8242
1267.594 188.8906
1268.076 241.1328
1268.558 270.5859
1269.041 259.7812
1269.523 241.5039
1270.005 255.4023
1270.487 270.7695
1270.969 250.8477
1271.451 204.8477
1271.933 185.7148
1272.415 194.4531
1272.897 191.4102
1273.380 164.1133
1273.862 145.0312
1274.344 179.3867
1274.826 207.5430
1275.308 183.8789
1275.790 128.1719
1276.272 101.6719
1276.754 102.1719
1277.237 123.0273
1277.719 165.1445
1278.201 203.3828
1278.683 222.2266
1279.165 235.8828
1279.647 249.2930
1280.129 262.6758
1280.611 273.5938
1281.094 286.5156
1281.576 317.4336
1282.058 370.2031
1282.540 415.2031
1283.022 429.7617
1283.504 459.7070
1283.986 518.3711
1284.468 593.9531
1284.950 667.4102
1285.432 745.6211
1285.915 845.6758
1286.397 967.8711
1286.879 1066.930
1287.361 1137.051
1287.843 1192.062
1288.325 1235.148
1288.807 1260.746
1289.289 1279.504
1289.772 1264.621
1290.254 1175.477
1290.736 1018.285
1291.218 858.8516
1291.700 694.5234
1292.182 548.2227
1292.664 422.9844
1293.146 324.4102
1293.629 270.3867
1294.111 231.4648
1294.593 193.3828
1295.075 151.8047
1295.557 87.50000
1296.039 6.039063
1296.521 25.62500
1297.003 2.628906
1297.485 46.57812
1297.968 94.76562
1298.450 119.2812
1298.932 99.73438
1299.414 63.71094
1299.896 19.35938
1300.378 58.35547
1300.860 64.80078
1301.342 25.14844
1301.824 13.61719
1302.307 0.0000000E+00
