#\#CIF_2.0 #------------------------------------------------------------------------------ #$Date: 2018-05-24 15:23:10 +0300 (Thu, 24 May 2018) $ #$Revision: 698 $ #$URL: svn://172.16.1.111/rod/cif/1/00/02/1000209.rod $ #------------------------------------------------------------------------------ # # This file is available in the Raman Open Database (ROD), # http://solsa.crystallography.net/rod/ # # All data on this site have been placed in the public domain by the # contributors. # data_1000209 loop_ _publ_author_name 'Echigo, T.' 'Kimata, M.' 'Maruoka, T.' _publ_section_title ; Crystal-chemical and carbon-isotopic characteristics of karpatite (C24H12) from the Picacho Peak Area, San Benito County, California: Evidences for the hydrothermal formation Locality: Picacho Peak Area, San Benito County, California, USA ; _journal_name_full 'American Mineralogist' _journal_page_first 1262 _journal_page_last 1269 _journal_paper_doi 10.2138/am.2007.2509 _journal_volume 92 _journal_year 2007 _chemical_compound_source R060162 _chemical_formula_sum 'C2 H' _chemical_name_mineral Carpathite/Karpalite? _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yab' _symmetry_space_group_name_H-M 'P 1 21/a 1' _cell_angle_alpha 90 _cell_angle_beta 110.79 _cell_angle_gamma 90 _cell_length_a 16.094 _cell_length_b 4.690 _cell_length_c 10.049 _cell_volume 709.119 _cod_data_source_file 04410.cif _cod_data_source_block global _cod_original_formula_sum 'C2 H1' _cod_database_code 9010291 _raman_determination_method experimental _raman_measurement_device.location 'Arizona University' _raman_measurement_device.company 'Thermo Scientific' _raman_measurement_device.model 'Nicolet Almega XR' _raman_measurement_device.optics_type microscope _raman_measurement_device.microscope_system dispersive _raman_measurement_device.microscope_objective_magnification 50 _raman_measurement_device.microscope_numerical_aperture 0.5 _raman_measurement_device.excitation_laser_type other _raman_measurement_device.excitation_laser_wavelength 532 _raman_measurement_device.configuration simple _raman_measurement_device.resolution 4 _raman_measurement_device.power_on_sample 15 _raman_measurement_device.direction_polarization unoriented _raman_measurement_device.spot_size 1 _raman_measurement_device.diffraction_grating 400 _raman_measurement.environment Air _raman_measurement.environment_details ; The sample was measured in air. ; _raman_measurement.temperature 300 _raman_measurement.pressure 100 _raman_measurement.background_subtraction no _raman_measurement.background_subtraction_details ; No background subtraction method was applied. ; _raman_measurement.baseline_correction no _raman_measurement.baseline_correction_details ; No baseline correction method was applied. ; _raman_measurement.integration_time 10 _rod_data_source.file R060162.rod _rod_data_source.block 3500000 _rod_database.code 1000209 loop_ _raman_complementary.id _raman_complementary.method 1 XRD loop_ _raman_measurement_device_calibration.id _raman_measurement_device_calibration.standard 1 neon_lamp loop_ _rod_related_entry.id _rod_related_entry.code _rod_related_entry.database _rod_related_entry.uri _rod_related_entry.description 1 9010291 COD http://www.crystallography.net/cod/9010291.html ; XRD analysis data was done. ; loop_ _raman_spectrum.raman_shift _raman_spectrum.intensity 150.5283 0.0000000E+00 151.0105 390.0469 151.4926 418.3555 151.9747 394.5078 152.4568 400.4805 152.9389 455.3633 153.4210 521.7578 153.9032 553.4648 154.3853 514.7734 154.8674 462.4727 155.3495 412.2422 155.8316 364.3086 156.3138 317.7617 156.7959 269.8047 157.2780 221.5781 157.7601 176.0820 158.2422 125.7656 158.7243 82.21875 159.2065 50.38281 159.6886 30.32422 160.1707 19.82812 160.6528 15.66016 161.1349 18.83984 161.6170 33.46875 162.0992 62.66406 162.5813 101.5859 163.0634 147.7031 163.5455 206.5898 164.0276 263.4336 164.5097 309.5469 164.9919 347.3242 165.4740 386.1719 165.9561 435.9570 166.4382 486.6719 166.9203 530.2461 167.4025 561.1055 167.8846 588.2461 168.3667 615.4727 168.8488 643.4570 169.3309 676.0977 169.8130 718.2891 170.2952 765.5781 170.7773 811.5898 171.2594 858.9883 171.7415 900.4727 172.2236 926.9258 172.7057 938.8242 173.1879 949.8125 173.6700 962.6133 174.1521 981.2188 174.6342 1012.719 175.1163 1071.906 175.5984 1138.871 176.0806 1188.996 176.5627 1222.328 177.0448 1248.559 177.5269 1276.609 178.0090 1304.016 178.4911 1326.434 178.9733 1344.309 179.4554 1355.211 179.9375 1355.277 180.4196 1344.492 180.9017 1325.484 181.3839 1309.613 181.8660 1291.145 182.3481 1247.855 182.8302 1155.715 183.3123 1034.375 183.7944 926.6172 184.2766 833.7305 184.7587 753.5430 185.2408 680.8164 185.7229 617.0273 186.2050 567.0898 186.6871 538.8516 187.1693 527.2695 187.6514 512.3516 188.1335 490.4805 188.6156 472.5508 189.0977 477.1328 189.5798 502.6133 190.0620 531.4961 190.5441 554.9531 191.0262 573.1953 191.5083 594.0742 191.9904 621.7773 192.4725 643.6836 192.9547 632.4688 193.4368 587.3008 193.9189 543.4531 194.4010 520.9922 194.8831 519.1562 195.3652 521.2852 195.8474 526.2969 196.3295 535.8125 196.8116 556.9023 197.2937 591.3633 197.7758 620.4883 198.2579 629.5938 198.7401 618.0156 199.2222 609.8594 199.7043 605.8750 200.1864 605.9922 200.6685 611.2617 201.1507 621.5859 201.6328 634.4727 202.1149 652.7305 202.5970 678.2734 203.0791 684.3047 203.5612 661.7617 204.0434 623.6094 204.5255 607.0195 205.0076 617.3320 205.4897 631.9961 205.9718 637.5586 206.4539 632.9180 206.9361 628.8555 207.4182 628.2969 207.9003 628.6211 208.3824 607.0117 208.8645 573.1836 209.3466 541.5938 209.8288 520.2695 210.3109 509.2305 210.7930 508.7695 211.2751 522.7344 211.7572 546.1641 212.2393 562.2383 212.7215 569.2891 213.2036 573.1953 213.6857 577.6680 214.1678 582.5703 214.6499 588.9414 215.1321 594.1797 215.6142 599.4648 216.0963 614.0039 216.5784 640.7500 217.0605 669.6055 217.5426 694.1016 218.0248 711.6836 218.5069 736.0625 218.9890 772.9375 219.4711 817.9297 219.9532 848.1445 220.4353 854.5430 220.9175 857.4297 221.3996 871.3164 221.8817 900.5273 222.3638 934.8789 222.8459 978.1406 223.3280 1025.719 223.8102 1050.180 224.2923 1038.172 224.7744 1027.336 225.2565 1040.602 225.7386 1085.398 226.2208 1129.859 226.7029 1170.355 227.1850 1208.871 227.6671 1254.734 228.1492 1315.719 228.6313 1372.805 229.1135 1413.938 229.5956 1434.879 230.0777 1448.988 230.5598 1446.074 231.0419 1436.188 231.5240 1470.086 232.0062 1566.348 232.4883 1682.355 232.9704 1794.520 233.4525 1903.293 233.9346 2007.691 234.4167 2105.098 234.8989 2197.434 235.3810 2298.906 235.8631 2444.301 236.3452 2553.770 236.8273 2584.438 237.3095 2529.531 237.7916 2405.512 238.2737 2186.582 238.7558 1896.188 239.2379 1627.191 239.7200 1369.016 240.2022 1145.125 240.6843 968.5156 241.1664 854.6953 241.6485 755.1602 242.1306 672.2344 242.6127 602.3242 243.0949 532.6445 243.5770 459.2578 244.0591 393.6328 244.5412 343.5820 245.0233 315.9570 245.5054 291.2188 245.9876 271.7188 246.4697 255.3438 246.9518 232.9688 247.4339 198.3984 247.9160 167.1562 248.3981 145.7148 248.8803 131.9609 249.3624 132.2930 249.8445 152.3320 250.3266 183.9219 250.8087 205.2305 251.2909 209.9258 251.7730 211.7969 252.2551 216.4883 252.7372 224.9805 253.2193 232.1172 253.7014 237.7695 254.1836 241.5781 254.6657 243.2734 255.1478 244.8008 255.6299 241.0625 256.1120 228.4883 256.5941 202.6328 257.0763 184.5156 257.5584 177.8633 258.0405 177.3711 258.5226 171.3242 259.0047 156.5742 259.4868 143.8711 259.9690 139.7070 260.4511 148.7344 260.9332 143.5078 261.4153 114.4648 261.8974 79.49609 262.3795 73.07031 262.8617 108.6445 263.3438 140.5391 263.8259 149.0391 264.3080 129.0781 264.7901 120.6289 265.2722 129.3633 265.7544 143.5078 266.2365 144.4258 266.7186 127.0469 267.2007 112.8945 267.6829 112.8555 268.1650 129.3125 268.6471 116.7617 269.1292 64.30859 269.6113 0.9843750 270.0934 35.50000 270.5756 38.61328 271.0577 40.92969 271.5398 53.24219 272.0219 74.96875 272.5040 84.39453 272.9861 79.02734 273.4683 66.83594 273.9504 52.53125 274.4325 33.91016 274.9146 27.80078 275.3967 41.64844 275.8788 72.83203 276.3610 101.6953 276.8431 130.9922 277.3252 149.1055 277.8073 138.6562 278.2894 96.12109 278.7715 62.47266 279.2537 47.74219 279.7358 46.55078 280.2179 34.34766 280.7000 7.292969 281.1821 16.00781 281.6642 13.36719 282.1464 15.31641 282.6285 25.83203 283.1106 10.13672 283.5927 27.16406 284.0748 79.20312 284.5569 147.5977 285.0391 213.0625 285.5212 257.2812 286.0033 282.0664 286.4854 317.2656 286.9675 369.4297 287.4496 427.5664 287.9318 472.4141 288.4139 503.9688 288.8960 522.8398 289.3781 523.2969 289.8602 509.9961 290.3424 507.5273 290.8245 520.8906 291.3066 540.0469 291.7887 548.2109 292.2708 546.9336 292.7530 546.3320 293.2351 552.3828 293.7172 563.9102 294.1993 574.3320 294.6814 581.9648 295.1635 595.5938 295.6457 620.2266 296.1278 657.6836 296.6099 717.5742 297.0920 815.8477 297.5741 935.5625 298.0562 1044.383 298.5384 1140.531 299.0205 1228.191 299.5026 1308.027 299.9847 1381.699 300.4668 1457.461 300.9489 1571.359 301.4311 1671.551 301.9132 1673.207 302.3953 1579.168 302.8774 1449.820 303.3595 1306.535 303.8416 1165.086 304.3238 1050.980 304.8059 992.1875 305.2880 948.1953 305.7701 879.7109 306.2522 788.9531 306.7343 694.3047 307.2165 596.5898 307.6986 504.3008 308.1807 427.6641 308.6628 367.8203 309.1449 323.5742 309.6270 296.3750 310.1092 283.1992 310.5913 276.3711 311.0734 271.2422 311.5555 269.9414 312.0376 276.8984 312.5197 297.9805 313.0019 312.3828 313.4840 301.7891 313.9661 276.3398 314.4482 256.7969 314.9304 262.3516 315.4125 269.8984 315.8946 262.8672 316.3767 235.9258 316.8588 214.4844 317.3409 225.0000 317.8231 243.6016 318.3052 238.7305 318.7873 176.5898 319.2694 110.6680 319.7515 58.18750 320.2336 19.87109 320.7158 1.812500 321.1979 24.08984 321.6800 58.88672 322.1621 80.99609 322.6442 76.99609 323.1263 67.77734 323.6085 50.28516 324.0906 26.22656 324.5727 20.53516 325.0548 50.17969 325.5369 91.29688 326.0190 129.6289 326.5012 172.6641 326.9833 204.1680 327.4654 215.5039 327.9475 211.3555 328.4296 215.4531 328.9117 236.2578 329.3939 257.6641 329.8760 273.3086 330.3581 284.5820 330.8402 287.1836 331.3223 272.7070 331.8044 250.8203 332.2866 241.8477 332.7687 248.3008 333.2508 259.3906 333.7329 271.8789 334.2150 286.4844 334.6971 296.9297 335.1793 308.5352 335.6614 314.1523 336.1435 303.9922 336.6256 272.6055 337.1077 234.7188 337.5899 192.2227 338.0720 148.2852 338.5541 125.6055 339.0362 130.0469 339.5183 139.8164 340.0005 136.8828 340.4826 121.6562 340.9647 110.6914 341.4468 105.8750 341.9289 107.0078 342.4110 122.2422 342.8932 153.9688 343.3753 186.0898 343.8574 195.3242 344.3395 180.9336 344.8216 182.0469 345.3037 202.5781 345.7859 239.9336 346.2680 294.4727 346.7501 364.8984 347.2322 432.6172 347.7143 476.4414 348.1964 509.2578 348.6786 572.0039 349.1607 667.2852 349.6428 790.8086 350.1249 931.7891 350.6070 1096.496 351.0891 1308.852 351.5713 1619.945 352.0534 1961.562 352.5355 2257.746 353.0176 2503.223 353.4997 2669.777 353.9818 2680.613 354.4640 2609.957 354.9461 2572.676 355.4282 2618.266 355.9103 2688.359 356.3924 2724.457 356.8745 2738.582 357.3567 2776.828 357.8388 2866.770 358.3209 2991.246 358.8030 3134.832 359.2851 3289.176 359.7672 3476.457 360.2494 3684.504 360.7315 3936.766 361.2136 4272.160 361.6957 4679.945 362.1779 5197.016 362.6600 5868.164 363.1421 6713.043 363.6242 7574.297 364.1063 8444.695 364.5884 9294.988 365.0706 10087.92 365.5527 10649.96 366.0348 11323.50 366.5169 12258.84 366.9990 13435.59 367.4811 14496.70 367.9633 16229.97 368.4454 17275.51 368.9275 16823.24 369.4096 13703.31 369.8917 10704.70 370.3738 7628.309 370.8560 4699.883 371.3381 2616.414 371.8202 1686.125 372.3023 1157.336 372.7844 794.3633 373.2665 631.5938 373.7487 500.5664 374.2308 406.2891 374.7129 339.2109 375.1950 286.5625 375.6771 250.1758 376.1592 224.0117 376.6414 211.4844 377.1235 210.1719 377.6056 187.4219 378.0877 135.6367 378.5698 86.47266 379.0519 74.44922 379.5341 100.3516 380.0162 117.0312 380.4983 114.9297 380.9804 100.2031 381.4625 84.61328 381.9446 67.53516 382.4268 54.01172 382.9089 49.68750 383.3910 52.00391 383.8731 50.81641 384.3553 43.90625 384.8374 38.36719 385.3195 44.13281 385.8016 58.25391 386.2837 72.19922 386.7658 81.64062 387.2480 88.99609 387.7301 99.56641 388.2122 112.9531 388.6943 120.6797 389.1764 110.8555 389.6585 93.56250 390.1407 82.60156 390.6228 87.55859 391.1049 91.44141 391.5870 83.37500 392.0691 65.23828 392.5512 42.83594 393.0334 7.093750 393.5155 23.85938 393.9976 35.23828 394.4797 18.09375 394.9618 5.730469 395.4439 18.32812 395.9261 39.04297 396.4082 45.34375 396.8903 12.24219 397.3724 15.93750 397.8545 24.00781 398.3366 10.84375 398.8188 2.578125 399.3009 15.58203 399.7830 24.25000 400.2651 10.87500 400.7472 59.83203 401.2293 99.42969 401.7115 92.28516 402.1936 52.89062 402.6757 24.71094 403.1578 12.91406 403.6399 3.914063 404.1220 9.035156 404.6042 28.07812 405.0863 36.31250 405.5684 30.71875 406.0505 18.95703 406.5326 11.15625 407.0147 8.023438 407.4969 4.097656 407.9790 2.750000 408.4611 11.03125 408.9432 15.92969 409.4254 17.16406 409.9075 13.69141 410.3896 1.851563 410.8717 16.34375 411.3538 29.86719 411.8359 34.68750 412.3181 40.48438 412.8002 69.68359 413.2823 114.4258 413.7644 144.5859 414.2465 129.7695 414.7286 97.15625 415.2108 82.49609 415.6929 87.75391 416.1750 99.19922 416.6571 113.1406 417.1392 124.8750 417.6213 127.6562 418.1035 109.6484 418.5856 92.39844 419.0677 87.25391 419.5498 93.19141 420.0319 106.8828 420.5140 141.2969 420.9962 172.9961 421.4783 187.1562 421.9604 177.4648 422.4425 162.1445 422.9246 141.1406 423.4067 118.1289 423.8889 97.62891 424.3710 75.50000 424.8531 61.23047 425.3352 59.75000 425.8173 71.03516 426.2994 80.32031 426.7816 82.34375 427.2637 87.73828 427.7458 104.9883 428.2279 142.7578 428.7100 170.7422 429.1921 184.2812 429.6743 188.7852 430.1564 195.1406 430.6385 201.9883 431.1206 215.9570 431.6028 240.4609 432.0849 275.3359 432.5670 315.3320 433.0491 361.3750 433.5312 409.6992 434.0133 458.5703 434.4955 507.5742 434.9776 551.8203 435.4597 587.3750 435.9418 621.7422 436.4239 666.8594 436.9060 722.1367 437.3882 784.5586 437.8703 856.6602 438.3524 932.6914 438.8345 1000.312 439.3166 1055.141 439.7987 1119.629 440.2809 1211.383 440.7630 1324.352 441.2451 1448.336 441.7272 1588.289 442.2093 1729.137 442.6914 1858.117 443.1736 1978.266 443.6557 2109.324 444.1378 2271.625 444.6199 2439.250 445.1020 2595.406 445.5841 2734.414 446.0663 2869.555 446.5484 3008.145 447.0305 3143.777 447.5126 3267.207 447.9947 3417.441 448.4768 3507.645 448.9590 3515.262 449.4411 3439.066 449.9232 3314.160 450.4053 3123.426 450.8874 2904.254 451.3695 2672.336 451.8517 2410.070 452.3338 2211.375 452.8159 2091.297 453.2980 2030.539 453.7801 1996.633 454.2622 1991.164 454.7444 2006.555 455.2265 2042.617 455.7086 2095.195 456.1907 2151.238 456.6729 2211.801 457.1550 2272.855 457.6371 2324.020 458.1192 2372.859 458.6013 2439.930 459.0834 2543.668 459.5656 2650.121 460.0477 2706.797 460.5298 2731.867 461.0119 2777.328 461.4940 2866.355 461.9761 2990.242 462.4583 3138.754 462.9404 3310.957 463.4225 3523.992 463.9046 3757.055 464.3867 4049.668 464.8688 4433.965 465.3510 4923.211 465.8331 5501.188 466.3152 6195.008 466.7973 6981.809 467.2794 7772.434 467.7615 8640.230 468.2437 9440.938 468.7258 10122.42 469.2079 10655.98 469.6900 11159.76 470.1721 11629.65 470.6542 12074.07 471.1364 12494.18 471.6185 12879.95 472.1006 13278.21 472.5827 13672.45 473.0648 14094.59 473.5469 14636.65 474.0291 15296.00 474.5112 16113.93 474.9933 17114.67 475.4754 18294.05 475.9575 19645.96 476.4396 21175.65 476.9218 22842.86 477.4039 24587.87 477.8860 26425.21 478.3681 28371.38 478.8503 30420.33 479.3324 32593.20 479.8145 35005.11 480.2966 37604.05 480.7787 40088.56 481.2608 42822.80 481.7430 45080.20 482.2251 46544.02 482.7072 47301.38 483.1893 46513.08 483.6714 43043.90 484.1535 38249.07 484.6357 33508.48 485.1178 28835.80 485.5999 24430.33 486.0820 20258.24 486.5641 16380.59 487.0462 12917.76 487.5284 9776.059 488.0105 7175.000 488.4926 5217.863 488.9747 3984.320 489.4568 3001.660 489.9389 2309.125 490.4211 1811.793 490.9032 1440.164 491.3853 1196.125 491.8674 1007.000 492.3495 865.3867 492.8316 763.7227 493.3138 695.0625 493.7959 656.5312 494.2780 624.3672 494.7601 581.9922 495.2422 536.9688 495.7243 505.1133 496.2065 486.5078 496.6886 477.2070 497.1707 482.0703 497.6528 490.7539 498.1349 488.0273 498.6170 459.6250 499.0992 433.1133 499.5813 426.4102 500.0634 432.7031 500.5455 435.1875 501.0276 421.5391 501.5097 409.3086 501.9919 408.4922 502.4740 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