#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-05-24 15:23:26 +0300 (Thu, 24 May 2018) $
#$Revision: 702 $
#$URL: svn://172.16.1.111/rod/cif/1/00/02/1000212.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000212
loop_
_publ_author_name
'Peacor, D. R.'
'Buerger, M. J.'
_publ_section_title
;
 The determination and refinement of the structure of narsarsukite,
 Na2TiOSi4O10
;
_journal_name_full               'American Mineralogist'
_journal_page_first              539
_journal_page_last               556
_journal_volume                  47
_journal_year                    1962
_chemical_compound_source        R060203
_chemical_formula_sum            'Na4 O22 Si8 Ti2'
_chemical_name_mineral           Narsarsukite
_space_group_IT_number           87
_symmetry_space_group_name_Hall  '-I 4'
_symmetry_space_group_name_H-M   'I 4/m'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_length_a                   10.7269
_cell_length_b                   10.7269
_cell_length_c                   7.9476
_cell_volume                     914.502
_exptl_crystal_density_diffrn    2.776
_cod_original_formula_sum        'Ti Na2 Si4 O11'
_cod_database_code               9000110
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 15
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R060203.rod
_rod_data_source.block           3500000
_rod_database.code               1000212
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9000110 COD http://www.crystallography.net/cod/9000110.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
135.4686 0.0000000E+00
135.9507 7.271240
136.4328 30.87207
136.9150 119.1470
137.3971 226.8318
137.8792 352.1147
138.3613 466.3374
138.8434 549.1157
139.3255 597.3103
139.8077 609.7581
140.2898 577.2610
140.7719 504.1125
141.2540 432.7642
141.7361 357.8020
142.2182 292.8521
142.7004 249.7612
143.1825 226.8699
143.6646 229.5686
144.1467 260.1482
144.6288 319.5544
145.1109 395.0640
145.5931 488.2566
146.0752 596.6445
146.5573 720.0630
147.0394 863.3862
147.5215 1013.451
148.0036 1161.847
148.4858 1305.346
148.9679 1467.603
149.4500 1646.925
149.9321 1845.798
150.4142 2063.878
150.8963 2299.440
151.3785 2559.767
151.8606 2841.059
152.3427 3139.136
152.8248 3477.303
153.3069 3854.624
153.7890 4273.875
154.2712 4713.106
154.7533 5152.364
155.2354 5607.390
155.7175 6080.127
156.1996 6577.295
156.6817 7063.017
157.1639 7551.168
157.6460 8027.520
158.1281 8449.267
158.6102 8807.457
159.0923 9111.808
159.5744 9366.563
160.0566 9555.529
160.5387 9720.088
161.0208 9888.248
161.5029 10043.88
161.9850 10137.95
162.4671 10197.84
162.9493 10167.60
163.4314 10010.70
163.9135 9716.396
164.3956 9301.865
164.8777 8742.522
165.3598 8057.971
165.8420 7327.024
166.3241 6525.855
166.8062 5722.206
167.2883 4974.801
167.7704 4283.852
168.2525 3667.923
168.7346 3135.213
169.2168 2682.602
169.6989 2292.643
170.1810 1968.676
170.6631 1696.457
171.1452 1458.407
171.6273 1255.467
172.1095 1081.238
172.5916 934.8320
173.0737 814.9277
173.5558 713.0835
174.0379 625.1543
174.5201 552.7778
175.0022 495.7034
175.4843 454.9990
175.9664 423.5273
176.4485 400.1213
176.9306 384.9305
177.4128 379.6985
177.8949 387.8911
178.3770 405.9895
178.8591 425.4352
179.3412 441.2440
179.8233 457.6034
180.3055 479.2317
180.7876 505.2490
181.2697 533.8607
181.7518 563.9709
182.2339 595.7837
182.7160 631.9606
183.1982 675.7745
183.6803 725.0591
184.1624 773.9445
184.6445 822.3594
185.1266 872.3506
185.6087 926.6510
186.0909 985.0918
186.5730 1043.464
187.0551 1100.689
187.5372 1156.329
188.0193 1212.241
188.5014 1269.008
188.9836 1322.656
189.4657 1373.441
189.9478 1420.179
190.4299 1453.675
190.9120 1470.810
191.3941 1471.409
191.8763 1453.302
192.3584 1415.661
192.8405 1361.777
193.3226 1292.965
193.8047 1210.470
194.2868 1118.921
194.7690 1013.511
195.2511 896.1604
195.7332 787.6904
196.2153 688.8668
196.6974 597.9678
197.1795 515.8701
197.6617 442.1425
198.1438 376.0239
198.6259 317.5927
199.1080 267.0356
199.5901 221.9507
200.0722 182.6013
200.5544 148.5791
201.0365 120.2489
201.5186 97.64062
202.0007 78.85718
202.4828 63.60522
202.9649 52.04187
203.4471 41.48254
203.9292 31.61755
204.4113 22.69885
204.8934 14.98621
205.3755 8.594849
205.8576 3.433960
206.3398 0.4957280
206.8219 3.193481
207.3040 4.413452
207.7861 3.114258
208.2682 1.233765
208.7503 3.305786
209.2325 10.41638
209.7146 17.66016
210.1967 22.63354
210.6788 24.80908
211.1609 27.15002
211.6430 29.48669
212.1252 32.19299
212.6073 36.12012
213.0894 41.60645
213.5715 47.29163
214.0536 53.15051
214.5357 60.28210
215.0179 63.11243
215.5000 59.61731
215.9821 53.20239
216.4642 51.83252
216.9463 57.21667
217.4284 63.88904
217.9105 70.12366
218.3927 76.45789
218.8748 80.10083
219.3569 80.46973
219.8390 78.47131
220.3211 76.27942
220.8032 74.30737
221.2854 71.37952
221.7675 66.76489
222.2496 59.51807
222.7317 53.59351
223.2138 49.68799
223.6959 46.76428
224.1781 42.68970
224.6602 37.51526
225.1423 31.07935
225.6244 23.14099
226.1065 13.01294
226.5886 3.431641
227.0708 5.027832
227.5529 13.25964
228.0350 23.38074
228.5171 36.90918
228.9992 49.88928
229.4813 60.82300
229.9635 69.26514
230.4456 76.87683
230.9277 82.91919
231.4098 88.46143
231.8919 95.82678
232.3740 106.5200
232.8562 116.5294
233.3383 123.8706
233.8204 126.6982
234.3025 133.0828
234.7846 144.4954
235.2667 158.6556
235.7489 171.3407
236.2310 182.1689
236.7131 192.1235
237.1952 201.1512
237.6773 208.1340
238.1594 218.0267
238.6416 231.5718
239.1237 247.6125
239.6058 264.1626
240.0879 280.7547
240.5700 298.9612
241.0521 319.5991
241.5343 342.9845
242.0164 366.3865
242.4985 388.4769
242.9806 411.4813
243.4627 438.8258
243.9448 472.0891
244.4270 506.8770
244.9091 541.0912
245.3912 573.5042
245.8733 612.8746
246.3554 661.5955
246.8375 715.5644
247.3197 769.0967
247.8018 819.5517
248.2839 874.2399
248.7660 935.1161
249.2481 1002.794
249.7302 1073.734
250.2124 1147.998
250.6945 1226.011
251.1766 1309.187
251.6587 1397.219
252.1408 1491.147
252.6229 1592.066
253.1051 1701.280
253.5872 1810.742
254.0693 1920.109
254.5514 2032.062
255.0335 2149.697
255.5156 2271.916
255.9978 2399.348
256.4799 2531.322
256.9620 2668.452
257.4441 2814.384
257.9262 2969.368
258.4083 3132.461
258.8904 3300.179
259.3726 3472.635
259.8547 3652.405
260.3368 3838.259
260.8189 4031.720
261.3010 4232.183
261.7831 4441.984
262.2653 4654.535
262.7474 4861.621
263.2295 5064.195
263.7116 5264.666
264.1937 5469.508
264.6758 5673.317
265.1580 5858.139
265.6401 6025.727
266.1222 6169.116
266.6043 6284.585
267.0864 6375.262
267.5685 6429.687
268.0507 6447.968
268.5328 6429.755
269.0149 6373.674
269.4970 6277.630
269.9791 6147.248
270.4612 5980.658
270.9434 5775.133
271.4255 5548.682
271.9076 5296.806
272.3897 5025.970
272.8718 4748.164
273.3539 4460.858
273.8361 4177.067
274.3182 3901.103
274.8003 3632.756
275.2824 3376.006
275.7645 3132.046
276.2466 2900.867
276.7288 2682.563
277.2109 2478.067
277.6930 2285.608
278.1751 2108.478
278.6572 1946.114
279.1393 1794.807
279.6215 1655.301
280.1036 1526.073
280.5857 1404.442
281.0678 1290.533
281.5499 1184.437
282.0320 1088.592
282.5142 1002.371
282.9963 923.0022
283.4784 851.1276
283.9605 785.2063
284.4426 722.0776
284.9247 661.5558
285.4069 608.8634
285.8890 566.8890
286.3711 534.5419
286.8532 504.5387
287.3353 476.5994
287.8174 451.5350
288.2996 430.2869
288.7817 412.7296
289.2638 398.8083
289.7459 388.0160
290.2280 381.2271
290.7101 380.9175
291.1923 387.2108
291.6744 397.7289
292.1565 412.0046
292.6386 429.5134
293.1207 446.9266
293.6028 462.6189
294.0850 478.8929
294.5671 500.6150
295.0492 527.6948
295.5313 559.2217
296.0134 595.1720
296.4955 634.9268
296.9777 675.9705
297.4598 716.6636
297.9419 760.1470
298.4240 810.0004
298.9061 865.7172
299.3882 926.2030
299.8704 993.8398
300.3525 1064.865
300.8346 1132.721
301.3167 1195.199
301.7988 1259.148
302.2809 1332.888
302.7631 1414.447
303.2452 1500.540
303.7273 1589.455
304.2094 1681.383
304.6915 1775.270
305.1736 1872.094
305.6558 1969.524
306.1379 2069.136
306.6200 2167.960
307.1021 2260.001
307.5842 2347.570
308.0663 2424.910
308.5485 2490.755
309.0306 2544.303
309.5127 2578.166
309.9948 2588.022
310.4769 2574.885
310.9590 2540.056
311.4412 2480.477
311.9233 2402.257
312.4054 2306.867
312.8875 2194.814
313.3696 2072.450
313.8517 1937.978
314.3339 1799.181
314.8160 1661.107
315.2981 1523.521
315.7802 1391.305
316.2623 1265.298
316.7444 1146.864
317.2266 1037.350
317.7087 939.7146
318.1908 850.9761
318.6729 768.6455
319.1550 692.7743
319.6371 622.1964
320.1193 556.0029
320.6014 495.1041
321.0835 440.1284
321.5656 393.2582
322.0477 351.2462
322.5298 312.5973
323.0120 277.2114
323.4941 244.9520
323.9762 216.4437
324.4583 190.7767
324.9404 166.9757
325.4225 144.2013
325.9047 123.8558
326.3868 107.7827
326.8689 96.03723
327.3510 82.79297
327.8331 64.56519
328.3152 46.60022
328.7974 32.53760
329.2795 25.60852
329.7616 18.82349
330.2437 11.15759
330.7258 3.055786
331.2079 3.066406
331.6901 6.651855
332.1722 8.850220
332.6543 10.10815
333.1364 9.789429
333.6185 9.791626
334.1006 10.27148
334.5828 11.08801
335.0649 11.97205
335.5470 12.87256
336.0291 13.95276
336.5112 15.58228
336.9933 18.18945
337.4755 18.99036
337.9576 17.53601
338.4397 14.80908
338.9218 11.99060
339.4039 8.198730
339.8860 3.005981
340.3681 3.133545
340.8503 10.52539
341.3324 21.93188
341.8145 37.84521
342.2966 55.82202
342.7787 73.91321
343.2608 91.78210
343.7430 111.0668
344.2251 132.1259
344.7072 154.3629
345.1893 175.2463
345.6714 194.5746
346.1535 214.5084
346.6357 236.1606
347.1178 259.0328
347.5999 282.6516
348.0820 307.6123
348.5641 331.8237
349.0462 353.6770
349.5284 373.4149
350.0105 393.2262
350.4926 412.5647
350.9747 433.0133
351.4568 458.5874
351.9389 489.5474
352.4211 523.3942
352.9032 557.1475
353.3853 591.4485
353.8674 627.8242
354.3495 666.1323
354.8316 707.3062
355.3138 752.4365
355.7959 801.4922
356.2780 853.7990
356.7601 911.4912
357.2422 971.8717
357.7243 1032.169
358.2065 1091.373
358.6886 1149.564
359.1707 1208.843
359.6528 1267.451
360.1349 1320.058
360.6170 1366.964
361.0992 1405.020
361.5813 1432.015
362.0634 1446.931
362.5455 1451.921
363.0276 1444.224
363.5097 1427.780
363.9919 1408.477
364.4740 1385.795
364.9561 1362.558
365.4382 1337.458
365.9203 1309.650
366.4024 1290.384
366.8846 1282.213
367.3667 1283.051
367.8488 1291.205
368.3309 1309.465
368.8130 1331.736
369.2951 1355.974
369.7773 1383.197
370.2594 1418.651
370.7415 1467.556
371.2236 1520.173
371.7057 1572.472
372.1878 1622.493
372.6700 1676.516
373.1521 1736.258
373.6342 1798.832
374.1163 1858.738
374.5984 1916.093
375.0805 1969.557
375.5627 2019.568
376.0448 2066.562
376.5269 2107.022
377.0090 2142.540
377.4911 2169.346
377.9732 2183.452
378.4554 2184.072
378.9375 2176.361
379.4196 2162.276
379.9017 2140.363
380.3838 2103.598
380.8659 2051.641
381.3481 1990.136
381.8302 1922.355
382.3123 1848.612
382.7944 1770.738
383.2765 1687.527
383.7586 1602.257
384.2408 1517.717
384.7229 1434.534
385.2050 1351.520
385.6871 1267.874
386.1692 1185.383
386.6513 1103.991
387.1335 1024.319
387.6156 947.1213
388.0977 873.8618
388.5798 804.4316
389.0619 737.7213
389.5440 674.6099
390.0262 613.9850
390.5083 554.2771
390.9904 495.2640
391.4725 438.1023
391.9546 382.4358
392.4367 329.4745
392.9189 279.4619
393.4010 232.3191
393.8831 189.3033
394.3652 153.6917
394.8473 122.5719
395.3294 91.08228
395.8116 54.97778
396.2937 21.11475
396.7758 7.264526
397.2579 29.56006
397.7400 50.35583
398.2221 71.40674
398.7043 90.79858
399.1864 106.9202
399.6685 119.2213
400.1506 128.7428
400.6327 135.5385
401.1148 139.6697
401.5970 141.3783
402.0791 141.1345
402.5612 137.9718
403.0433 131.8534
403.5254 124.0598
404.0075 109.6040
404.4897 87.81396
404.9718 59.88025
405.4539 27.68994
405.9360 8.609619
406.4181 50.18970
406.9002 97.86523
407.3824 151.1804
407.8645 210.4137
408.3466 276.0776
408.8287 345.7067
409.3108 417.2118
409.7929 490.3948
410.2751 567.4919
410.7572 649.5737
411.2393 735.6914
411.7214 821.2831
412.2035 907.2422
412.6856 999.1182
413.1678 1099.703
413.6499 1208.604
414.1320 1325.198
414.6141 1450.434
415.0962 1583.750
415.5783 1722.302
416.0605 1869.690
416.5426 2035.472
417.0247 2226.002
417.5068 2434.361
417.9889 2654.875
418.4710 2887.339
418.9532 3137.283
419.4353 3409.653
419.9174 3697.441
420.3995 3993.132
420.8816 4302.977
421.3637 4609.108
421.8459 4916.941
422.3280 5213.125
422.8101 5481.688
423.2922 5747.005
423.7743 5953.511
424.2564 6086.160
424.7386 6144.398
425.2207 6122.513
425.7028 6000.842
426.1849 5809.978
426.6670 5567.698
427.1491 5243.679
427.6313 4916.365
428.1134 4581.929
428.5955 4249.949
429.0776 3946.712
429.5597 3669.168
430.0418 3419.406
430.5240 3196.176
431.0061 3000.389
431.4882 2828.406
431.9703 2682.901
432.4524 2557.687
432.9345 2445.671
433.4167 2347.029
433.8988 2265.574
434.3809 2204.578
434.8630 2161.171
435.3451 2130.205
435.8272 2111.627
436.3094 2104.293
436.7915 2109.022
437.2736 2124.383
437.7557 2147.087
438.2378 2177.117
438.7199 2213.269
439.2020 2257.424
439.6841 2306.698
440.1663 2355.165
440.6484 2397.054
441.1305 2439.761
441.6126 2491.146
442.0947 2549.774
442.5768 2605.597
443.0590 2651.957
443.5411 2694.180
444.0232 2736.858
444.5053 2783.085
444.9874 2824.900
445.4695 2859.846
445.9517 2888.291
446.4338 2911.188
446.9159 2934.459
447.3980 2946.506
447.8801 2944.431
448.3622 2928.054
448.8444 2898.321
449.3265 2854.795
449.8086 2798.080
450.2907 2729.129
450.7728 2649.380
451.2549 2552.615
451.7371 2436.515
452.2192 2305.593
452.7013 2169.365
453.1834 2028.835
453.6655 1883.394
454.1476 1731.724
454.6298 1574.372
455.1119 1419.886
455.5940 1269.171
456.0761 1123.376
456.5582 985.8181
457.0403 855.9498
457.5225 732.2831
458.0046 616.2749
458.4867 508.1552
458.9688 410.7499
459.4509 323.4224
459.9330 247.0210
460.4152 180.0187
460.8973 124.3661
461.3794 82.84595
461.8615 55.39600
462.3436 41.22705
462.8257 39.17920
463.3079 50.37256
463.7900 75.56836
464.2721 113.1876
464.7542 164.0704
465.2363 232.4355
465.7184 314.7937
466.2006 401.2377
466.6827 498.3179
467.1648 591.2046
467.6469 673.5970
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