#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-05-24 15:23:44 +0300 (Thu, 24 May 2018) $
#$Revision: 707 $
#$URL: svn://172.16.1.111/rod/cif/1/00/02/1000216.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000216
loop_
_publ_author_name
'Burns, P. C.'
'Hawthorne, F. C.'
_publ_section_title
;
 Edge-sharing MnO4 tetrahedra in the structure of akatoreite,
 Mn9Al2Si8O24(OH)8
;
_journal_name_full               'The Canadian Mineralogist'
_journal_page_first              321
_journal_page_last               329
_journal_volume                  31
_journal_year                    1993
_chemical_compound_source        R060230
_chemical_formula_sum            'Al2 H8 Mn9 O32 Si8'
_chemical_name_mineral           Akatoreite
_space_group_IT_number           2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                104.46
_cell_angle_beta                 93.81
_cell_angle_gamma                104.18
_cell_length_a                   8.337
_cell_length_b                   10.367
_cell_length_c                   7.629
_cell_volume                     613.285
_exptl_crystal_density_diffrn    3.501
_cod_original_formula_sum        'Mn9 Al2 Si8 O32 H8'
_cod_database_code               9004265
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 15
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R060230.rod
_rod_data_source.block           3500000
_rod_database.code               1000216
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9004265 COD http://www.crystallography.net/cod/9004265.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
164.3956 0.0000000E+00
164.8777 0.6132690
165.3598 0.8523490
165.8420 0.2531290
166.3241 9.0500002E-04
166.8062 1.249466
167.2883 3.598421
167.7704 7.304824
168.2525 11.68827
168.7346 16.72041
169.2168 22.23842
169.6989 27.40460
170.1810 32.40765
170.6631 36.55118
171.1452 39.02239
171.6273 38.97844
172.1095 37.59968
172.5916 35.30605
173.0737 32.18808
173.5558 29.43613
174.0379 27.94359
174.5201 27.37409
175.0022 27.18010
175.4843 27.86138
175.9664 28.42654
176.4485 27.57587
176.9306 25.37984
177.4128 22.79077
177.8949 20.10255
178.3770 17.54162
178.8591 15.58584
179.3412 14.54340
179.8233 14.08144
180.3055 13.63168
180.7876 13.16950
181.2697 13.04372
181.7518 13.73249
182.2339 15.07116
182.7160 16.54422
183.1982 17.32659
183.6803 18.15717
184.1624 20.89013
184.6445 25.66540
185.1266 31.37173
185.6087 37.15135
186.0909 42.96129
186.5730 48.23761
187.0551 53.06413
187.5372 57.22315
188.0193 60.06878
188.5014 61.51717
188.9836 62.38309
189.4657 63.95740
189.9478 65.26250
190.4299 64.84340
190.9120 59.77611
191.3941 51.38922
191.8763 44.91646
192.3584 40.53647
192.8405 37.71555
193.3226 35.25702
193.8047 32.67675
194.2868 31.05474
194.7690 30.88715
195.2511 32.05016
195.7332 32.60569
196.2153 32.25813
196.6974 31.91392
197.1795 33.30439
197.6617 36.56205
198.1438 39.91396
198.6259 43.07022
199.1080 46.03134
199.5901 46.67685
200.0722 44.46564
200.5544 40.69619
201.0365 37.66652
201.5186 35.43301
202.0007 33.42098
202.4828 31.40088
202.9649 29.36780
203.4471 27.29807
203.9292 25.13397
204.4113 22.95684
204.8934 20.78312
205.3755 18.49435
205.8576 16.72018
206.3398 15.91715
206.8219 16.25612
207.3040 16.41855
207.7861 16.42077
208.2682 16.20417
208.7503 15.68863
209.2325 14.94569
209.7146 13.71871
210.1967 11.68549
210.6788 8.553455
211.1609 6.133451
211.6430 4.721320
212.1252 3.825297
212.6073 2.265689
213.0894 0.2513900
213.5715 2.637446
214.0536 2.785178
214.5357 1.935440
215.0179 1.010477
215.5000 0.2163920
215.9821 1.390975
216.4642 1.569594
216.9463 0.2619900
217.4284 0.9811390
217.9105 1.390989
218.3927 0.5539700
218.8748 0.2567690
219.3569 0.6913210
219.8390 1.549837
220.3211 2.082589
220.8032 1.909348
221.2854 2.120693
221.7675 3.194755
222.2496 2.050323
222.7317 0.4616150
223.2138 3.732440
223.6959 7.263832
224.1781 10.12978
224.6602 12.23182
225.1423 13.73243
225.6244 14.55796
226.1065 14.41739
226.5886 14.48677
227.0708 14.76005
227.5529 15.51614
228.0350 16.56756
228.5171 18.05619
228.9992 19.53365
229.4813 20.80848
229.9635 21.94271
230.4456 23.16414
230.9277 24.63564
231.4098 26.09896
231.8919 26.94707
232.3740 26.42569
232.8562 26.52698
233.3383 28.17303
233.8204 32.11058
234.3025 35.14687
234.7846 36.97783
235.2667 38.08721
235.7489 39.27460
236.2310 40.50189
236.7131 41.88165
237.1952 43.66034
237.6773 46.23614
238.1594 47.58313
238.6416 47.04883
239.1237 45.69218
239.6058 45.27981
240.0879 46.49829
240.5700 47.55140
241.0521 47.84820
241.5343 47.21521
242.0164 46.63257
242.4985 46.50003
242.9806 46.13289
243.4627 44.30586
243.9448 39.61345
244.4270 35.86994
244.9091 34.65198
245.3912 36.84079
245.8733 36.54631
246.3554 32.42045
246.8375 26.86535
247.3197 23.06962
247.8018 21.83222
248.2839 20.93040
248.7660 19.95046
249.2481 18.94520
249.7302 17.32618
250.2124 14.39972
250.6945 11.50418
251.1766 10.28743
251.6587 11.71751
252.1408 12.96285
252.6229 13.28935
253.1051 12.61763
253.5872 12.42716
254.0693 13.08059
254.5514 13.81957
255.0335 13.76035
255.5156 12.36253
255.9978 11.37239
256.4799 11.36328
256.9620 12.31582
257.4441 12.30383
257.9262 10.88294
258.4083 9.061540
258.8904 7.777581
259.3726 7.255445
259.8547 6.651675
260.3368 5.653828
260.8189 4.352106
261.3010 3.987844
261.7831 5.052613
262.2653 6.278276
262.7474 6.530375
263.2295 5.300663
263.7116 4.586025
264.1937 4.668987
264.6758 5.484366
265.1580 6.771350
265.6401 8.764135
266.1222 10.78601
266.6043 12.29963
267.0864 13.11475
267.5685 14.15073
268.0507 15.46654
268.5328 17.18200
269.0149 19.54025
269.4970 22.80210
269.9791 25.85164
270.4612 27.77857
270.9434 28.36660
271.4255 29.31563
271.9076 31.14595
272.3897 33.50217
272.8718 35.18464
273.3539 35.94911
273.8361 36.42028
274.3182 37.24086
274.8003 38.68533
275.2824 38.94936
275.7645 37.78627
276.2466 35.54740
276.7288 32.60370
277.2109 28.76430
277.6930 25.21674
278.1751 22.67351
278.6572 21.17489
279.1393 19.39083
279.6215 17.35545
280.1036 15.30793
280.5857 13.31430
281.0678 11.25325
281.5499 9.139317
282.0320 6.851154
282.5142 4.440573
282.9963 2.905301
283.4784 2.483236
283.9605 2.217090
284.4426 0.4159370
284.9247 2.652837
285.4069 0.4853270
285.8890 0.9941000
286.3711 2.012315
286.8532 0.4469460
287.3353 8.7879999E-03
287.8174 3.6309998E-02
288.2996 0.4302500
288.7817 1.141457
289.2638 1.785271
289.7459 2.273531
290.2280 2.621737
290.7101 2.771905
291.1923 2.703923
291.6744 2.820038
292.1565 3.545416
292.6386 4.786283
293.1207 6.097911
293.6028 7.457099
294.0850 8.742920
294.5671 9.860239
295.0492 10.79317
295.5313 11.38900
296.0134 11.36984
296.4955 10.90065
296.9777 10.39191
297.4598 9.804666
297.9419 9.426347
298.4240 9.919826
298.9061 11.11765
299.3882 12.15442
299.8704 12.29756
300.3525 11.96414
300.8346 12.00048
301.3167 12.55987
301.7988 13.25062
302.2809 13.82961
302.7631 14.23653
303.2452 14.29775
303.7273 13.45320
304.2094 12.39953
304.6915 12.17320
305.1736 12.87553
305.6558 13.81316
306.1379 14.19202
306.6200 14.37833
307.1021 15.05899
307.5842 17.01797
308.0663 19.28094
308.5485 20.97894
309.0306 22.09458
309.5127 22.94837
309.9948 23.47126
310.4769 23.93596
310.9590 24.68832
311.4412 25.94372
311.9233 27.54140
312.4054 29.75728
312.8875 32.40508
313.3696 34.40980
313.8517 34.91317
314.3339 34.59389
314.8160 33.99017
315.2981 33.02244
315.7802 32.32725
316.2623 32.68784
316.7444 33.64004
317.2266 33.92566
317.7087 32.70667
318.1908 30.87359
318.6729 28.91744
319.1550 26.85763
319.6371 24.83265
320.1193 23.18832
320.6014 21.56587
321.0835 19.35214
321.5656 15.56600
322.0477 11.83720
322.5298 8.660370
323.0120 6.009518
323.4941 4.252429
323.9762 4.490485
324.4583 5.265738
324.9404 5.004886
325.4225 2.018653
325.9047 0.5896850
326.3868 0.8780380
326.8689 0.5382090
327.3510 0.8166630
327.8331 9.1020003E-02
328.3152 2.126964
328.7974 2.575135
329.2795 0.6302220
329.7616 0.1237760
330.2437 1.010760
330.7258 0.6682950
331.2079 0.5035720
331.6901 0.7910960
332.1722 0.9933050
332.6543 0.8310910
333.1364 3.3466998E-02
333.6185 0.5959080
334.1006 0.9426990
334.5828 1.133922
335.0649 1.308501
335.5470 0.9303710
336.0291 0.3574100
336.5112 0.5438780
336.9933 1.925050
337.4755 2.890979
337.9576 3.372700
338.4397 3.512146
338.9218 3.379627
339.4039 2.795885
339.8860 2.635062
340.3681 3.378910
340.8503 4.917073
341.3324 5.496687
341.8145 4.907422
342.2966 3.974168
342.7787 3.087471
343.2608 2.511052
343.7430 2.473347
344.2251 3.328254
344.7072 4.728021
345.1893 5.368283
345.6714 5.186876
346.1535 4.718583
346.6357 4.099290
347.1178 3.544710
347.5999 3.968662
348.0820 5.548880
348.5641 7.672752
349.0462 9.281921
349.5284 10.54858
350.0105 11.75815
350.4926 12.75753
350.9747 13.72288
351.4568 15.98191
351.9389 19.70236
352.4211 23.00008
352.9032 23.52091
353.3853 22.16401
353.8674 20.99822
354.3495 20.81103
354.8316 21.26929
355.3138 22.03883
355.7959 22.96750
356.2780 24.12924
356.7601 26.02854
357.2422 27.97592
357.7243 29.01683
358.2065 28.35740
358.6886 27.53864
359.1707 27.98310
359.6528 29.20170
360.1349 29.72057
360.6170 27.66385
361.0992 25.38169
361.5813 24.80601
362.0634 26.85481
362.5455 28.47096
363.0276 28.81280
363.5097 27.86884
363.9919 25.62384
364.4740 20.43328
364.9561 15.41211
365.4382 11.82268
365.9203 9.816984
366.4024 8.032507
366.8846 6.279572
367.3667 4.582584
367.8488 2.962666
368.3309 1.057756
368.8130 0.3513010
369.2951 0.3961450
369.7773 0.3834360
370.2594 0.4409750
370.7415 0.4902980
371.2236 0.6979960
371.7057 0.3308990
372.1878 0.5848210
372.6700 1.371371
373.1521 1.939460
373.6342 2.412019
374.1163 3.039231
374.5984 3.925956
375.0805 4.730579
375.5627 5.245584
376.0448 5.406944
376.5269 6.075258
377.0090 7.330235
377.4911 8.949531
377.9732 10.84677
378.4554 13.09406
378.9375 15.02573
379.4196 16.44279
379.9017 17.47676
380.3838 18.56971
380.8659 19.67914
381.3481 21.11579
381.8302 23.35237
382.3123 26.24228
382.7944 28.61391
383.2765 30.27763
383.7586 31.54057
384.2408 32.80933
384.7229 34.23491
385.2050 36.26262
385.6871 40.33766
386.1692 44.90260
386.6513 47.01201
387.1335 46.40638
387.6156 44.95650
388.0977 44.09723
388.5798 43.70629
389.0619 43.44010
389.5440 43.25701
390.0262 43.02192
390.5083 42.72086
390.9904 42.32850
391.4725 41.62715
391.9546 40.19505
392.4367 38.57498
392.9189 37.36923
393.4010 37.10622
393.8831 36.32515
394.3652 33.73593
394.8473 30.21031
395.3294 27.24452
395.8116 26.24352
396.2937 25.14220
396.7758 22.81277
397.2579 19.01044
397.7400 15.88253
398.2221 14.36785
398.7043 13.45654
399.1864 12.33567
399.6685 10.77372
400.1506 9.176704
400.6327 7.685683
401.1148 6.221585
401.5970 4.361760
402.0791 1.631502
402.5612 0.9241300
403.0433 1.872846
403.5254 0.8733580
404.0075 0.1195090
404.4897 1.514845
404.9718 2.532419
405.4539 1.587027
405.9360 2.278603
406.4181 0.2462520
406.9002 0.8126650
407.3824 0.6728700
407.8645 2.446689
408.3466 0.3131860
408.8287 1.482729
409.3108 1.840229
409.7929 0.8298090
410.2751 4.5474999E-02
410.7572 0.4981850
411.2393 0.7940490
411.7214 1.238274
412.2035 1.864473
412.6856 2.285887
413.1678 4.2621002E-02
413.6499 3.018802
414.1320 5.728034
414.6141 8.211023
415.0962 9.820080
415.5783 9.068811
416.0605 7.134942
416.5426 6.246089
417.0247 7.940701
417.5068 10.34958
417.9889 11.79847
418.4710 12.49599
418.9532 13.44166
419.4353 15.43015
419.9174 17.72338
420.3995 19.68606
420.8816 21.11140
421.3637 22.47774
421.8459 23.85403
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423.2922 29.02603
423.7743 30.95483
424.2564 32.58003
424.7386 33.92221
425.2207 34.38152
425.7028 33.33601
426.1849 31.76063
426.6670 30.19116
427.1491 28.66365
427.6313 27.31894
428.1134 26.39034
428.5955 25.62951
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429.5597 22.12813
430.0418 20.03878
430.5240 18.11305
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431.4882 15.83161
431.9703 17.44230
432.4524 18.98886
432.9345 17.36750
433.4167 12.45678
433.8988 9.124539
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435.3451 11.57624
435.8272 11.54688
436.3094 11.41354
436.7915 11.59673
437.2736 12.09747
437.7557 12.76195
438.2378 13.56414
438.7199 14.94259
439.2020 17.77814
439.6841 21.50207
440.1663 24.94887
440.6484 27.17018
441.1305 29.30491
441.6126 32.31117
442.0947 36.07554
442.5768 39.90845
443.0590 43.37679
443.5411 46.84831
444.0232 50.59954
444.5053 54.71082
444.9874 59.04386
445.4695 63.32979
445.9517 67.79984
446.4338 72.87898
446.9159 78.46671
447.3980 84.87000
447.8801 92.41766
448.3622 101.2406
448.8444 109.6154
449.3265 117.1609
449.8086 124.6275
450.2907 132.4840
450.7728 140.8635
451.2549 149.6159
451.7371 159.1899
452.2192 168.7858
452.7013 176.6003
453.1834 182.4721
453.6655 186.9624
454.1476 190.3744
454.6298 192.6295
455.1119 193.0856
455.5940 191.8533
456.0761 188.1874
456.5582 180.8615
457.0403 170.2715
457.5225 158.3059
458.0046 145.0402
458.4867 131.5902
458.9688 119.6565
459.4509 109.1066
459.9330 99.91283
460.4152 92.64344
460.8973 86.17003
461.3794 78.95101
461.8615 70.75877
462.3436 63.67812
462.8257 59.55224
463.3079 57.18842
463.7900 55.07452
464.2721 52.67601
464.7542 50.73332
465.2363 49.67885
465.7184 49.25642
466.2006 49.10147
466.6827 49.03370
467.1648 49.06668
467.6469 49.19235
468.1290 49.28830
468.6111 49.85848
469.0933 51.01344
469.5754 52.57949
470.0575 54.45543
470.5396 56.84374
471.0217 59.34919
471.5038 61.96541
471.9860 64.48642
472.4681 66.21290
472.9502 67.03416
473.4323 67.43269
473.9144 67.80679
474.3965 68.12288
474.8787 67.19853
475.3608 64.94023
475.8429 61.88721
476.3250 58.54276
476.8071 54.91087
477.2892 50.95174
477.7714 46.51026
478.2535 42.01924
478.7356 38.22615
479.2177 34.98429
479.6998 31.75515
480.1819 27.88003
480.6641 24.00492
481.1462 20.80067
481.6283 18.31109
482.1104 16.41962
482.5925 15.41438
483.0746 14.83420
483.5568 14.20197
484.0389 13.75475
484.5210 12.85318
485.0031 11.01796
485.4852 8.557413
485.9673 6.369349
486.4495 4.123378
486.9316 2.635175
487.4137 2.384741
487.8958 3.732641
488.3779 4.455357
488.8600 4.364841
489.3422 3.827119
489.8243 3.078027
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