#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-05-24 15:26:36 +0300 (Thu, 24 May 2018) $
#$Revision: 708 $
#$URL: svn://172.16.1.111/rod/cif/1/00/02/1000217.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000217
loop_
_publ_author_name
'Gasperin, M.'
_publ_section_title
;
 Synthese et identification de deux oxydes doubles de tantale et d'etain
 Sample: synthetic
;
_journal_name_full
'Comptes Rendus Hebdomadaires des Seances de l Academie des Sciences'
_journal_page_first              2340
_journal_page_last               2342
_journal_volume                  240
_journal_year                    1955
_chemical_compound_source        R050546
_chemical_formula_sum            'O7 Pb2 Sb2'
_chemical_name_mineral           Bindheimite
_space_group_IT_number           227
_symmetry_space_group_name_Hall  'F 4d 2 3 -1d'
_symmetry_space_group_name_H-M   'F d -3 m :1'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_length_a                   10.40
_cell_length_b                   10.40
_cell_length_c                   10.40
_cell_volume                     1124.864
_exptl_crystal_density_diffrn    9.092
_cod_original_sg_symbol_H-M      'F d -3 m'
_cod_original_formula_sum        'Sb2 Pb2 O7'
_cod_database_code               9009948
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 15
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R050546.rod
_rod_data_source.block           3500000
_rod_database.code               1000217
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9009948 COD http://www.crystallography.net/cod/9009948.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
129.4954 0.0000000E+00
129.9775 17.62769
130.4596 52.92041
130.9418 94.11621
131.4239 130.7981
131.9060 158.7810
132.3881 180.2144
132.8702 201.6489
133.3523 223.1577
133.8345 240.2563
134.3166 248.6482
134.7987 248.2322
135.2808 243.2278
135.7629 233.9126
136.2450 220.6235
136.7272 205.4631
137.2093 188.1614
137.6914 169.2861
138.1735 148.7854
138.6556 126.2646
139.1377 104.4771
139.6199 83.10303
140.1020 62.35059
140.5841 46.30713
141.0662 35.42163
141.5483 29.12134
142.0304 26.67554
142.5126 28.15845
142.9947 32.10303
143.4768 32.13013
143.9589 23.58472
144.4410 16.63916
144.9231 11.18115
145.4053 7.412354
145.8874 5.589844
146.3695 6.575195
146.8516 8.156250
147.3337 9.679688
147.8158 10.71094
148.2980 12.83105
148.7801 16.17505
149.2622 20.69165
149.7443 25.92114
150.2264 33.57983
150.7085 40.90747
151.1907 46.47852
151.6728 50.21777
152.1549 54.82153
152.6370 60.27783
153.1191 66.60718
153.6012 68.76831
154.0834 62.85498
154.5655 56.54810
155.0476 51.23975
155.5297 48.56226
156.0118 43.97900
156.4939 36.84814
156.9761 28.70410
157.4582 22.58765
157.9403 17.99243
158.4224 14.04688
158.9045 11.05127
159.3866 7.206055
159.8688 5.000244
160.3509 5.926270
160.8330 9.905273
161.3151 13.29980
161.7972 12.93726
162.2793 11.23755
162.7615 11.21313
163.2436 14.57324
163.7257 17.47632
164.2078 20.03528
164.6899 21.62390
165.1720 23.11682
165.6541 25.92957
166.1363 28.38696
166.6184 29.42664
167.1005 27.12769
167.5826 24.35474
168.0647 21.75232
168.5468 20.19482
169.0290 18.99951
169.5111 18.18579
169.9932 18.64954
170.4753 17.80884
170.9574 15.42224
171.4395 13.10193
171.9217 11.38831
172.4038 10.57715
172.8859 9.466919
173.3680 6.517090
173.8501 2.714478
174.3322 0.2458500
174.8144 0.8256840
175.2965 0.5649410
175.7786 1.796387
176.2607 4.641724
176.7428 6.836060
177.2249 5.387329
177.7071 1.631958
178.1892 1.232178
178.6713 0.8698730
179.1534 1.058105
179.6355 0.5489385
180.1176 1.427979
180.5998 0.3513180
181.0819 0.4826660
181.5640 1.332275
182.0461 3.266113
182.5282 9.270996
183.0103 16.48486
183.4925 17.08838
183.9746 9.852295
184.4567 0.7868650
184.9388 2.524902
185.4209 0.8427730
185.9030 1.295410
186.3852 2.335205
186.8673 2.197021
187.3494 3.778814
187.8315 2.660156
188.3136 6.557129
188.7957 9.188965
189.2779 10.59106
189.7600 11.37573
190.2421 11.47168
190.7242 11.06860
191.2063 11.43628
191.6884 12.89355
192.1706 14.53247
192.6527 14.97559
193.1348 14.23901
193.6169 12.99756
194.0990 11.19385
194.5811 8.960205
195.0633 7.951416
195.5454 8.607910
196.0275 9.862305
196.5096 9.300293
196.9917 6.681396
197.4738 4.846924
197.9560 5.796875
198.4381 9.512939
198.9202 11.96899
199.4023 12.68652
199.8844 12.39624
200.3665 12.56958
200.8487 13.25659
201.3308 13.84351
201.8129 13.86914
202.2950 13.24658
202.7771 13.04712
203.2592 13.41553
203.7414 14.10571
204.2235 14.82837
204.7056 15.86035
205.1877 15.98926
205.6698 14.13428
206.1519 9.813965
206.6341 6.983398
207.1162 6.279541
207.5983 6.777588
208.0804 6.127686
208.5625 3.733154
209.0446 2.103760
209.5268 3.230225
210.0089 8.343262
210.4910 9.974365
210.9731 6.514893
211.4552 0.4077150
211.9373 1.944092
212.4195 1.124512
212.9016 3.673096
213.3837 2.294434
213.8658 4.699951
214.3479 9.484863
214.8300 11.44775
215.3121 11.42261
215.7943 11.35547
216.2764 11.18066
216.7585 11.01196
217.2406 10.81982
217.7227 10.41431
218.2048 10.42480
218.6870 10.82495
219.1691 11.59546
219.6512 12.99194
220.1333 15.79321
220.6154 17.76123
221.0975 17.57275
221.5797 13.74390
222.0618 12.22290
222.5439 13.97754
223.0260 17.62988
223.5081 20.28223
223.9902 22.01294
224.4724 22.68872
224.9545 21.95142
225.4366 18.93628
225.9187 17.26367
226.4008 17.50269
226.8829 18.83716
227.3651 19.44531
227.8472 18.75732
228.3293 18.31567
228.8114 18.75610
229.2935 20.39062
229.7757 21.72534
230.2578 22.28955
230.7399 22.72192
231.2220 24.45166
231.7041 28.38184
232.1862 31.87451
232.6684 34.12134
233.1505 34.94849
233.6326 35.01123
234.1147 33.54297
234.5968 31.59229
235.0789 31.33008
235.5611 33.88989
236.0432 36.63647
236.5253 38.73682
237.0074 40.18237
237.4895 40.27173
237.9716 37.83740
238.4538 34.95068
238.9359 35.09595
239.4180 40.31958
239.9001 45.36401
240.3822 48.62622
240.8643 49.45264
241.3465 50.30713
241.8286 51.21802
242.3107 51.92041
242.7928 52.35376
243.2749 52.82568
243.7570 53.30981
244.2392 53.52856
244.7213 53.22876
245.2034 53.90723
245.6855 56.28198
246.1676 58.77979
246.6497 59.36694
247.1319 56.74609
247.6140 54.92285
248.0961 55.16602
248.5782 57.82642
249.0603 59.91626
249.5424 61.19824
250.0246 62.08032
250.5067 63.08081
250.9888 64.13867
251.4709 65.72363
251.9530 68.06909
252.4351 71.26685
252.9173 74.24438
253.3994 76.67603
253.8815 78.98242
254.3636 81.78125
254.8457 85.37280
255.3278 88.89038
255.8100 91.95117
256.2921 94.38818
256.7742 96.58618
257.2563 98.60718
257.7384 100.6047
258.2205 102.5754
258.7026 104.5352
259.1848 106.5095
259.6669 108.7429
260.1490 111.2053
260.6311 112.5168
261.1132 111.9258
261.5953 111.3882
262.0775 112.3547
262.5596 115.1941
263.0417 118.6428
263.5238 123.0359
264.0059 128.1941
264.4880 132.5527
264.9702 135.2788
265.4523 138.1875
265.9344 142.4924
266.4165 148.5073
266.8986 155.4253
267.3807 163.6357
267.8629 172.1709
268.3450 178.9617
268.8271 184.2556
269.3092 188.6006
269.7913 191.5640
270.2734 192.3945
270.7556 195.4438
271.2377 201.9053
271.7198 210.3491
272.2019 217.2461
272.6840 222.1877
273.1661 227.1995
273.6483 232.9536
274.1304 239.2988
274.6125 247.7473
275.0946 259.0466
275.5767 271.3135
276.0588 280.3518
276.5410 285.0422
277.0231 291.8657
277.5052 304.9587
277.9873 324.5034
278.4694 338.2871
278.9515 345.0134
279.4337 348.5173
279.9158 353.9197
280.3979 361.2986
280.8800 369.2842
281.3621 377.6833
281.8442 386.3743
282.3264 393.3403
282.8085 398.1963
283.2906 402.8462
283.7727 409.9150
284.2548 419.4709
284.7369 428.3838
285.2191 435.6538
285.7012 441.6086
286.1833 447.5481
286.6654 453.3826
287.1475 459.8933
287.6296 468.3049
288.1118 478.3931
288.5939 487.5298
289.0760 494.9258
289.5581 501.0679
290.0402 507.6123
290.5223 514.6057
291.0045 520.7703
291.4866 524.4807
291.9687 526.3281
292.4508 529.3079
292.9329 534.3696
293.4150 540.1948
293.8972 545.1726
294.3793 549.2817
294.8614 551.9746
295.3435 552.1589
295.8256 550.6333
296.3077 549.2708
296.7899 548.0613
297.2720 547.8867
297.7541 551.3665
298.2362 557.5037
298.7183 561.8784
299.2004 560.3936
299.6826 555.7900
300.1647 553.4067
300.6468 553.8870
301.1289 554.7769
301.6110 553.5586
302.0931 550.7017
302.5753 547.4670
303.0574 544.7397
303.5395 541.8203
304.0216 537.5374
304.5037 531.8054
304.9858 526.1584
305.4680 522.4204
305.9501 519.5972
306.4322 515.9971
306.9143 510.9219
307.3964 504.9014
307.8785 497.7688
308.3607 489.7429
308.8428 482.4038
309.3249 477.5898
309.8070 473.7761
310.2891 469.0044
310.7712 461.0615
311.2534 454.0166
311.7355 451.7119
312.2176 452.9365
312.6997 453.3672
313.1818 450.5015
313.6639 445.9524
314.1461 440.7856
314.6282 434.8315
315.1103 429.1738
315.5924 424.0930
316.0745 419.7178
316.5566 416.2429
317.0388 415.0461
317.5209 413.9043
318.0030 411.5691
318.4851 407.7949
318.9672 403.3293
319.4493 397.9680
319.9315 392.2441
320.4136 386.7773
320.8957 380.7209
321.3778 375.9597
321.8599 373.7368
322.3420 374.3711
322.8242 374.1980
323.3063 372.4529
323.7884 369.5645
324.2705 365.9038
324.7526 360.3132
325.2347 355.1929
325.7169 351.2927
326.1990 348.4812
326.6811 345.6265
327.1632 342.3284
327.6453 339.1782
328.1274 336.5095
328.6096 334.7153
329.0917 332.9189
329.5738 331.4167
330.0559 329.9587
330.5380 327.6655
331.0201 324.1599
331.5023 320.2341
331.9844 315.9822
332.4665 310.6653
332.9486 307.0491
333.4307 306.2764
333.9128 306.6194
334.3950 305.1689
334.8771 301.3379
335.3592 296.7344
335.8413 291.6543
336.3234 285.9541
336.8055 280.8870
337.2877 276.5320
337.7698 273.1001
338.2519 270.4270
338.7340 268.2368
339.2161 266.2070
339.6982 265.0037
340.1803 264.4348
340.6624 261.6440
341.1446 255.9021
341.6267 249.7341
342.1088 245.0500
342.5909 242.0510
343.0730 240.2312
343.5551 240.0327
344.0373 240.2292
344.5194 237.9443
345.0015 233.0288
345.4836 227.3953
345.9657 221.7358
346.4478 216.1514
346.9300 211.4290
347.4121 207.6506
347.8942 204.8652
348.3763 203.7234
348.8584 203.8711
349.3405 203.0063
349.8227 198.9421
350.3048 193.2634
350.7869 189.8179
351.2690 188.8228
351.7511 188.2815
352.2332 186.2075
352.7154 182.9753
353.1975 179.5007
353.6796 175.6113
354.1617 172.1394
354.6438 169.9653
355.1259 169.0378
355.6081 169.0247
356.0902 171.1274
356.5723 173.2192
357.0544 172.4529
357.5365 167.0811
358.0186 161.8542
358.5008 160.5933
358.9829 161.6252
359.4650 161.7068
359.9471 159.5488
360.4292 156.1443
360.9113 151.5020
361.3935 145.3809
361.8756 140.2603
362.3577 137.5918
362.8398 136.2622
363.3219 135.0691
363.8040 135.1438
364.2862 133.9849
364.7683 130.6416
365.2504 125.1709
365.7325 119.0195
366.2146 110.4231
366.6967 102.6079
367.1789 97.61890
367.6610 99.08838
368.1431 99.77222
368.6252 99.26416
369.1073 97.03247
369.5894 92.69604
370.0716 82.92188
370.5537 74.78174
371.0358 71.15161
371.5179 74.12964
372.0000 75.33252
372.4821 74.32471
372.9643 71.81274
373.4464 68.54443
373.9285 63.95654
374.4106 59.79468
374.8927 56.40576
375.3748 53.74561
375.8570 51.57056
376.3391 49.93555
376.8212 48.54907
377.3033 47.01318
377.7854 45.21948
378.2675 44.29639
378.7497 44.84009
379.2318 45.92651
379.7139 44.96851
380.1960 41.85596
380.6781 38.36694
381.1602 35.80225
381.6424 33.92944
382.1245 30.78931
382.6066 25.95728
383.0887 21.26343
383.5708 19.59570
384.0529 20.33545
384.5351 20.32007
385.0172 17.72363
385.4993 13.87109
385.9814 10.55566
386.4635 7.829102
386.9456 6.205322
387.4278 7.096924
387.9099 9.170898
388.3920 10.19336
388.8741 9.113770
389.3562 7.616943
389.8383 7.114014
390.3205 7.342041
390.8026 7.624756
391.2847 7.575195
391.7668 7.437744
392.2489 7.571289
392.7310 8.184570
393.2132 8.135742
393.6953 6.878662
394.1774 4.665771
394.6595 1.765137
395.1416 4.409424
395.6237 2.452017
396.1059 2.190220
396.5880 1.971436
397.0701 1.844971
397.5522 0.6320800
398.0343 1.732178
398.5164 2.954590
398.9986 1.006348
399.4807 0.2651370
399.9628 1.588379
400.4449 4.125732
400.9270 5.956299
401.4091 6.875732
401.8913 7.305908
402.3734 7.317627
402.8555 6.855957
403.3376 6.212646
403.8197 5.060303
404.3018 4.136963
404.7840 4.355469
405.2661 6.053467
405.7482 7.886475
406.2303 9.856445
406.7124 11.76025
407.1945 12.45581
407.6767 11.67114
408.1588 11.15747
408.6409 12.64429
409.1230 15.93213
409.6051 17.74756
410.0872 17.63745
410.5694 16.63354
411.0515 16.02905
411.5336 15.80713
412.0157 15.97681
412.4978 16.83740
412.9799 17.96387
413.4621 18.34375
413.9442 17.97485
414.4263 17.72461
414.9084 18.87842
415.3905 20.46191
415.8727 20.75366
416.3548 18.54541
416.8369 16.14819
417.3190 15.72681
417.8011 16.69263
418.2832 17.47583
418.7654 17.67017
419.2475 17.18433
419.7296 15.82422
420.2117 13.45825
420.6938 10.99585
421.1759 8.594971
421.6581 6.403320
422.1402 4.530762
422.6223 2.841553
423.1044 1.710205
423.5865 1.089600
424.0686 1.049316
424.5508 2.048096
425.0329 6.825928
425.5150 10.44507
425.9971 10.48804
426.4792 4.718506
426.9613 6.6895001E-02
427.4435 3.604736
427.9256 6.313232
428.4077 8.738770
428.8898 10.72290
429.3719 12.92505
429.8540 15.65967
430.3362 18.85449
430.8183 21.24268
431.3004 22.16113
431.7825 24.15234
432.2646 30.65039
432.7467 41.64648
433.2289 49.12061
433.7110 51.25513
434.1931 50.38208
434.6752 50.25366
435.1573 50.82324
435.6394 51.70679
436.1216 51.97607
436.6036 52.53931
437.0858 55.85596
437.5679 62.03027
438.0500 68.76221
438.5321 74.50513
439.0142 79.34937
439.4963 83.27930
439.9785 85.33325
440.4606 87.86377
440.9427 93.52051
441.4248 101.3464
441.9069 108.3875
442.3890 113.4526
442.8712 117.1541
443.3533 119.2388
443.8354 119.0554
444.3175 120.6104
444.7996 127.0000
445.2817 135.0117
445.7639 141.3428
446.2460 142.1150
446.7281 144.7402
447.2102 151.7322
447.6923 162.3235
448.1744 170.7971
448.6566 175.3503
449.1387 179.6145
449.6208 185.3037
450.1029 193.2988
450.5850 200.1455
451.0671 205.7104
451.5493 210.1619
452.0314 213.4590
452.5135 215.2539
452.9956 216.9707
453.4777 219.2024
453.9598 222.0471
454.4420 224.8459
454.9241 227.3865
455.4062 229.8271
455.8883 232.1401
456.3704 234.5059
456.8525 237.7134
457.3347 241.8301
457.8168 246.0024
458.2989 249.0083
458.7810 251.2183
459.2631 253.4775
459.7452 256.8499
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