#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-05-24 15:34:35 +0300 (Thu, 24 May 2018) $
#$Revision: 738 $
#$URL: svn://172.16.1.111/rod/cif/1/00/02/1000242.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000242
loop_
_publ_author_name
'Burns, P. C.'
_publ_section_title
;
 The structure of edoylerite determined from a microcrystal
;
_journal_name_full               'The Canadian Mineralogist'
_journal_page_first              113
_journal_page_last               118
_journal_volume                  37
_journal_year                    1999
_chemical_compound_source        R060543
_chemical_formula_sum            'Cr Hg3 O4 S2'
_chemical_name_mineral           Edoylerite
_space_group_IT_number           14
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90
_cell_angle_beta                 118.746
_cell_angle_gamma                90
_cell_length_a                   7.5283
_cell_length_b                   14.8325
_cell_length_c                   7.4629
_cell_volume                     730.634
_exptl_crystal_density_diffrn    7.108
_cod_original_formula_sum        'Hg3 Cr S2 O4'
_cod_database_code               9004520
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 15
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R060543.rod
_rod_data_source.block           3500000
_rod_database.code               1000242
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9004520 COD http://www.crystallography.net/cod/9004520.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
97.01495 0.0000000E+00
97.49707 5.359863
97.97919 13.82422
98.46130 23.44385
98.94342 25.03223
99.42554 14.93066
99.90765 5.117676
100.3898 3.291992
100.8719 18.23291
101.3540 38.34912
101.8361 48.83008
102.3182 51.23682
102.8004 46.41113
103.2825 34.27100
103.7646 22.02832
104.2467 7.640137
104.7288 5.363770
105.2109 8.612793
105.6931 0.4238280
106.1752 15.58203
106.6573 34.85645
107.1394 61.15039
107.6215 87.32666
108.1036 113.6963
108.5858 140.4170
109.0679 166.9399
109.5500 195.2163
110.0321 222.5952
110.5142 247.5098
110.9963 273.6147
111.4785 293.9272
111.9606 306.6289
112.4427 312.0859
112.9248 315.5913
113.4069 319.0786
113.8890 320.4692
114.3712 318.1514
114.8533 307.9189
115.3354 297.5161
115.8175 289.4673
116.2996 283.9790
116.7817 279.1143
117.2639 275.3154
117.7460 271.4531
118.2281 266.0874
118.7102 255.7920
119.1923 245.5742
119.6744 238.6221
120.1566 235.5396
120.6387 233.4985
121.1208 229.3545
121.6029 224.7222
122.0850 223.0347
122.5671 227.1743
123.0493 234.2573
123.5314 241.8457
124.0135 250.0859
124.4956 256.8638
124.9777 258.6255
125.4598 256.3970
125.9420 254.3584
126.4241 254.7227
126.9062 256.9937
127.3883 260.6787
127.8704 266.4062
128.3525 272.2861
128.8347 274.7515
129.3168 273.9893
129.7989 273.4565
130.2810 277.4302
130.7631 284.4561
131.2452 288.5659
131.7274 287.0303
132.2095 282.2910
132.6916 281.2656
133.1737 284.5171
133.6558 288.7573
134.1379 290.3843
134.6201 289.5469
135.1022 290.1641
135.5843 294.0259
136.0664 300.4512
136.5485 304.4087
137.0306 305.1802
137.5128 305.6875
137.9949 310.1270
138.4770 319.6865
138.9591 329.4385
139.4412 335.7891
139.9233 338.1890
140.4055 341.5488
140.8876 346.7427
141.3697 352.2065
141.8518 357.6191
142.3339 363.9097
142.8160 367.2329
143.2982 364.8594
143.7803 355.1948
144.2624 350.1587
144.7445 352.1987
145.2266 357.8916
145.7087 359.2993
146.1909 354.2212
146.6730 347.7651
147.1551 341.7734
147.6372 336.0391
148.1193 332.6646
148.6014 333.0908
149.0836 336.2114
149.5657 335.8647
150.0478 329.9326
150.5299 322.7388
151.0120 316.4604
151.4941 308.2515
151.9763 301.0273
152.4584 296.8789
152.9405 295.4595
153.4226 294.4683
153.9047 295.6504
154.3868 295.2378
154.8690 292.1777
155.3511 281.1079
155.8332 270.1187
156.3153 259.4204
156.7974 249.1855
157.2795 241.1113
157.7617 239.5044
158.2438 238.5752
158.7259 234.2153
159.2080 220.9541
159.6901 208.7266
160.1722 201.3496
160.6544 198.6992
161.1365 195.6675
161.6186 189.8120
162.1007 183.2192
162.5828 177.4175
163.0649 173.5337
163.5471 171.1416
164.0292 169.9941
164.5113 169.9248
164.9934 168.4351
165.4755 162.7295
165.9576 155.0923
166.4398 148.4600
166.9219 144.9854
167.4040 142.1870
167.8861 138.5254
168.3682 133.7964
168.8503 128.8218
169.3325 123.8936
169.8146 119.0752
170.2967 114.4614
170.7788 111.2266
171.2609 107.8330
171.7430 102.5522
172.2252 95.20020
172.7073 87.87744
173.1894 81.63525
173.6715 76.59473
174.1536 73.07715
174.6357 71.81641
175.1179 71.75293
175.6000 72.06055
176.0821 72.96582
176.5642 72.95020
177.0463 70.37793
177.5284 65.57031
178.0106 59.59082
178.4927 52.32910
178.9748 44.48438
179.4569 36.71582
179.9390 28.64062
180.4211 22.49219
180.9033 21.88574
181.3854 26.05176
181.8675 30.95215
182.3496 35.68945
182.8317 39.44336
183.3138 40.17383
183.7960 36.88574
184.2781 32.48242
184.7602 31.50977
185.2423 33.55957
185.7244 35.01953
186.2065 32.50879
186.6887 27.31348
187.1708 24.29883
187.6529 23.74805
188.1350 25.80371
188.6171 32.49316
189.0992 43.72852
189.5814 52.94727
190.0635 54.86426
190.5456 50.58203
191.0277 46.75098
191.5098 44.11230
191.9919 42.38770
192.4741 41.15332
192.9562 40.42969
193.4383 39.57129
193.9204 37.72168
194.4025 34.97070
194.8846 33.09668
195.3668 32.37598
195.8489 32.50586
196.3310 33.27734
196.8131 34.87500
197.2952 35.46777
197.7773 32.68555
198.2595 26.33398
198.7416 23.57520
199.2237 26.44922
199.7058 32.48047
200.1879 34.39746
200.6700 31.68652
201.1522 27.91211
201.6343 25.84863
202.1164 25.83789
202.5985 24.39355
203.0806 20.83301
203.5627 15.67090
204.0449 9.880859
204.5270 2.754883
205.0091 2.902344
205.4912 4.043945
205.9733 0.5429690
206.4554 1.851563
206.9376 1.955078
207.4197 9.573242
207.9018 16.36914
208.3839 22.76562
208.8660 27.12695
209.3481 27.59570
209.8303 22.91309
210.3124 19.32812
210.7945 17.31543
211.2766 16.80566
211.7587 18.00098
212.2408 22.05371
212.7230 25.21484
213.2051 24.83301
213.6872 20.23535
214.1693 14.45996
214.6514 7.264648
215.1335 0.6250000
215.6157 5.253906
216.0978 5.228516
216.5799 4.180664
217.0620 4.960938
217.5441 9.106445
218.0262 10.03613
218.5084 6.040039
218.9905 1.697266
219.4726 7.454102
219.9547 10.85840
220.4368 12.69336
220.9189 13.26953
221.4011 11.88965
221.8832 10.39746
222.3653 8.472656
222.8474 6.348633
223.3295 4.742188
223.8116 3.284180
224.2938 3.081055
224.7759 5.344727
225.2580 12.12891
225.7401 16.63379
226.2222 18.03418
226.7043 16.92383
227.1865 15.08984
227.6686 12.07910
228.1507 9.476563
228.6328 8.193359
229.1149 8.064453
229.5970 9.893555
230.0792 14.86328
230.5613 21.78809
231.0434 26.22070
231.5255 27.78809
232.0076 27.19238
232.4897 24.41797
232.9719 17.76270
233.4540 12.42578
233.9361 9.146484
234.4182 7.076172
234.9003 7.328649
235.3824 4.030273
235.8646 11.31543
236.3467 17.12109
236.8288 20.13770
237.3109 24.04199
237.7930 28.25488
238.2751 33.32324
238.7573 41.17480
239.2394 54.14258
239.7215 66.61816
240.2036 75.82227
240.6857 79.16992
241.1678 84.31934
241.6500 90.71387
242.1321 98.67383
242.6142 110.3027
243.0963 128.9971
243.5784 146.3896
244.0605 158.1514
244.5427 161.3789
245.0248 166.4590
245.5069 173.0859
245.9890 182.1416
246.4711 195.5615
246.9532 216.4521
247.4354 237.2119
247.9175 253.5928
248.3996 262.1895
248.8817 278.1504
249.3638 303.1104
249.8459 334.7666
250.3281 368.9150
250.8102 405.8555
251.2923 445.2461
251.7744 487.3506
252.2565 531.4160
252.7386 579.3506
253.2208 630.5059
253.7029 686.0762
254.1850 749.8467
254.6671 825.7490
255.1492 902.2549
255.6313 974.0293
256.1135 1038.704
256.5956 1110.368
257.0777 1187.970
257.5598 1274.358
258.0419 1365.761
258.5240 1467.585
259.0062 1574.829
259.4883 1689.088
259.9704 1808.925
260.4525 1924.381
260.9346 2029.146
261.4167 2135.318
261.8989 2258.313
262.3810 2402.803
262.8631 2548.602
263.3452 2688.708
263.8273 2825.663
264.3094 2969.431
264.7916 3121.892
265.2737 3281.308
265.7558 3449.060
266.2379 3624.604
266.7200 3808.279
267.2021 4007.103
267.6843 4217.755
268.1664 4412.143
268.6485 4585.764
269.1306 4751.059
269.6127 4919.094
270.0948 5093.704
270.5770 5249.403
271.0591 5379.739
271.5412 5486.711
272.0233 5585.355
272.5054 5678.286
272.9875 5750.256
273.4697 5789.452
273.9518 5794.675
274.4339 5776.084
274.9160 5738.310
275.3981 5676.012
275.8802 5570.095
276.3624 5420.134
276.8445 5233.582
277.3266 5009.629
277.8087 4746.681
278.2908 4470.561
278.7729 4179.149
279.2551 3881.200
279.7372 3600.392
280.2193 3335.525
280.7014 3090.418
281.1835 2863.952
281.6656 2656.166
282.1478 2471.582
282.6299 2311.903
283.1120 2171.979
283.5941 2045.258
284.0762 1931.580
284.5583 1828.795
285.0405 1736.791
285.5226 1654.938
286.0047 1575.960
286.4868 1498.484
286.9689 1427.928
287.4510 1380.560
287.9332 1354.456
288.4153 1312.027
288.8974 1232.333
289.3795 1124.841
289.8616 1023.650
290.3438 928.2881
290.8259 843.2021
291.3080 775.9629
291.7901 724.8701
292.2722 676.7891
292.7543 627.3203
293.2365 578.6357
293.7186 535.9971
294.2007 499.7197
294.6828 468.6035
295.1649 443.7266
295.6470 423.7314
296.1292 403.5312
296.6113 381.9326
297.0934 359.6348
297.5755 337.3477
298.0576 315.0703
298.5397 293.1924
299.0219 270.4736
299.5040 248.3633
299.9861 230.6924
300.4682 219.6064
300.9503 210.6035
301.4324 197.6934
301.9146 181.9775
302.3967 167.4854
302.8788 157.5684
303.3609 150.2822
303.8430 142.5928
304.3251 133.6836
304.8073 125.7451
305.2894 119.9775
305.7715 116.5508
306.2536 116.0342
306.7357 118.4375
307.2178 123.7822
307.7000 132.3584
308.1821 144.1855
308.6642 157.5732
309.1463 171.4131
309.6284 185.7031
310.1105 200.8047
310.5927 214.4502
311.0748 230.2959
311.5569 253.1338
312.0390 282.9541
312.5211 311.0557
313.0032 330.6182
313.4854 347.1768
313.9675 366.2979
314.4496 393.6436
314.9317 420.7402
315.4138 441.7109
315.8959 458.0537
316.3781 479.1621
316.8602 509.6855
317.3423 546.0859
317.8244 585.9814
318.3065 630.9033
318.7886 676.3418
319.2708 717.6104
319.7529 757.5303
320.2350 804.3652
320.7171 858.1465
321.1992 920.4492
321.6813 992.9229
322.1635 1079.345
322.6456 1167.225
323.1277 1253.423
323.6098 1339.511
324.0919 1428.585
324.5740 1525.843
325.0562 1620.464
325.5383 1711.987
326.0204 1804.168
326.5025 1877.479
326.9846 1931.846
327.4667 1966.271
327.9489 1980.535
328.4310 1978.021
328.9131 1952.237
329.3952 1900.533
329.8773 1822.824
330.3594 1727.941
330.8416 1604.984
331.3237 1475.268
331.8058 1353.552
332.2879 1238.708
332.7700 1132.654
333.2521 1031.368
333.7343 937.3438
334.2164 863.8799
334.6985 818.8164
335.1806 782.9775
335.6627 745.4619
336.1448 702.3340
336.6270 670.3389
337.1091 650.8984
337.5912 642.3408
338.0733 643.1455
338.5554 656.1807
339.0375 669.3320
339.5197 676.2783
340.0018 676.0801
340.4839 683.7686
340.9660 701.2207
341.4481 722.5137
341.9302 741.9102
342.4124 760.0605
342.8945 769.2822
343.3766 766.5088
343.8587 752.2998
344.3408 730.7852
344.8229 702.0801
345.3051 668.9316
345.7872 632.6123
346.2693 592.5967
346.7514 547.2139
347.2335 494.7236
347.7156 440.7998
348.1978 396.4521
348.6799 361.5117
349.1620 333.2607
349.6441 312.9199
350.1262 297.7656
350.6083 280.3535
351.0905 258.6709
351.5726 240.1367
352.0547 231.9932
352.5368 232.4512
353.0189 238.1982
353.5010 249.3711
353.9832 265.6025
354.4653 286.9600
354.9474 313.4746
355.4295 340.6318
355.9116 362.9434
356.3937 384.2227
356.8759 409.7031
357.3580 443.1221
357.8401 479.2891
358.3222 514.2842
358.8043 549.5244
359.2864 588.5566
359.7686 632.0293
360.2507 680.5312
360.7328 734.7715
361.2149 798.8027
361.6970 862.5127
362.1791 921.9316
362.6613 977.9209
363.1434 1032.558
363.6255 1084.654
364.1076 1136.800
364.5897 1193.704
365.0718 1260.466
365.5540 1311.388
366.0361 1339.427
366.5182 1350.014
367.0003 1349.618
367.4824 1329.588
367.9645 1308.577
368.4467 1289.161
368.9288 1271.715
369.4109 1259.056
369.8930 1255.320
370.3751 1253.660
370.8572 1250.033
371.3394 1248.613
371.8215 1238.491
372.3036 1220.527
372.7857 1193.233
373.2678 1150.627
373.7499 1088.518
374.2321 1017.927
374.7142 941.9473
375.1963 856.4805
375.6784 778.6768
376.1605 708.5879
376.6426 647.4141
377.1248 599.9307
377.6069 566.6758
378.0890 538.7832
378.5711 514.6201
379.0532 493.4023
379.5353 470.9199
380.0175 446.0342
380.4996 425.4863
380.9817 417.3467
381.4638 420.7236
381.9459 425.8701
382.4280 429.8262
382.9102 434.3369
383.3923 442.3066
383.8744 453.8828
384.3565 469.1973
384.8386 493.6289
385.3207 521.1045
385.8029 537.4805
386.2850 540.4912
386.7671 536.7959
387.2492 535.9375
387.7313 533.8867
388.2134 521.2393
388.6956 490.4941
389.1777 449.6416
389.6598 403.0586
390.1419 351.4971
390.6240 300.6982
391.1061 253.3350
391.5883 208.6836
392.0704 165.3398
392.5525 118.8525
393.0346 79.81641
393.5167 54.16113
393.9988 39.28125
394.4810 27.65723
394.9631 18.38379
395.4452 10.41602
395.9273 2.827148
396.4094 5.507813
396.8915 0.1920472
397.3737 6.808594
397.8558 0.7880860
398.3379 0.8916020
398.8200 7.285156
399.3021 15.07324
399.7842 21.98340
400.2664 28.10938
400.7485 28.74121
401.2306 18.26367
401.7127 8.080078
402.1948 6.549805
402.6769 21.54004
403.1591 27.63672
403.6412 19.09473
404.1233 2.829102
404.6054 3.605469
405.0875 2.461914
405.5696 10.53125
406.0518 16.62500
406.5339 20.61719
407.0160 23.34961
407.4981 24.01270
407.9802 25.02832
408.4623 31.50781
408.9445 43.12402
409.4266 47.48145
409.9087 38.01562
410.3908 21.74902
410.8729 16.31738
411.3550 21.34668
411.8372 27.92090
412.3193 30.24316
412.8014 29.35449
413.2835 28.18555
413.7656 27.55566
414.2477 25.15430
414.7299 16.34082
415.2120 3.852539
415.6941 5.677734
416.1762 4.520508
416.6583 1.738281
417.1404 6.436523
417.6226 18.39551
418.1047 29.85156
418.5868 34.63672
419.0689 37.30078
419.5510 42.56348
420.0331 54.54004
420.5153 65.21582
420.9974 72.83789
421.4795 77.02637
421.9616 76.29883
422.4437 64.66016
422.9258 53.12402
423.4080 47.31836
423.8901 50.30859
424.3722 50.05371
424.8543 42.98145
425.3364 33.87402
425.8185 27.41895
426.3007 25.56836
426.7828 23.62207
427.2649 20.42969
427.7470 16.42871
428.2291 14.64941
428.7112 16.03027
429.1934 17.78125
429.6755 18.60156
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