#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-05-24 15:34:39 +0300 (Thu, 24 May 2018) $
#$Revision: 739 $
#$URL: svn://172.16.1.111/rod/cif/1/00/02/1000243.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000243
loop_
_publ_author_name
'Hill, R. J.'
_publ_section_title
;
 The crystal structure and infrared properties of adamite
;
_journal_name_full               'American Mineralogist'
_journal_page_first              979
_journal_page_last               986
_journal_volume                  61
_journal_year                    1976
_chemical_compound_source        R060593
_chemical_formula_sum            'As H O5 Zn2'
_chemical_name_mineral           Adamite
_space_group_IT_number           58
_symmetry_space_group_name_Hall  '-P 2 2n'
_symmetry_space_group_name_H-M   'P n n m'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_length_a                   8.306
_cell_length_b                   8.524
_cell_length_c                   6.043
_cell_volume                     427.846
_exptl_crystal_density_diffrn    4.451
_cod_original_formula_sum        'As Zn2 O5 H'
_cod_database_code               9000521
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 15
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R060593.rod
_rod_data_source.block           3500000
_rod_database.code               1000243
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9000521 COD http://www.crystallography.net/cod/9000521.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
177.7553 0.0000000E+00
178.2374 3.211426
178.7195 3.595459
179.2017 3.695068
179.6838 4.126526
180.1659 2.734070
180.6480 6.160767
181.1301 6.980286
181.6122 5.060730
182.0944 3.746582
182.5765 2.188232
183.0586 1.287476
183.5407 5.095032
184.0228 5.298096
184.5049 1.591064
184.9871 3.752930
185.4692 8.779175
185.9513 13.38062
186.4334 16.46082
186.9155 15.92780
187.3976 13.31171
187.8798 14.35022
188.3619 19.74579
188.8440 26.59210
189.3261 31.14374
189.8082 33.53296
190.2903 34.46234
190.7725 33.38025
191.2546 30.81995
191.7367 29.96436
192.2188 31.27197
192.7009 33.47107
193.1830 34.21826
193.6652 33.48962
194.1473 33.02026
194.6294 33.35608
195.1115 34.53479
195.5936 37.79626
196.0757 43.96375
196.5579 50.91187
197.0400 53.81885
197.5221 52.25989
198.0042 51.22180
198.4863 53.83447
198.9684 60.11804
199.4506 66.39270
199.9327 72.41174
200.4148 78.19727
200.8969 83.20862
201.3790 87.14490
201.8611 92.28369
202.3433 101.0494
202.8254 114.0043
203.3075 123.7031
203.7896 128.6919
204.2717 130.8086
204.7538 134.3556
205.2360 139.3462
205.7181 145.6063
206.2002 153.8616
206.6823 164.8049
207.1644 172.9113
207.6465 177.2958
208.1287 178.7882
208.6108 179.8799
209.0929 180.5068
209.5750 180.8967
210.0571 181.5221
210.5392 182.8866
211.0214 182.1642
211.5035 178.6675
211.9856 173.1113
212.4677 167.7178
212.9498 162.3845
213.4319 157.4988
213.9140 153.0427
214.3962 148.6498
214.8783 146.1891
215.3604 146.3604
215.8425 148.5211
216.3246 149.7872
216.8067 149.2848
217.2889 149.5808
217.7710 152.1313
218.2531 156.9692
218.7352 164.0784
219.2173 174.1248
219.6994 186.5475
220.1816 198.0853
220.6637 208.4713
221.1458 218.7061
221.6279 228.8105
222.1100 237.5568
222.5921 249.7637
223.0743 266.8950
223.5564 287.8118
224.0385 308.0616
224.5206 326.4966
225.0027 345.3816
225.4848 366.0897
225.9670 388.8317
226.4491 412.7091
226.9312 438.6992
227.4133 465.8933
227.8954 491.5608
228.3775 516.3184
228.8597 537.9696
229.3418 554.9661
229.8239 567.1907
230.3060 575.1371
230.7881 579.4427
231.2702 579.5175
231.7524 572.1416
232.2345 555.8650
232.7166 534.3517
233.1987 509.4155
233.6808 479.5326
234.1629 449.5402
234.6451 418.9353
235.1272 388.2520
235.6093 358.2228
236.0914 328.1246
236.5735 301.3646
237.0556 279.8779
237.5378 264.4055
238.0199 252.8600
238.5020 246.2352
238.9841 243.4838
239.4662 240.3942
239.9483 235.9105
240.4305 232.5992
240.9126 231.6866
241.3947 233.3673
241.8768 237.0863
242.3589 242.9906
242.8410 250.8688
243.3232 260.7439
243.8053 273.5400
244.2874 286.9965
244.7695 299.7418
245.2516 311.0952
245.7337 323.3523
246.2159 336.6005
246.6980 350.8074
247.1801 365.6854
247.6622 381.7222
248.1443 397.8563
248.6264 413.4355
249.1086 428.4713
249.5907 443.2444
250.0728 458.3911
250.5549 473.1189
251.0370 485.3407
251.5191 495.0105
252.0013 502.3400
252.4834 507.4631
252.9655 510.1616
253.4476 511.1090
253.9297 509.7925
254.4118 506.9884
254.8940 504.5476
255.3761 503.2935
255.8582 500.9192
256.3403 496.2867
256.8224 488.7080
257.3046 481.1309
257.7867 473.7988
258.2688 466.3322
258.7509 457.7664
259.2330 447.1954
259.7151 437.4852
260.1973 429.7644
260.6794 424.4940
261.1615 419.8738
261.6436 416.5166
262.1257 413.3541
262.6078 408.2456
263.0900 400.1216
263.5721 392.8180
264.0542 387.9817
264.5363 386.0195
265.0184 383.5356
265.5005 380.0146
265.9827 376.5858
266.4648 374.7051
266.9469 374.3893
267.4290 375.6685
267.9111 378.8135
268.3932 383.9004
268.8754 389.1560
269.3575 394.3785
269.8396 400.0005
270.3217 406.3573
270.8038 413.2535
271.2859 421.4514
271.7681 431.4501
272.2502 443.1073
272.7323 454.3533
273.2144 465.2008
273.6965 475.1948
274.1786 483.8081
274.6608 491.1008
275.1429 497.3350
275.6250 503.5918
276.1071 509.1550
276.5892 508.4122
277.0714 501.0322
277.5535 488.3247
278.0356 470.8979
278.5177 448.5349
278.9998 423.5110
279.4819 395.7069
279.9641 365.6150
280.4462 336.3020
280.9283 307.5914
281.4104 280.0161
281.8925 253.4117
282.3746 227.7684
282.8568 204.1602
283.3389 182.6057
283.8210 163.3651
284.3031 147.7737
284.7852 136.1361
285.2673 126.0281
285.7495 115.2903
286.2316 104.0894
286.7137 94.97058
287.1958 88.57874
287.6779 83.97241
288.1600 79.45972
288.6422 75.03369
289.1243 70.45349
289.6064 65.30640
290.0885 59.76746
290.5706 55.12695
291.0527 51.51575
291.5349 48.79529
292.0170 47.15820
292.4991 46.47241
292.9812 45.66467
293.4633 44.46216
293.9454 42.77307
294.4276 39.79016
294.9097 35.12927
295.3918 30.83533
295.8739 29.85974
296.3560 31.66809
296.8381 33.67346
297.3203 35.04834
297.8024 35.76648
298.2845 35.50928
298.7666 34.24084
299.2487 32.91541
299.7308 31.96313
300.2130 31.62341
300.6951 32.57849
301.1772 35.63135
301.6593 39.94788
302.1414 44.72058
302.6235 49.88977
303.1057 54.63440
303.5878 57.30457
304.0699 59.12695
304.5520 62.39380
305.0341 68.69458
305.5162 75.96448
305.9984 81.82532
306.4805 86.49915
306.9626 91.83862
307.4447 99.54871
307.9268 108.5074
308.4089 117.1788
308.8911 125.1396
309.3732 132.7697
309.8553 139.8171
310.3374 146.6088
310.8195 154.4215
311.3016 164.3574
311.7838 175.3250
312.2659 186.6807
312.7480 198.7023
313.2301 209.9683
313.7122 219.0072
314.1943 226.7877
314.6765 235.1694
315.1586 245.4110
315.6407 256.2018
316.1228 267.0999
316.6049 278.2433
317.0870 288.4287
317.5692 297.0823
318.0513 304.4080
318.5334 310.6277
319.0155 314.1932
319.4976 318.0718
319.9797 324.3102
320.4619 333.3820
320.9440 340.4208
321.4261 343.2959
321.9082 343.6968
322.3903 343.1941
322.8724 345.0729
323.3546 343.0850
323.8367 334.5317
324.3188 319.5920
324.8009 303.9406
325.2830 289.5415
325.7651 274.2461
326.2473 256.7091
326.7294 234.7828
327.2115 213.0144
327.6936 190.8268
328.1757 168.9296
328.6578 149.7393
329.1400 134.8280
329.6221 121.3228
330.1042 107.8712
330.5863 93.74536
331.0684 80.96411
331.5505 69.13623
332.0327 58.64160
332.5148 50.89075
332.9969 47.73303
333.4790 44.87122
333.9611 40.45764
334.4432 33.52527
334.9254 28.82141
335.4075 27.50684
335.8896 27.52026
336.3717 25.83813
336.8538 21.63049
337.3359 17.37280
337.8180 13.69019
338.3001 10.63904
338.7823 8.404663
339.2644 7.378540
339.7465 6.608276
340.2286 5.179932
340.7107 3.066650
341.1928 0.3826900
341.6750 3.027832
342.1571 6.845215
342.6392 9.569946
343.1213 11.11035
343.6034 12.15833
344.0855 13.08459
344.5677 13.88538
345.0498 15.04382
345.5319 16.84521
346.0140 18.62158
346.4961 18.73328
346.9782 17.25208
347.4604 16.00500
347.9425 16.80493
348.4246 18.80286
348.9067 18.46155
349.3888 15.24121
349.8709 11.44141
350.3531 9.907959
350.8352 10.19080
351.3173 10.60693
351.7994 10.44080
352.2815 9.973389
352.7636 10.06616
353.2458 10.72705
353.7279 10.47620
354.2100 7.079346
354.6921 2.073242
355.1742 1.889648
355.6563 3.843018
356.1385 4.607300
356.6206 4.322998
357.1027 3.266724
357.5848 2.850952
358.0669 4.561523
358.5490 6.986206
359.0312 8.596069
359.5133 8.483154
359.9954 8.976685
360.4775 12.39868
360.9596 17.43457
361.4417 21.24268
361.9239 21.48206
362.4060 21.15649
362.8881 21.85815
363.3702 23.85498
363.8523 26.36768
364.3344 29.79126
364.8166 33.37500
365.2987 36.27466
365.7808 37.21338
366.2629 38.47278
366.7450 40.75427
367.2271 44.06348
367.7093 47.43970
368.1914 50.34546
368.6735 53.53418
369.1556 57.53577
369.6377 63.71179
370.1198 68.87671
370.6020 72.51733
371.0841 74.98853
371.5662 77.60645
372.0483 80.54199
372.5304 83.36218
373.0125 86.00769
373.4947 88.81702
373.9768 90.32678
374.4589 90.06116
374.9410 88.88708
375.4231 88.36035
375.9052 89.02307
376.3874 88.87769
376.8695 87.48901
377.3516 84.85339
377.8337 80.67273
378.3158 74.57678
378.7979 67.85596
379.2801 61.69739
379.7622 56.04492
380.2443 50.89917
380.7264 46.37061
381.2085 42.22571
381.6906 37.20264
382.1728 31.21240
382.6549 26.17395
383.1370 24.14539
383.6191 24.34326
384.1012 23.81323
384.5833 22.17017
385.0655 19.90234
385.5476 17.26257
386.0297 14.42322
386.5118 12.20325
386.9939 11.75366
387.4760 11.82947
387.9582 10.15234
388.4403 6.650146
388.9224 3.709473
389.4045 3.965820
389.8866 5.857788
390.3687 7.172241
390.8509 6.868408
391.3330 6.132568
391.8151 5.815308
392.2972 5.798340
392.7793 5.565796
393.2614 3.996582
393.7436 2.670044
394.2257 2.840698
394.7078 5.335388
395.1899 7.827515
395.6720 9.718567
396.1541 11.03223
396.6363 11.81476
397.1184 10.96344
397.6005 10.60211
398.0826 11.51648
398.5647 13.85602
399.0468 16.51544
399.5290 20.24689
400.0111 23.53687
400.4932 25.24823
400.9753 24.00067
401.4574 23.18390
401.9395 23.03601
402.4217 23.54504
402.9038 24.68536
403.3859 26.80786
403.8680 28.96729
404.3501 30.94458
404.8322 33.01746
405.3144 34.16333
405.7965 33.92114
406.2786 32.94385
406.7607 32.33984
407.2428 32.19629
407.7249 33.12439
408.2071 35.58899
408.6892 39.13074
409.1713 41.30823
409.6534 42.02673
410.1355 42.19238
410.6176 42.46851
411.0998 42.80237
411.5819 43.10547
412.0640 43.45239
412.5461 44.16382
413.0282 45.73364
413.5103 47.89636
413.9925 49.87891
414.4746 51.03577
414.9567 51.76831
415.4388 52.90662
415.9209 54.67834
416.4030 56.17371
416.8852 56.55823
417.3673 56.16650
417.8494 55.55579
418.3315 54.52490
418.8136 53.70312
419.2957 53.89319
419.7779 54.87830
420.2600 55.18127
420.7421 53.45728
421.2242 51.22046
421.7063 49.66956
422.1884 49.52466
422.6706 49.08789
423.1527 48.00024
423.6348 46.33862
424.1169 44.24915
424.5990 41.84888
425.0811 38.88452
425.5633 35.10559
426.0454 30.36267
426.5275 25.74207
427.0096 20.64465
427.4917 16.05737
427.9738 12.73242
428.4560 10.67371
428.9381 9.977295
429.4202 11.47522
429.9023 14.16931
430.3844 14.48071
430.8665 11.73364
431.3487 8.510864
431.8308 6.060547
432.3129 4.431641
432.7950 2.875000
433.2771 1.407837
433.7592 2.4400000E-04
434.2414 1.529907
434.7235 3.136841
435.2056 4.368896
435.6877 5.255127
436.1698 5.544861
436.6519 4.022095
437.1341 0.8215330
437.6162 1.576538
438.0983 0.2291260
438.5804 2.870483
439.0625 4.197021
439.5446 2.923462
440.0268 0.6496580
440.5089 1.798584
440.9910 4.184814
441.4731 5.996704
441.9552 6.632324
442.4373 6.918823
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443.4016 6.412720
443.8837 7.483765
444.3658 12.84607
444.8479 18.84924
445.3300 22.52332
445.8122 21.31201
446.2943 20.17773
446.7764 19.79150
447.2585 20.20166
447.7406 21.25330
448.2227 23.39526
448.7049 25.60706
449.1870 27.80176
449.6691 30.13892
450.1512 31.35278
450.6333 30.12195
451.1154 29.12878
451.5976 31.63013
452.0797 39.45740
452.5618 44.85352
453.0439 45.71741
453.5260 43.78918
454.0081 44.87512
454.4903 49.42017
454.9724 54.02258
455.4545 56.26001
455.9366 56.66785
456.4187 59.28662
456.9008 64.42285
457.3830 70.53992
457.8651 75.45972
458.3472 79.73108
458.8293 85.09973
459.3114 93.41736
459.7935 101.8081
460.2757 105.7096
460.7578 106.0167
461.2399 107.4144
461.7220 114.0237
462.2041 122.4215
462.6862 129.1970
463.1684 133.5249
463.6505 137.7386
464.1326 142.7996
464.6147 148.4778
465.0968 154.5685
465.5789 160.8946
466.0611 167.6139
466.5432 175.0645
467.0253 183.1525
467.5074 191.0120
467.9895 197.5099
468.4716 204.6345
468.9538 213.4797
469.4359 225.4399
469.9180 235.8072
470.4001 244.1722
470.8822 251.2972
471.3643 258.1148
471.8465 264.1250
472.3286 271.3705
472.8107 281.1708
473.2928 292.6230
473.7749 300.8660
474.2570 305.3792
474.7392 309.1177
475.2213 314.4906
475.7034 321.1657
476.1855 327.0323
476.6676 332.0090
477.1497 335.7229
477.6319 337.2262
478.1140 336.9526
478.5961 336.2484
479.0782 335.3617
479.5603 334.5693
480.0424 334.8911
480.5246 336.0304
481.0067 335.6429
481.4888 331.7590
481.9709 325.9744
482.4530 319.4662
482.9352 311.9394
483.4173 304.9858
483.8994 299.7748
484.3815 295.3710
484.8636 290.4135
485.3457 284.4155
485.8279 278.0259
486.3100 271.1184
486.7921 263.6895
487.2742 257.0389
487.7563 251.1346
488.2384 246.0018
488.7206 241.7502
489.2027 238.6163
489.6848 235.9469
490.1669 234.1541
490.6490 232.3948
491.1311 228.9299
491.6133 223.4631
492.0954 218.6227
492.5775 215.5770
493.0596 213.6539
493.5417 210.3740
494.0238 205.7514
494.5060 200.3264
494.9881 194.4188
495.4702 187.9605
495.9523 180.9014
496.4344 173.3524
496.9165 164.5414
497.3987 152.5880
497.8808 138.9436
498.3629 126.5486
498.8450 117.0980
499.3271 108.8749
499.8092 101.1639
500.2914 93.83856
500.7735 86.88745
501.2556 80.19379
501.7377 73.79993
502.2198 67.67438
502.7019 61.47821
503.1841 56.22864
503.6662 53.11023
504.1483 50.73248
504.6304 47.32471
505.1125 41.79858
505.5946 36.54712
506.0768 31.71893
506.5589 27.64966
507.0410 25.22559
507.5231 24.67365
508.0052 24.51917
508.4873 24.10156
508.9695 23.46539
509.4516 22.88513
509.9337 22.41327
510.4158 22.11780
510.8979 21.92310
511.3800 21.79419
511.8622 21.96130
512.3443 22.73187
512.8264 23.34961
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1303.016 0.0000000E+00
