#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-05-24 15:34:58 +0300 (Thu, 24 May 2018) $
#$Revision: 744 $
#$URL: svn://172.16.1.111/rod/cif/1/00/02/1000248.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000248
loop_
_publ_author_name
'Ercit, T. S.'
_publ_section_title
;
 Caryinite revisited Locality: Langban, Sweden
;
_journal_name_full               'Mineralogical Magazine'
_journal_page_first              721
_journal_page_last               727
_journal_paper_doi               10.1180/minmag.1993.057.389.16
_journal_volume                  57
_journal_year                    1993
_chemical_compound_source        R060663
_chemical_formula_sum
'As2.892 Ca1.91 Mg0.56 Mn1.77 Na1.376 O12 P0.09 Pb0.384 V0.018'
_chemical_name_mineral           Caryinite
_space_group_IT_number           15
_symmetry_space_group_name_Hall  '-I 2ya'
_symmetry_space_group_name_H-M   'I 1 2/a 1'
_cell_angle_alpha                90
_cell_angle_beta                 98.97
_cell_angle_gamma                90
_cell_length_a                   6.855
_cell_length_b                   13.147
_cell_length_c                   11.479
_cell_volume                     1021.866
_exptl_crystal_density_diffrn    4.621
_cod_original_formula_sum
'Ca1.91 Na1.376 Pb.384 Mn1.77 Mg.56 (As2.892 P.09 V.018) O12'
_cod_database_code               9009485
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 15
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R060663.rod
_rod_data_source.block           3500000
_rod_database.code               1000248
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9009485 COD http://www.crystallography.net/cod/9009485.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
129.719 0.000
130.201 4.528
130.683 16.611
131.165 36.678
131.648 56.709
132.130 66.264
132.612 66.271
133.094 67.660
133.576 74.250
134.058 85.843
134.540 100.881
135.022 120.302
135.504 141.346
135.986 159.917
136.469 176.062
136.951 188.859
137.433 194.906
137.915 192.456
138.397 200.315
138.879 224.020
139.361 256.504
139.843 275.075
140.326 275.231
140.808 272.088
141.290 276.169
141.772 290.786
142.254 302.700
142.736 309.398
143.218 311.434
143.700 315.150
144.182 321.231
144.665 328.205
145.147 334.229
145.629 336.445
146.111 342.384
146.593 355.514
147.075 378.603
147.557 393.296
148.039 395.025
148.521 390.193
149.004 387.301
149.486 391.111
149.968 392.108
150.450 386.793
150.932 369.577
151.414 358.356
151.896 357.409
152.378 362.447
152.861 364.818
153.343 364.669
153.825 361.550
154.307 354.862
154.789 336.899
155.271 325.962
155.753 331.671
156.235 348.432
156.717 355.294
157.200 336.415
157.682 313.386
158.164 299.455
158.646 310.149
159.128 317.641
159.610 310.651
160.092 290.669
160.574 275.962
161.057 276.926
161.539 284.300
162.021 289.458
162.503 288.119
162.985 285.116
163.467 282.653
163.949 280.881
164.431 278.287
164.913 271.384
165.396 263.776
165.878 260.390
166.360 270.701
166.842 281.131
167.324 281.852
167.806 270.783
168.288 256.079
168.770 234.559
169.253 212.862
169.735 204.814
170.217 235.635
170.699 275.105
171.181 291.947
171.663 275.322
172.145 250.340
172.627 236.104
173.109 230.810
173.592 227.853
174.074 223.922
174.556 219.692
175.038 215.735
175.520 210.762
176.002 208.035
176.484 214.718
176.966 229.150
177.449 240.262
177.931 235.010
178.413 220.582
178.895 212.200
179.377 218.234
179.859 229.684
180.341 230.918
180.823 222.050
181.305 213.422
181.788 215.806
182.270 226.383
182.752 236.151
183.234 241.873
183.716 244.533
184.198 246.139
184.680 246.706
185.162 245.939
185.645 242.741
186.127 237.523
186.609 232.678
187.091 228.314
187.573 224.839
188.055 225.480
188.537 231.179
189.019 237.863
189.501 239.351
189.984 235.922
190.466 232.943
190.948 235.069
191.430 241.062
191.912 240.700
192.394 232.042
192.876 219.924
193.358 212.586
193.840 210.166
194.323 209.789
194.805 211.499
195.287 215.094
195.769 213.970
196.251 206.047
196.733 194.811
197.215 188.288
197.697 186.595
198.180 188.582
198.662 195.276
199.144 207.186
199.626 215.603
200.108 218.900
200.590 218.267
201.072 216.043
201.554 210.675
202.036 209.312
202.519 221.359
203.001 249.824
203.483 268.228
203.965 269.835
204.447 257.537
204.929 247.469
205.411 238.875
205.893 234.167
206.376 237.410
206.858 251.014
207.340 261.073
207.822 264.712
208.304 262.197
208.786 255.896
209.268 243.608
209.750 231.678
210.232 227.351
210.714 232.454
211.197 239.396
211.679 248.360
212.161 259.548
212.643 260.990
213.125 248.438
213.607 231.935
214.089 223.055
214.572 222.885
215.054 227.891
215.536 240.382
216.018 262.632
216.500 269.300
216.982 254.051
217.464 229.208
217.946 210.581
218.428 196.900
218.911 192.787
219.393 204.235
219.875 237.581
220.357 252.215
220.839 240.631
221.321 215.593
221.803 197.616
222.285 188.452
222.767 183.525
223.250 182.958
223.732 190.149
224.214 189.331
224.696 177.042
225.178 158.680
225.660 143.330
226.142 128.478
226.624 121.263
227.107 127.035
227.589 155.200
228.071 170.502
228.553 168.448
229.035 154.905
229.517 144.567
229.999 139.819
230.481 134.320
230.963 123.861
231.445 100.364
231.928 90.780
232.410 101.711
232.892 125.319
233.374 138.334
233.856 135.623
234.338 130.102
234.820 123.689
235.303 98.355
235.785 89.358
236.267 96.618
236.749 99.930
237.231 99.507
237.713 84.164
238.195 88.086
238.677 84.306
239.159 80.190
239.641 86.821
240.124 80.811
240.606 70.449
241.088 57.796
241.570 36.247
242.052 21.349
242.534 23.763
243.016 56.669
243.498 79.224
243.981 87.094
244.463 82.618
244.945 75.965
245.427 65.211
245.909 54.636
246.391 45.890
246.873 36.179
247.355 34.703
247.837 46.342
248.320 67.462
248.802 78.687
249.284 73.887
249.766 67.265
250.248 68.883
250.730 87.787
251.212 94.268
251.694 80.700
252.176 52.043
252.659 33.633
253.141 29.830
253.623 30.333
254.105 28.679
254.587 23.705
255.069 19.603
255.551 17.272
256.033 16.236
256.516 13.263
256.998 5.777
257.480 0.105
257.962 1.328
258.444 13.308
258.926 22.463
259.408 29.006
259.890 31.863
260.372 22.987
260.855 6.107
261.337 33.350
261.819 42.064
262.301 24.551
262.783 11.526
263.265 7.851
263.747 11.237
264.229 9.389
264.711 0.317
265.194 10.300
265.676 15.662
266.158 16.203
266.640 12.282
267.122 2.225
267.604 12.134
268.086 22.662
268.569 29.605
269.051 32.292
269.533 28.663
270.015 16.415
270.497 8.139
270.979 5.769
271.461 8.191
271.943 11.406
272.425 15.415
272.908 20.107
273.390 26.309
273.872 34.744
274.354 39.514
274.836 39.442
275.318 35.522
275.800 29.612
276.282 20.205
276.764 14.357
277.247 19.945
277.729 38.937
278.211 49.279
278.693 46.576
279.175 35.399
279.657 27.875
280.139 24.193
280.621 23.299
281.103 26.315
281.586 33.354
282.068 35.923
282.550 32.084
283.032 24.410
283.514 18.101
283.996 13.028
284.478 10.485
284.960 13.738
285.443 22.133
285.925 24.156
286.407 17.205
286.889 5.732
287.371 2.727
287.853 8.197
288.335 10.222
288.817 4.562
289.299 6.508
289.782 7.070
290.264 7.257
290.746 26.117
291.228 31.383
291.710 23.818
292.192 14.915
292.674 10.445
293.156 9.949
293.638 13.433
294.121 22.453
294.603 30.737
295.085 26.071
295.567 10.940
296.049 0.271
296.531 5.971
297.013 21.934
297.496 34.415
297.978 42.031
298.460 46.962
298.942 52.890
299.424 58.538
299.906 59.182
300.388 45.161
300.870 26.473
301.352 22.321
301.835 35.570
302.317 50.450
302.799 47.827
303.281 34.594
303.763 27.513
304.245 43.993
304.727 66.459
305.209 70.754
305.691 54.552
306.174 38.249
306.656 39.423
307.138 51.689
307.620 63.604
308.102 72.205
308.584 77.454
309.066 78.444
309.548 75.225
310.030 71.265
310.513 65.246
310.995 60.792
311.477 62.673
311.959 80.178
312.441 98.684
312.923 101.530
313.405 90.436
313.887 96.198
314.370 145.715
314.852 215.282
315.334 281.529
315.816 344.100
316.298 395.298
316.780 428.769
317.262 446.245
317.744 461.258
318.226 438.521
318.709 446.116
319.191 446.228
319.673 439.329
320.155 404.639
320.637 405.990
321.119 392.937
321.601 379.279
322.083 385.708
322.565 355.184
323.048 361.350
323.530 352.878
324.012 351.108
324.494 331.831
324.976 320.567
325.458 324.917
325.940 327.110
326.422 329.834
326.905 335.139
327.387 351.708
327.869 356.157
328.351 337.167
328.833 307.000
329.315 289.124
329.797 291.156
330.279 297.539
330.762 304.942
331.244 316.117
331.726 319.972
332.208 313.367
332.690 301.245
333.172 290.352
333.654 278.784
334.136 272.145
334.618 274.652
335.100 288.458
335.583 289.978
336.065 273.033
336.547 251.146
337.029 239.489
337.511 240.463
337.993 244.609
338.475 250.792
338.957 258.583
339.440 263.148
339.922 263.032
340.404 263.177
340.886 270.046
341.368 284.793
341.850 293.750
342.332 291.292
342.814 282.204
343.297 283.127
343.779 294.636
344.261 312.771
344.743 339.140
345.225 372.296
345.707 395.673
346.189 403.539
346.671 405.841
347.153 422.029
347.635 451.700
348.118 486.082
348.600 521.185
349.082 556.765
349.564 593.200
350.046 631.797
350.528 668.452
351.010 693.363
351.492 710.708
351.975 736.783
352.457 787.870
352.939 850.097
353.421 895.624
353.903 918.673
354.385 958.564
354.867 986.811
355.349 1036.336
355.832 1080.702
356.314 1120.183
356.796 1140.144
357.278 1185.330
357.760 1220.409
358.242 1255.077
358.724 1298.253
359.206 1325.570
359.688 1357.365
360.171 1395.196
360.653 1430.389
361.135 1461.661
361.617 1488.151
362.099 1503.580
362.581 1495.287
363.063 1481.440
363.545 1474.313
364.027 1476.081
364.510 1485.073
364.992 1511.793
365.474 1547.020
365.956 1563.761
366.438 1539.319
366.920 1509.522
367.402 1487.349
367.884 1466.882
368.366 1467.615
368.849 1512.276
369.331 1574.635
369.813 1610.103
370.295 1598.355
370.777 1584.070
371.259 1577.169
371.741 1577.312
372.224 1587.393
372.706 1611.880
373.188 1642.468
373.670 1669.073
374.152 1688.421
374.634 1711.754
375.116 1743.575
375.598 1782.463
376.080 1811.613
376.562 1829.042
377.045 1840.644
377.527 1850.188
378.009 1857.629
378.491 1865.156
378.973 1874.770
379.455 1883.408
379.937 1882.244
380.419 1871.036
380.902 1854.183
381.384 1829.197
381.866 1799.016
382.348 1782.340
382.830 1783.767
383.312 1790.464
383.794 1785.283
384.276 1769.382
384.759 1748.247
385.241 1721.254
385.723 1691.541
386.205 1665.547
386.687 1643.376
387.169 1623.769
387.651 1603.931
388.133 1586.178
388.615 1574.650
389.098 1578.885
389.580 1584.239
390.062 1575.940
390.544 1555.685
391.026 1536.566
391.508 1521.026
391.990 1512.798
392.472 1515.813
392.954 1536.361
393.437 1561.002
393.919 1583.630
394.401 1605.735
394.883 1632.352
395.365 1674.852
395.847 1714.631
396.329 1740.501
396.811 1743.776
397.293 1752.598
397.776 1774.451
398.258 1803.516
398.740 1831.536
399.222 1859.393
399.704 1884.446
400.186 1905.237
400.668 1921.176
401.151 1938.801
401.633 1964.325
402.115 1986.078
402.597 1991.462
403.079 1965.703
403.561 1958.239
404.043 1985.079
404.525 2035.688
405.007 2056.742
405.490 2039.882
405.972 2014.839
406.454 2002.766
406.936 2005.753
407.418 1990.635
407.900 1950.392
408.382 1899.403
408.864 1863.779
409.346 1843.516
409.828 1822.011
410.311 1791.353
410.793 1753.410
411.275 1711.638
411.757 1665.047
412.239 1622.703
412.721 1598.660
413.203 1586.255
413.685 1566.994
414.168 1532.385
414.650 1490.103
415.132 1448.430
415.614 1407.045
416.096 1366.610
416.578 1327.085
417.060 1288.263
417.542 1250.492
418.025 1214.463
418.507 1178.113
418.989 1138.000
419.471 1096.709
419.953 1058.552
420.435 1031.994
420.917 1003.958
421.399 966.477
421.881 916.804
422.364 870.672
422.846 834.761
423.328 802.698
423.810 768.734
424.292 728.700
424.774 690.180
425.256 652.324
425.738 615.354
426.220 587.432
426.703 571.360
427.185 560.912
427.667 553.679
428.149 552.617
428.631 546.837
429.113 533.259
429.595 516.386
430.077 506.306
430.560 504.015
431.042 504.280
431.524 507.095
432.006 512.088
432.488 507.947
432.970 492.591
433.452 476.301
433.934 470.943
434.417 475.558
434.899 481.362
435.381 485.197
435.863 489.641
436.345 501.118
436.827 518.891
437.309 536.161
437.791 545.703
438.273 552.253
438.755 564.201
439.238 584.909
439.720 603.991
440.202 606.021
440.684 600.489
441.166 606.049
441.648 641.541
442.130 682.342
442.612 712.269
443.095 730.178
443.577 751.304
444.059 785.682
444.541 823.615
445.023 856.999
445.505 881.189
445.987 904.293
446.469 925.257
446.952 945.630
447.434 971.555
447.916 1010.508
448.398 1047.791
448.880 1076.574
449.362 1092.624
449.844 1114.496
450.326 1146.699
450.808 1180.406
451.290 1202.129
451.773 1207.759
452.255 1214.909
452.737 1227.895
453.219 1246.049
453.701 1269.270
454.183 1299.463
454.665 1323.415
455.147 1327.424
455.630 1314.326
456.112 1302.596
456.594 1294.648
457.076 1289.642
457.558 1291.688
458.040 1297.572
458.522 1293.580
459.004 1262.783
459.487 1222.791
459.969 1196.993
460.451 1186.789
460.933 1178.038
461.415 1164.638
461.897 1145.856
462.379 1120.452
462.861 1084.778
463.343 1046.272
463.826 1003.715
464.308 960.374
464.790 926.579
465.272 921.793
465.754 914.793
466.236 887.458
466.718 824.508
467.200 776.867
467.682 757.229
468.165 750.348
468.647 739.083
469.129 721.729
469.611 702.623
470.093 682.442
470.575 661.154
471.057 637.338
471.539 610.289
472.022 582.501
472.504 553.923
472.986 523.993
473.468 502.594
473.950 492.549
474.432 487.197
474.914 476.867
475.396 461.802
475.878 444.125
476.361 423.021
476.843 400.461
477.325 379.373
477.807 359.836
478.289 345.790
478.771 345.904
479.253 351.900
479.735 351.605
480.217 340.264
480.700 325.413
481.182 308.738
481.664 292.405
482.146 281.462
482.628 282.780
483.110 285.973
483.592 286.470
484.074 283.736
484.556 278.758
485.039 268.491
485.521 257.707
486.003 250.495
486.485 250.713
486.967 249.222
487.449 245.420
487.931 239.509
488.414 231.421
488.896 218.818
489.378 209.198
489.860 207.054
490.342 213.240
490.824 217.729
491.306 222.572
491.788 220.332
492.270 194.033
492.753 146.817
493.235 116.505
493.717 118.189
494.199 136.646
494.681 146.073
495.163 147.534
495.645 148.718
496.127 157.938
496.609 168.359
497.092 168.844
497.574 156.906
498.056 145.646
498.538 147.930
499.020 155.166
499.502 156.182
499.984 140.102
500.466 124.181
500.948 113.634
501.431 108.414
501.913 108.611
502.395 117.964
502.877 129.679
503.359 140.615
503.841 149.990
504.323 160.706
504.805 174.862
505.288 188.572
505.770 196.663
506.252 197.257
506.734 198.016
507.216 201.556
507.698 206.274
508.180 203.017
508.662 190.298
509.145 181.314
509.627 186.740
510.109 203.918
510.591 222.466
511.073 242.541
511.555 259.224
512.037 266.989
512.519 267.109
513.001 262.364
513.484 247.753
513.966 233.830
514.448 230.287
514.930 235.705
515.412 243.252
515.894 257.280
516.376 266.900
516.858 261.893
517.341 233.090
517.823 213.127
518.305 214.669
518.787 226.771
519.269 235.578
519.751 237.649
520.233 240.073
520.715 245.151
521.197 251.817
521.680 252.850
522.162 246.393
522.644 238.262
523.126 231.154
523.608 224.977
524.090 220.485
524.572 217.394
525.054 217.037
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