#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-05-24 15:35:06 +0300 (Thu, 24 May 2018) $
#$Revision: 746 $
#$URL: svn://172.16.1.111/rod/cif/1/00/02/1000250.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000250
loop_
_publ_author_name
'Karpenko, V. Y.'
'Pautov, L. A.'
'Sokolova, E. V.'
'Hawthorne, F. C.'
'Agakhanov, A. A.'
'Dikaya, T. V.'
_publ_section_title
;
 Ankinovichite - the nickel analogue of alvanite - a new mineral from
 Kurumsak (Kazakhstan) and Kara-Chagyr (Kyrgystan) Locality: Kara-Chagyr,
 Kyrgystan Note: isostructural with alvanite
;
_journal_name_full
'Zapiski Vserossijskogo Mineralogicheskogo Obshchestva'
_journal_page_first              59
_journal_page_last               70
_journal_volume                  133
_journal_year                    2004
_chemical_compound_source        R060671
_chemical_formula_sum            'Al4 H16 Ni0.72 O20 V1.88 Zn0.28'
_chemical_name_mineral           Ankinovichite
_space_group_IT_number           14
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_cell_angle_alpha                90
_cell_angle_beta                 92.141
_cell_angle_gamma                90
_cell_length_a                   17.8098
_cell_length_b                   5.1228
_cell_length_c                   8.8665
_cell_volume                     808.380
_exptl_crystal_density_diffrn    2.467
_cod_original_formula_sum        '(Ni.72 Zn.28) Al4 V1.88 O20 H16'
_cod_database_code               9012777
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 15
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R060671.rod
_rod_data_source.block           3500000
_rod_database.code               1000250
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9012777 COD http://www.crystallography.net/cod/9012777.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
134.540 0.000
135.022 357.029
135.504 771.512
135.986 1186.775
136.469 1592.770
136.951 2013.574
137.433 2464.568
137.915 2943.166
138.397 3429.822
138.879 3933.436
139.361 4439.914
139.843 4908.789
140.326 5335.502
140.808 5745.209
141.290 6163.805
141.772 6598.840
142.254 7011.949
142.736 7397.658
143.218 7758.699
143.700 8087.621
144.182 8399.342
144.665 8662.307
145.147 8846.115
145.629 8962.379
146.111 8980.555
146.593 8892.291
147.075 8691.609
147.557 8405.383
148.039 8036.486
148.521 7582.111
149.004 7028.395
149.486 6256.010
149.968 5511.178
150.450 4846.861
150.932 4279.094
151.414 3770.506
151.896 3313.422
152.378 2917.045
152.861 2600.518
153.343 2390.863
153.825 2239.268
154.307 2127.949
154.789 2063.820
155.271 2028.131
155.753 2020.219
156.235 2040.021
156.717 2085.398
157.200 2169.947
157.682 2272.059
158.164 2378.311
158.646 2500.676
159.128 2610.807
159.610 2695.391
160.092 2755.488
160.574 2812.680
161.057 2879.943
161.539 2943.420
162.021 2990.193
162.503 2999.643
162.985 3003.154
163.467 3023.561
163.949 3063.176
164.431 3077.176
164.913 3020.789
165.396 2930.594
165.878 2856.664
166.360 2847.600
166.842 2844.598
167.324 2805.123
167.806 2720.305
168.288 2626.988
168.770 2550.582
169.253 2483.436
169.735 2408.650
170.217 2301.107
170.699 2190.945
171.181 2111.879
171.663 2079.182
172.145 2053.648
172.627 1993.336
173.109 1909.428
173.592 1838.299
174.074 1805.094
174.556 1797.400
175.038 1799.635
175.520 1813.078
176.002 1827.973
176.484 1835.336
176.966 1834.846
177.449 1825.363
177.931 1795.916
178.413 1757.070
178.895 1730.951
179.377 1730.807
179.859 1741.664
180.341 1740.043
180.823 1725.975
181.305 1708.801
181.788 1695.117
182.270 1684.752
182.752 1676.963
183.234 1673.037
183.716 1670.988
184.198 1667.562
184.680 1662.941
185.162 1654.014
185.645 1637.859
186.127 1614.496
186.609 1583.707
187.091 1538.439
187.573 1484.035
188.055 1446.932
188.537 1430.941
189.019 1417.900
189.501 1377.631
189.984 1311.340
190.466 1249.963
190.948 1219.283
191.430 1212.445
191.912 1178.004
192.394 1106.342
192.876 1016.730
193.358 935.912
193.840 864.564
194.323 795.572
194.805 719.090
195.287 636.369
195.769 580.832
196.251 561.422
196.733 563.693
197.215 548.828
197.697 513.158
198.180 485.383
198.662 486.883
199.144 519.178
199.626 556.129
200.108 594.219
200.590 635.266
201.072 681.201
201.554 729.348
202.036 792.189
202.519 881.869
203.001 1000.572
203.483 1125.406
203.965 1248.342
204.447 1373.816
204.929 1524.842
205.411 1703.371
205.893 1902.268
206.376 2118.109
206.858 2353.254
207.340 2590.342
207.822 2817.293
208.304 3037.814
208.786 3309.016
209.268 3637.879
209.750 4000.471
210.232 4371.193
210.714 4741.844
211.197 5138.822
211.679 5565.617
212.161 6022.670
212.643 6529.568
213.125 7097.654
213.607 7695.266
214.089 8289.486
214.572 8874.262
215.054 9475.920
215.536 10099.020
216.018 10748.693
216.500 11399.625
216.982 12061.135
217.464 12703.867
217.946 13293.443
218.428 13812.199
218.911 14300.703
219.393 14774.365
219.875 15233.391
220.357 15653.154
220.839 16050.939
221.321 16396.197
221.803 16656.152
222.285 16836.010
222.767 16918.221
223.250 16892.770
223.732 16750.379
224.214 16532.779
224.696 16216.570
225.178 15839.176
225.660 15456.578
226.142 15074.877
226.624 14682.840
227.107 14263.906
227.589 13757.385
228.071 13381.518
228.553 13170.016
229.035 13074.152
229.517 12975.771
229.999 12855.037
230.481 12758.152
230.963 12701.621
231.445 12677.617
231.928 12711.486
232.410 12811.287
232.892 12968.752
233.374 13155.273
233.856 13380.357
234.338 13621.637
234.820 13871.721
235.303 14127.828
235.785 14396.848
236.267 14680.451
236.749 14978.637
237.231 15287.166
237.713 15627.957
238.195 15945.094
238.677 16209.238
239.159 16408.404
239.641 16578.193
240.124 16707.043
240.606 16807.893
241.088 16947.814
241.570 17201.174
242.052 17392.977
242.534 17418.809
243.016 17208.662
243.498 16977.156
243.981 16742.492
244.463 16494.727
244.945 16188.561
245.427 15801.166
245.909 15381.221
246.391 14955.373
246.873 14541.699
247.355 14077.613
247.837 13534.777
248.320 12933.133
248.802 12377.205
249.284 11894.707
249.766 11429.510
250.248 10941.924
250.730 10409.328
251.212 9909.619
251.694 9458.920
252.176 9051.799
252.659 8632.082
253.141 8183.355
253.623 7746.969
254.105 7348.221
254.587 7013.727
255.069 6664.457
255.551 6290.182
256.033 5897.018
256.516 5496.680
256.998 5080.125
257.480 4666.039
257.962 4263.951
258.444 3862.645
258.926 3490.689
259.408 3148.035
259.890 2832.684
260.372 2544.986
260.855 2280.320
261.337 2044.525
261.819 1845.492
262.301 1692.418
262.783 1542.629
263.265 1387.088
263.747 1230.789
264.229 1092.350
264.711 976.742
265.194 871.877
265.676 770.150
266.158 671.443
266.640 582.248
267.122 507.752
267.604 443.668
268.086 371.273
268.569 284.330
269.051 202.215
269.533 139.359
270.015 99.533
270.497 64.477
270.979 35.301
271.461 9.062
271.943 28.789
272.425 83.893
272.908 133.791
273.390 162.598
273.872 168.625
274.354 159.668
274.836 127.461
275.318 84.992
275.800 82.189
276.282 129.742
276.764 179.004
277.247 189.812
277.729 156.145
278.211 148.045
278.693 178.785
279.175 235.924
279.657 287.344
280.139 333.729
280.621 372.100
281.103 400.264
281.586 418.338
282.068 428.562
282.550 429.875
283.032 425.105
283.514 422.227
283.996 421.945
284.478 415.896
284.960 398.205
285.443 368.910
285.925 332.635
286.407 288.014
286.889 239.408
287.371 197.213
287.853 161.463
288.335 122.742
288.817 82.398
289.299 37.066
289.782 37.223
290.264 145.447
290.746 273.109
291.228 401.988
291.710 531.295
292.192 651.586
292.674 752.955
293.156 839.592
293.638 918.416
294.121 983.033
294.603 1059.641
295.085 1198.363
295.567 1390.230
296.049 1579.945
296.531 1737.217
297.013 1869.826
297.496 1986.602
297.978 2081.211
298.460 2185.059
298.942 2339.961
299.424 2535.793
299.906 2735.199
300.388 2916.871
300.870 3089.270
301.352 3255.586
301.835 3412.148
302.317 3584.336
302.799 3839.281
303.281 4131.979
303.763 4361.715
304.245 4433.979
304.727 4435.406
305.209 4456.070
305.691 4499.115
306.174 4569.254
306.656 4687.613
307.138 4835.262
307.620 4978.840
308.102 5084.838
308.584 5195.736
309.066 5353.865
309.548 5563.025
310.030 5783.400
310.513 5999.977
310.995 6213.004
311.477 6419.221
311.959 6584.988
312.441 6769.629
312.923 7020.428
313.405 7335.402
313.887 7648.617
314.370 7941.971
314.852 8216.510
315.334 8474.615
315.816 8696.863
316.298 8920.713
316.780 9186.822
317.262 9482.697
317.744 9729.531
318.226 9904.854
318.709 10012.994
319.191 10055.664
319.673 10000.975
320.155 9917.693
320.637 9833.764
321.119 9739.809
321.601 9595.279
322.083 9350.797
322.565 9080.156
323.048 8823.904
323.530 8600.938
324.012 8372.975
324.494 8107.723
324.976 7829.332
325.458 7609.016
325.940 7496.408
326.422 7409.949
326.905 7313.318
327.387 7173.953
327.869 7077.121
328.351 7039.967
328.833 7044.539
329.315 7055.037
329.797 7045.416
330.279 7069.787
330.762 7151.227
331.244 7314.391
331.726 7463.645
332.208 7587.791
332.690 7705.586
333.172 7844.703
333.654 8005.027
334.136 8185.395
334.618 8393.852
335.100 8633.729
335.583 8858.318
336.065 9062.279
336.547 9257.287
337.029 9456.438
337.511 9656.367
337.993 9874.578
338.475 10128.732
338.957 10410.326
339.440 10632.086
339.922 10780.998
340.404 10900.361
340.886 11039.889
341.368 11204.502
341.850 11331.453
342.332 11408.385
342.814 11437.936
343.297 11422.363
343.779 11361.479
344.261 11262.127
344.743 11125.455
345.225 10953.402
345.707 10753.807
346.189 10519.615
346.671 10269.000
347.153 10023.133
347.635 9782.783
348.118 9545.498
348.600 9287.158
349.082 9026.904
349.564 8823.441
350.046 8685.648
350.528 8587.020
351.010 8483.344
351.492 8384.414
351.975 8326.578
352.457 8350.600
352.939 8420.625
353.421 8482.047
353.903 8528.781
354.385 8589.400
354.867 8677.877
355.349 8799.475
355.832 8963.811
356.314 9216.139
356.796 9487.529
357.278 9712.639
357.760 9891.959
358.242 10071.887
358.724 10274.707
359.206 10497.473
359.688 10736.803
360.171 11005.398
360.653 11277.465
361.135 11552.670
361.617 11827.379
362.099 12069.943
362.581 12262.961
363.063 12424.787
363.545 12569.164
364.027 12723.408
364.510 12826.621
364.992 12865.355
365.474 12842.330
365.956 12765.541
366.438 12608.924
366.920 12422.453
367.402 12229.230
367.884 12052.082
368.366 11827.598
368.849 11528.012
369.331 11183.570
369.813 10847.688
370.295 10532.002
370.777 10212.066
371.259 9874.381
371.741 9512.840
372.224 9182.137
372.706 8889.156
373.188 8619.240
373.670 8359.557
374.152 8112.428
374.634 7869.119
375.116 7632.430
375.598 7399.875
376.080 7149.303
376.562 6866.486
377.045 6603.748
377.527 6438.510
378.009 6390.170
378.491 6235.922
378.973 5908.285
379.455 5484.945
379.937 5199.338
380.419 5060.113
380.902 4925.643
381.384 4690.082
381.866 4373.158
382.348 4085.211
382.830 3839.596
383.312 3617.582
383.794 3395.529
384.276 3176.840
384.759 2973.217
385.241 2797.031
385.723 2638.014
386.205 2481.207
386.687 2324.852
387.169 2181.910
387.651 2082.381
388.133 2003.686
388.615 1903.869
389.098 1734.484
389.580 1560.539
390.062 1446.367
390.544 1383.988
391.026 1327.180
391.508 1253.574
391.990 1171.562
392.472 1087.984
392.954 1005.490
393.437 923.059
393.919 835.812
394.401 749.240
394.883 673.551
395.365 610.127
395.847 561.369
396.329 529.449
396.811 517.637
397.293 514.371
397.776 525.107
398.258 541.068
398.740 549.557
399.222 555.996
399.704 547.041
400.186 510.211
400.668 439.480
401.151 398.896
401.633 405.291
402.115 427.248
402.597 438.480
403.079 434.627
403.561 430.303
404.043 427.025
404.525 425.068
405.007 426.621
405.490 434.635
405.972 438.945
406.454 430.277
406.936 407.018
407.418 393.346
407.900 393.674
408.382 398.992
408.864 393.367
409.346 376.693
409.828 356.064
410.311 328.701
410.793 299.602
411.275 292.713
411.757 311.023
412.239 326.393
412.721 305.381
413.203 257.988
413.685 211.854
414.168 170.859
414.650 139.932
415.132 125.596
415.614 127.137
416.096 141.518
416.578 198.717
417.060 253.725
417.542 248.959
418.025 144.385
418.507 40.311
418.989 0.514
419.471 2.166
419.953 2.414
420.435 34.107
420.917 73.943
421.399 115.486
421.881 159.742
422.364 193.047
422.846 206.312
423.328 209.176
423.810 211.059
424.292 206.830
424.774 207.924
425.256 215.686
425.738 230.016
426.220 250.936
426.703 288.438
427.185 321.842
427.667 338.861
428.149 334.123
428.631 326.107
429.113 311.566
429.595 297.139
430.077 301.191
430.560 330.791
431.042 351.973
431.524 348.467
432.006 321.305
432.488 294.287
432.970 266.441
433.452 242.438
433.934 224.496
434.417 213.561
434.899 216.377
435.381 239.533
435.863 272.598
436.345 300.125
436.827 321.492
437.309 332.365
437.791 327.971
438.273 311.600
438.755 285.838
439.238 248.232
439.720 211.625
440.202 188.518
440.684 174.299
441.166 159.596
441.648 144.062
442.130 124.494
442.612 92.092
443.095 45.791
443.577 17.705
444.059 42.211
444.541 78.010
445.023 90.443
445.505 48.072
445.987 8.922
446.469 11.486
446.952 19.775
447.434 42.074
447.916 80.160
448.398 131.848
448.880 199.635
449.362 296.461
449.844 373.092
450.326 427.018
450.808 462.984
451.290 481.303
451.773 472.182
452.255 477.648
452.737 507.418
453.219 560.236
453.701 631.854
454.183 721.764
454.665 830.254
455.147 985.225
455.630 1170.965
456.112 1287.584
456.594 1309.426
457.076 1283.438
457.558 1261.619
458.040 1246.721
458.522 1249.742
459.004 1281.557
459.487 1332.250
459.969 1402.814
460.451 1493.309
460.933 1559.873
461.415 1548.291
461.897 1501.449
462.379 1469.023
462.861 1467.441
463.343 1482.971
463.826 1512.279
464.308 1554.150
464.790 1605.361
465.272 1700.074
465.754 1775.328
466.236 1800.355
466.718 1762.051
467.200 1701.311
467.682 1600.848
468.165 1488.299
468.647 1393.160
469.129 1316.943
469.611 1256.848
470.093 1216.635
470.575 1193.494
471.057 1158.135
471.539 1098.539
472.022 1053.475
472.504 1063.131
472.986 1133.758
473.468 1154.910
473.950 1103.936
474.432 1032.590
474.914 1023.881
475.396 1074.209
475.878 1144.525
476.361 1260.939
476.843 1374.432
477.325 1350.279
477.807 1194.242
478.289 1042.078
478.771 1016.369
479.253 1058.258
479.735 1081.725
480.217 1055.258
480.700 1026.705
481.182 1025.078
481.664 1045.637
482.146 1078.398
482.628 1118.098
483.110 1168.068
483.592 1233.211
484.074 1315.766
484.556 1391.967
485.039 1455.652
485.521 1509.549
486.003 1556.324
486.485 1595.107
486.967 1626.557
487.449 1634.480
487.931 1635.354
488.414 1692.781
488.896 1836.836
489.378 1977.121
489.860 2068.885
490.342 2106.240
490.824 2176.479
491.306 2283.793
491.788 2415.490
492.270 2580.752
492.753 2772.357
493.235 2910.764
493.717 2953.750
494.199 2952.719
494.681 2991.295
495.163 3066.414
495.645 3162.658
496.127 3281.301
496.609 3410.102
497.092 3525.254
497.574 3621.412
498.056 3727.303
498.538 3870.184
499.020 4031.846
499.502 4185.844
499.984 4313.180
500.466 4445.102
500.948 4614.746
501.431 4809.699
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