#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-05-24 15:35:14 +0300 (Thu, 24 May 2018) $
#$Revision: 748 $
#$URL: svn://172.16.1.111/rod/cif/1/00/02/1000252.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000252
loop_
_publ_author_name
'Atencio, D.'
'Matioli, P. A.'
'Smith, J. B.'
'Chukanov, N. V.'
'Coutinho, J. M. V.'
'Rastsvetaeva, R. K.'
'Mockel, S.'
_publ_section_title
;
 Footemineite, the Mn-analog of atencioite, from the Foote mine, Kings
 Mountain, Cleveland County, North Carolina, U.S.A., and its relationship
 with other roscherite-group minerals Locality: Foote mine, Kings
 Mountain, Cleveland County, North Carolina, USA
;
_journal_name_full               'American Mineralogist'
_journal_page_first              1
_journal_page_last               6
_journal_paper_doi               10.2138/am.2008.2469
_journal_volume                  93
_journal_year                    2008
_chemical_compound_source        R060893
_chemical_formula_sum
'Be4 Ca2 Fe0.52 H16 Li0.17 Mg0.05 Mn4.14 O34 P6'
_chemical_name_mineral           Footemineite
_space_group_IT_number           2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                73.84
_cell_angle_beta                 85.34
_cell_angle_gamma                87.44
_cell_length_a                   6.788
_cell_length_b                   9.972
_cell_length_c                   10.014
_cell_volume                     648.740
_exptl_crystal_density_diffrn    2.869
_cod_original_formula_sum        'Ca2 Mn4.14 Li.17 Mg.05 Fe.52 P6 Be4 O34 H16'
_cod_database_code               9010368
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 15
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R060893.rod
_rod_data_source.block           3500000
_rod_database.code               1000252
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9010368 COD http://www.crystallography.net/cod/9010368.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
111.9606 0.0000000E+00
112.4427 0.5073320
112.9248 1.280628
113.4069 2.288380
113.8890 3.317696
114.3712 4.235451
114.8533 4.987198
115.3354 5.577026
115.8175 6.068420
116.2996 6.372658
116.7817 6.454559
117.2639 6.322948
117.7460 6.024818
118.2281 5.678890
118.7102 5.547165
119.1923 5.643517
119.6744 5.276794
120.1566 4.869125
120.6387 4.318825
121.1208 3.528244
121.6029 2.859787
122.0850 2.241161
122.5671 1.848427
123.0493 1.569824
123.5314 1.274158
124.0135 0.9332890
124.4956 0.5798300
124.9777 0.1842990
125.4598 0.2208790
125.9420 0.5019800
126.4241 0.4706230
126.9062 0.2687720
127.3883 0.1703340
127.8704 0.2855450
128.3525 0.4592130
128.8347 0.4200820
129.3168 0.1793140
129.7989 4.9313001E-02
130.2810 3.2288000E-02
130.7631 0.1606670
131.2452 0.2287940
131.7274 4.4502001E-02
132.2095 0.2895010
132.6916 0.4981040
133.1737 0.5746610
133.6558 0.5872760
134.1379 0.5677150
134.6201 0.5181540
135.1022 0.5566640
135.5843 0.7330930
136.0664 1.033218
136.5485 1.320057
137.0306 1.564339
137.5128 1.872169
137.9949 2.399906
138.4770 3.179340
138.9591 4.040592
139.4412 4.985203
139.9233 6.021107
140.4055 6.881958
140.8876 7.517345
141.3697 8.029633
141.8518 8.615364
142.3339 9.355114
142.8160 9.977879
143.2982 10.36106
143.7803 10.41255
144.2624 10.53136
144.7445 10.88431
145.2266 11.24857
145.7087 11.07732
146.1909 10.05058
146.6730 8.898010
147.1551 7.886337
147.6372 7.051529
148.1193 6.314644
148.6014 5.715286
149.0836 5.221115
149.5657 4.694023
150.0478 3.962418
150.5299 3.346527
151.0120 2.984848
151.4941 3.120827
151.9763 3.224426
152.4584 3.308578
152.9405 3.360222
153.4226 3.322189
153.9047 3.024437
154.3868 2.742416
154.8690 2.626068
155.3511 2.938538
155.8332 3.154488
156.3153 3.128242
156.7974 2.893097
157.2795 2.723679
157.7617 2.724281
158.2438 2.788948
158.7259 2.841339
159.2080 2.865929
159.6901 2.876190
160.1722 2.882813
160.6544 2.884987
161.1365 2.858086
161.6186 2.743240
162.1007 2.615898
162.5828 2.544357
163.0649 2.589409
163.5471 2.661942
164.0292 2.674881
164.5113 2.624939
164.9934 2.710281
165.4755 3.150795
165.9576 3.753197
166.4398 4.271606
166.9219 4.511566
167.4040 4.713455
167.8861 5.017357
168.3682 5.432312
168.8503 5.934212
169.3325 6.589577
169.8146 7.325562
170.2967 7.990387
170.7788 8.515694
171.2609 8.953651
171.7430 9.342880
172.2252 9.689087
172.7073 9.984520
173.1894 10.16241
173.6715 10.28235
174.1536 10.46940
174.6357 10.83595
175.1179 11.28577
175.6000 11.67422
176.0821 11.96219
176.5642 12.31741
177.0463 12.94384
177.5284 13.78627
178.0106 14.65649
178.4927 15.49014
178.9748 16.28521
179.4569 17.00016
179.9390 17.62301
180.4211 18.22314
180.9033 18.86006
181.3854 19.54536
181.8675 20.31099
182.3496 21.37936
182.8317 22.52750
183.3138 23.27818
183.7960 23.56405
184.2781 23.51440
184.7602 23.21100
185.2423 22.66369
185.7244 22.01945
186.2065 21.36715
186.6887 20.70250
187.1708 19.95137
187.6529 19.07831
188.1350 18.14136
188.6171 17.25013
189.0992 16.40031
189.5814 15.61648
190.0635 14.85316
190.5456 14.12693
191.0277 13.66139
191.5098 13.54871
191.9919 13.59520
192.4741 13.35661
192.9562 12.81839
193.4383 12.33104
193.9204 12.19169
194.4025 12.37679
194.8846 12.45013
195.3668 12.29128
195.8489 12.07054
196.3310 12.28268
196.8131 12.98763
197.2952 13.66594
197.7773 13.89218
198.2595 13.64769
198.7416 13.59345
199.2237 13.85451
199.7058 14.31440
200.1879 14.61825
200.6700 14.72446
201.1522 14.88010
201.6343 15.32942
202.1164 16.12109
202.5985 16.70631
203.0806 16.98580
203.5627 17.03001
204.0449 17.02046
204.5270 16.92507
205.0091 16.87952
205.4912 16.99636
205.9733 17.30315
206.4554 17.60337
206.9376 17.86996
207.4197 18.11434
207.9018 18.37720
208.3839 18.63936
208.8660 18.97221
209.3481 19.43846
209.8303 20.07146
210.3124 20.69862
210.7945 21.28598
211.2766 21.85555
211.7587 22.53111
212.2408 23.35193
212.7230 24.20167
213.2051 25.04325
213.6872 25.92485
214.1693 26.61776
214.6514 27.03451
215.1335 27.24049
215.6157 27.57093
216.0978 28.18092
216.5799 28.62869
217.0620 28.60387
217.5441 27.97748
218.0262 27.23258
218.5084 26.37216
218.9905 25.41552
219.4726 24.49799
219.9547 23.58279
220.4368 22.74632
220.9189 22.05450
221.4011 21.54003
221.8832 21.07113
222.3653 20.61406
222.8474 20.19491
223.3295 19.93590
223.8116 19.95030
224.2938 19.96053
224.7759 19.75972
225.2580 19.13121
225.7401 18.79813
226.2222 18.95467
226.7043 19.46835
227.1865 19.72514
227.6686 19.62394
228.1507 19.39088
228.6328 19.14323
229.1149 18.86485
229.5970 18.60163
230.0792 18.37192
230.5613 18.15783
231.0434 17.89428
231.5255 17.53669
232.0076 17.21598
232.4897 17.04559
232.9719 17.23331
233.4540 17.08086
233.9361 16.43053
234.4182 15.42741
234.9003 14.54588
235.3824 13.72409
235.8646 13.09282
236.3467 12.76911
236.8288 12.96999
237.3109 13.03885
237.7930 12.95440
238.2751 12.68391
238.7573 12.15873
239.2394 11.21159
239.7215 10.29711
240.2036 9.603127
240.6857 9.204178
241.1678 8.861031
241.6500 8.647774
242.1321 8.476433
242.6142 8.087044
243.0963 7.285675
243.5784 6.555695
244.0605 6.134720
244.5427 6.192268
245.0248 6.115868
245.5069 5.868652
245.9890 5.502197
246.4711 5.107635
246.9532 4.573669
247.4354 4.193344
247.9175 4.131355
248.3996 4.551109
248.8817 4.747597
249.3638 4.613022
249.8459 4.318398
250.3281 4.182274
250.8102 4.274040
251.2923 4.405914
251.7744 4.511848
252.2565 4.571541
252.7386 4.696053
253.2208 4.931229
253.7029 5.197456
254.1850 5.366272
254.6671 5.387222
255.1492 5.406937
255.6313 5.466240
256.1135 5.566681
256.5956 5.694176
257.0777 5.882889
257.5598 6.060905
258.0419 6.118584
258.5240 5.999985
259.0062 5.884033
259.4883 5.830795
259.9704 5.848656
260.4525 5.803261
260.9346 5.686592
261.4167 5.517738
261.8989 5.301407
262.3810 5.001076
262.8631 4.760643
263.3452 4.633324
263.8273 4.618431
264.3094 4.568893
264.7916 4.471794
265.2737 4.363991
265.7558 4.291702
266.2379 4.283035
266.7200 4.204384
267.2021 3.947464
267.6843 3.562752
268.1664 3.601807
268.6485 4.233887
269.1306 4.935234
269.6127 5.208076
270.0948 4.930786
270.5770 4.772377
271.0591 4.886818
271.5412 5.199051
272.0233 5.355515
272.5054 5.329720
272.9875 5.207108
273.4697 4.987312
273.9518 4.622330
274.4339 4.506355
274.9160 4.806412
275.3981 5.313934
275.8802 5.350197
276.3624 4.822983
276.8445 4.183212
277.3266 3.710320
277.8087 3.416794
278.2908 3.106293
278.7729 2.749802
279.2551 2.384850
279.7372 2.144386
280.2193 2.058411
280.7014 1.896263
281.1835 1.437744
281.6656 0.6908650
282.1478 0.2401810
282.6299 0.1757510
283.1120 0.2799300
283.5941 0.1790160
284.0762 0.1376270
284.5583 0.4575120
285.0405 0.6940380
285.5226 0.8517840
286.0047 0.9664840
286.4868 1.034485
286.9689 1.072983
287.4510 1.090843
287.9332 1.090225
288.4153 1.111984
288.8974 1.193230
289.3795 1.311508
289.8616 1.380714
290.3438 1.399040
290.8259 1.382286
291.3080 1.352524
291.7901 1.306168
292.2722 1.209190
292.7543 1.003006
293.2365 0.7621920
293.7186 0.7226870
294.2007 0.8894200
294.6828 1.009140
295.1649 0.7709580
295.6470 0.2865830
296.1292 7.2273001E-02
296.6113 0.1432110
297.0934 0.1089710
297.5755 0.2530140
298.0576 0.5685960
298.5397 0.9628750
299.0219 1.468376
299.5040 2.006996
299.9861 2.355362
300.4682 2.384735
300.9503 2.382202
301.4324 2.705788
301.9146 3.304207
302.3967 3.981934
302.8788 4.765930
303.3609 5.507935
303.8430 5.880379
304.3251 5.723907
304.8073 5.639153
305.2894 6.370041
305.7715 7.622124
306.2536 8.701271
306.7357 9.091438
307.2178 9.201691
307.7000 9.398445
308.1821 9.704956
308.6642 10.13802
309.1463 10.82765
309.6284 11.62910
310.1105 12.32848
310.5927 12.79817
311.0748 13.14773
311.5569 13.44811
312.0390 13.70122
312.5211 13.90566
313.0032 13.97240
313.4854 14.02817
313.9675 14.20592
314.4496 14.69571
314.9317 15.18697
315.4138 15.56749
315.8959 15.83597
316.3781 15.99765
316.8602 16.10982
317.3423 16.08382
317.8244 15.84314
318.3065 15.25378
318.7886 14.61721
319.2708 13.95145
319.7529 13.30423
320.2350 12.80869
320.7171 12.81337
321.1992 12.75045
321.6813 12.28452
322.1635 11.11518
322.6456 10.13030
323.1277 9.559082
323.6098 9.266251
324.0919 9.025269
324.5740 9.064034
325.0562 8.910255
325.5383 8.338165
326.0204 7.190163
326.5025 6.234550
326.9846 5.657204
327.4667 5.242851
327.9489 4.755127
328.4310 3.967064
328.9131 3.359329
329.3952 3.056938
329.8773 3.068916
330.3594 3.033180
330.8416 2.933525
331.3237 2.800491
331.8058 2.636597
332.2879 2.284523
332.7700 2.188293
333.2521 2.542114
333.7343 3.204010
334.2164 3.451950
334.6985 3.047913
335.1806 2.593910
335.6627 2.427109
336.1448 2.668114
336.6270 2.812714
337.1091 2.785347
337.5912 2.700226
338.0733 2.841660
338.5554 3.308952
339.0375 3.672081
339.5197 3.666855
340.0018 3.248062
340.4839 3.177277
340.9660 3.544456
341.4481 4.076385
341.9302 4.396729
342.4124 4.490395
342.8945 4.628265
343.3766 4.984200
343.8587 5.452713
344.3408 5.489075
344.8229 5.041679
345.3051 4.518723
345.7872 4.318939
346.2693 4.392120
346.7514 4.421745
347.2335 4.358765
347.7156 4.197113
348.1978 3.861366
348.6799 3.369835
349.1620 2.916832
349.6441 2.667282
350.1262 2.555771
350.6083 2.443428
351.0905 2.329262
351.5726 2.152328
352.0547 1.760963
352.5368 1.233864
353.0189 0.8231050
353.5010 0.7165600
353.9832 0.7701110
354.4653 0.8557590
354.9474 0.9692920
355.4295 0.9645460
355.9116 0.6101910
356.3937 7.7972002E-02
356.8759 0.3649520
357.3580 0.6150280
357.8401 0.7509610
358.3222 0.8134770
358.8043 0.8040700
359.2864 0.7318950
359.7686 0.5628200
360.2507 0.3522640
360.7328 0.1519320
361.2149 1.2772000E-02
361.6970 0.1923370
362.1791 0.3960570
362.6613 0.6280670
363.1434 0.8984300
363.6255 1.166191
364.1076 1.506409
364.5897 1.972183
365.0718 2.590454
365.5540 3.221741
366.0361 3.842850
366.5182 4.463089
367.0003 5.093811
367.4824 5.815010
367.9645 6.467377
368.4467 6.934669
368.9288 7.191093
369.4109 7.717262
369.8930 8.626678
370.3751 9.721291
370.8572 10.88428
371.3394 12.15755
371.8215 13.40874
372.3036 14.62330
372.7857 15.80917
373.2678 16.97016
373.7499 17.95885
374.2321 19.20255
374.7142 20.99438
375.1963 23.57352
375.6784 25.65748
376.1605 27.00486
376.6426 28.14779
377.1248 29.91273
377.6069 32.42180
378.0890 34.91841
378.5711 37.10966
379.0532 39.06353
379.5353 41.14145
380.0175 43.38950
380.4996 45.63242
380.9817 47.69826
381.4638 49.59645
381.9459 51.54239
382.4280 53.67708
382.9102 55.71994
383.3923 56.99473
383.8744 57.56288
384.3565 57.94489
384.8386 58.70395
385.3207 59.48007
385.8029 59.44887
386.2850 58.46512
386.7671 57.01792
387.2492 55.54800
387.7313 53.99156
388.2134 52.22829
388.6956 50.14766
389.1777 47.90123
389.6598 45.58456
390.1419 43.21147
390.6240 40.80856
391.1061 38.31551
391.5883 35.81226
392.0704 33.35395
392.5525 30.79276
393.0346 28.51314
393.5167 26.81810
393.9988 25.53365
394.4810 24.14848
394.9631 22.14061
395.4452 20.25491
395.9273 18.91232
396.4094 18.32190
396.8915 17.75788
397.3737 17.07149
397.8558 16.34447
398.3379 15.67788
398.8200 14.87276
399.3021 14.35014
399.7842 14.26013
400.2664 14.59970
400.7485 14.93812
401.2306 15.31171
401.7127 15.64143
402.1948 15.85130
402.6769 15.79522
403.1591 15.94118
403.6412 16.37171
404.1233 16.99292
404.6054 17.56419
405.0875 18.01609
405.5696 18.60983
406.0518 19.53300
406.5339 20.80262
407.0160 21.84367
407.4981 22.65752
407.9802 23.21798
408.4623 23.39156
408.9445 23.18803
409.4266 23.06014
409.9087 23.18977
410.3908 23.42013
410.8729 23.35526
411.3550 23.00172
411.8372 22.57182
412.3193 22.20145
412.8014 21.86581
413.2835 21.49265
413.7656 21.05744
414.2477 20.63153
414.7299 20.27920
415.2120 19.99010
415.6941 19.75154
416.1762 19.61297
416.6583 19.48302
417.1404 19.33863
417.6226 19.17607
418.1047 18.82729
418.5868 17.87842
419.0689 16.82909
419.5510 16.18123
420.0331 16.46284
420.5153 16.62383
420.9974 16.14693
421.4795 15.23058
421.9616 14.40800
422.4437 13.97508
422.9258 13.53417
423.4080 12.87592
423.8901 11.86066
424.3722 11.03061
424.8543 10.48157
425.3364 10.10425
425.8185 9.800781
426.3007 9.564346
426.7828 9.408493
427.2649 9.293549
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