#\#CIF_2.0 #------------------------------------------------------------------------------ #$Date: 2018-05-24 15:35:14 +0300 (Thu, 24 May 2018) $ #$Revision: 748 $ #$URL: svn://172.16.1.111/rod/cif/1/00/02/1000252.rod $ #------------------------------------------------------------------------------ # # This file is available in the Raman Open Database (ROD), # http://solsa.crystallography.net/rod/ # # All data on this site have been placed in the public domain by the # contributors. # data_1000252 loop_ _publ_author_name 'Atencio, D.' 'Matioli, P. A.' 'Smith, J. B.' 'Chukanov, N. V.' 'Coutinho, J. M. V.' 'Rastsvetaeva, R. K.' 'Mockel, S.' _publ_section_title ; Footemineite, the Mn-analog of atencioite, from the Foote mine, Kings Mountain, Cleveland County, North Carolina, U.S.A., and its relationship with other roscherite-group minerals Locality: Foote mine, Kings Mountain, Cleveland County, North Carolina, USA ; _journal_name_full 'American Mineralogist' _journal_page_first 1 _journal_page_last 6 _journal_paper_doi 10.2138/am.2008.2469 _journal_volume 93 _journal_year 2008 _chemical_compound_source R060893 _chemical_formula_sum 'Be4 Ca2 Fe0.52 H16 Li0.17 Mg0.05 Mn4.14 O34 P6' _chemical_name_mineral Footemineite _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 73.84 _cell_angle_beta 85.34 _cell_angle_gamma 87.44 _cell_length_a 6.788 _cell_length_b 9.972 _cell_length_c 10.014 _cell_volume 648.740 _exptl_crystal_density_diffrn 2.869 _cod_original_formula_sum 'Ca2 Mn4.14 Li.17 Mg.05 Fe.52 P6 Be4 O34 H16' _cod_database_code 9010368 _raman_determination_method experimental _raman_measurement_device.location 'Arizona University' _raman_measurement_device.company 'Thermo Scientific' _raman_measurement_device.model 'Nicolet Almega XR' _raman_measurement_device.optics_type microscope _raman_measurement_device.microscope_system dispersive _raman_measurement_device.microscope_objective_magnification 50 _raman_measurement_device.microscope_numerical_aperture 0.5 _raman_measurement_device.excitation_laser_type other _raman_measurement_device.excitation_laser_wavelength 532 _raman_measurement_device.configuration simple _raman_measurement_device.resolution 4 _raman_measurement_device.power_on_sample 15 _raman_measurement_device.direction_polarization unoriented _raman_measurement_device.spot_size 1 _raman_measurement_device.diffraction_grating 400 _raman_measurement.environment Air _raman_measurement.environment_details ; The sample was measured in air. ; _raman_measurement.temperature 300 _raman_measurement.pressure 100 _raman_measurement.background_subtraction no _raman_measurement.background_subtraction_details ; No background subtraction method was applied. ; _raman_measurement.baseline_correction no _raman_measurement.baseline_correction_details ; No baseline correction method was applied. ; _raman_measurement.integration_time 10 _rod_data_source.file R060893.rod _rod_data_source.block 3500000 _rod_database.code 1000252 loop_ _raman_complementary.id _raman_complementary.method 1 XRD loop_ _raman_measurement_device_calibration.id _raman_measurement_device_calibration.standard 1 neon_lamp loop_ _rod_related_entry.id _rod_related_entry.code _rod_related_entry.database _rod_related_entry.uri _rod_related_entry.description 1 9010368 COD http://www.crystallography.net/cod/9010368.html ; XRD analysis data was done. ; loop_ _raman_spectrum.raman_shift _raman_spectrum.intensity 111.9606 0.0000000E+00 112.4427 0.5073320 112.9248 1.280628 113.4069 2.288380 113.8890 3.317696 114.3712 4.235451 114.8533 4.987198 115.3354 5.577026 115.8175 6.068420 116.2996 6.372658 116.7817 6.454559 117.2639 6.322948 117.7460 6.024818 118.2281 5.678890 118.7102 5.547165 119.1923 5.643517 119.6744 5.276794 120.1566 4.869125 120.6387 4.318825 121.1208 3.528244 121.6029 2.859787 122.0850 2.241161 122.5671 1.848427 123.0493 1.569824 123.5314 1.274158 124.0135 0.9332890 124.4956 0.5798300 124.9777 0.1842990 125.4598 0.2208790 125.9420 0.5019800 126.4241 0.4706230 126.9062 0.2687720 127.3883 0.1703340 127.8704 0.2855450 128.3525 0.4592130 128.8347 0.4200820 129.3168 0.1793140 129.7989 4.9313001E-02 130.2810 3.2288000E-02 130.7631 0.1606670 131.2452 0.2287940 131.7274 4.4502001E-02 132.2095 0.2895010 132.6916 0.4981040 133.1737 0.5746610 133.6558 0.5872760 134.1379 0.5677150 134.6201 0.5181540 135.1022 0.5566640 135.5843 0.7330930 136.0664 1.033218 136.5485 1.320057 137.0306 1.564339 137.5128 1.872169 137.9949 2.399906 138.4770 3.179340 138.9591 4.040592 139.4412 4.985203 139.9233 6.021107 140.4055 6.881958 140.8876 7.517345 141.3697 8.029633 141.8518 8.615364 142.3339 9.355114 142.8160 9.977879 143.2982 10.36106 143.7803 10.41255 144.2624 10.53136 144.7445 10.88431 145.2266 11.24857 145.7087 11.07732 146.1909 10.05058 146.6730 8.898010 147.1551 7.886337 147.6372 7.051529 148.1193 6.314644 148.6014 5.715286 149.0836 5.221115 149.5657 4.694023 150.0478 3.962418 150.5299 3.346527 151.0120 2.984848 151.4941 3.120827 151.9763 3.224426 152.4584 3.308578 152.9405 3.360222 153.4226 3.322189 153.9047 3.024437 154.3868 2.742416 154.8690 2.626068 155.3511 2.938538 155.8332 3.154488 156.3153 3.128242 156.7974 2.893097 157.2795 2.723679 157.7617 2.724281 158.2438 2.788948 158.7259 2.841339 159.2080 2.865929 159.6901 2.876190 160.1722 2.882813 160.6544 2.884987 161.1365 2.858086 161.6186 2.743240 162.1007 2.615898 162.5828 2.544357 163.0649 2.589409 163.5471 2.661942 164.0292 2.674881 164.5113 2.624939 164.9934 2.710281 165.4755 3.150795 165.9576 3.753197 166.4398 4.271606 166.9219 4.511566 167.4040 4.713455 167.8861 5.017357 168.3682 5.432312 168.8503 5.934212 169.3325 6.589577 169.8146 7.325562 170.2967 7.990387 170.7788 8.515694 171.2609 8.953651 171.7430 9.342880 172.2252 9.689087 172.7073 9.984520 173.1894 10.16241 173.6715 10.28235 174.1536 10.46940 174.6357 10.83595 175.1179 11.28577 175.6000 11.67422 176.0821 11.96219 176.5642 12.31741 177.0463 12.94384 177.5284 13.78627 178.0106 14.65649 178.4927 15.49014 178.9748 16.28521 179.4569 17.00016 179.9390 17.62301 180.4211 18.22314 180.9033 18.86006 181.3854 19.54536 181.8675 20.31099 182.3496 21.37936 182.8317 22.52750 183.3138 23.27818 183.7960 23.56405 184.2781 23.51440 184.7602 23.21100 185.2423 22.66369 185.7244 22.01945 186.2065 21.36715 186.6887 20.70250 187.1708 19.95137 187.6529 19.07831 188.1350 18.14136 188.6171 17.25013 189.0992 16.40031 189.5814 15.61648 190.0635 14.85316 190.5456 14.12693 191.0277 13.66139 191.5098 13.54871 191.9919 13.59520 192.4741 13.35661 192.9562 12.81839 193.4383 12.33104 193.9204 12.19169 194.4025 12.37679 194.8846 12.45013 195.3668 12.29128 195.8489 12.07054 196.3310 12.28268 196.8131 12.98763 197.2952 13.66594 197.7773 13.89218 198.2595 13.64769 198.7416 13.59345 199.2237 13.85451 199.7058 14.31440 200.1879 14.61825 200.6700 14.72446 201.1522 14.88010 201.6343 15.32942 202.1164 16.12109 202.5985 16.70631 203.0806 16.98580 203.5627 17.03001 204.0449 17.02046 204.5270 16.92507 205.0091 16.87952 205.4912 16.99636 205.9733 17.30315 206.4554 17.60337 206.9376 17.86996 207.4197 18.11434 207.9018 18.37720 208.3839 18.63936 208.8660 18.97221 209.3481 19.43846 209.8303 20.07146 210.3124 20.69862 210.7945 21.28598 211.2766 21.85555 211.7587 22.53111 212.2408 23.35193 212.7230 24.20167 213.2051 25.04325 213.6872 25.92485 214.1693 26.61776 214.6514 27.03451 215.1335 27.24049 215.6157 27.57093 216.0978 28.18092 216.5799 28.62869 217.0620 28.60387 217.5441 27.97748 218.0262 27.23258 218.5084 26.37216 218.9905 25.41552 219.4726 24.49799 219.9547 23.58279 220.4368 22.74632 220.9189 22.05450 221.4011 21.54003 221.8832 21.07113 222.3653 20.61406 222.8474 20.19491 223.3295 19.93590 223.8116 19.95030 224.2938 19.96053 224.7759 19.75972 225.2580 19.13121 225.7401 18.79813 226.2222 18.95467 226.7043 19.46835 227.1865 19.72514 227.6686 19.62394 228.1507 19.39088 228.6328 19.14323 229.1149 18.86485 229.5970 18.60163 230.0792 18.37192 230.5613 18.15783 231.0434 17.89428 231.5255 17.53669 232.0076 17.21598 232.4897 17.04559 232.9719 17.23331 233.4540 17.08086 233.9361 16.43053 234.4182 15.42741 234.9003 14.54588 235.3824 13.72409 235.8646 13.09282 236.3467 12.76911 236.8288 12.96999 237.3109 13.03885 237.7930 12.95440 238.2751 12.68391 238.7573 12.15873 239.2394 11.21159 239.7215 10.29711 240.2036 9.603127 240.6857 9.204178 241.1678 8.861031 241.6500 8.647774 242.1321 8.476433 242.6142 8.087044 243.0963 7.285675 243.5784 6.555695 244.0605 6.134720 244.5427 6.192268 245.0248 6.115868 245.5069 5.868652 245.9890 5.502197 246.4711 5.107635 246.9532 4.573669 247.4354 4.193344 247.9175 4.131355 248.3996 4.551109 248.8817 4.747597 249.3638 4.613022 249.8459 4.318398 250.3281 4.182274 250.8102 4.274040 251.2923 4.405914 251.7744 4.511848 252.2565 4.571541 252.7386 4.696053 253.2208 4.931229 253.7029 5.197456 254.1850 5.366272 254.6671 5.387222 255.1492 5.406937 255.6313 5.466240 256.1135 5.566681 256.5956 5.694176 257.0777 5.882889 257.5598 6.060905 258.0419 6.118584 258.5240 5.999985 259.0062 5.884033 259.4883 5.830795 259.9704 5.848656 260.4525 5.803261 260.9346 5.686592 261.4167 5.517738 261.8989 5.301407 262.3810 5.001076 262.8631 4.760643 263.3452 4.633324 263.8273 4.618431 264.3094 4.568893 264.7916 4.471794 265.2737 4.363991 265.7558 4.291702 266.2379 4.283035 266.7200 4.204384 267.2021 3.947464 267.6843 3.562752 268.1664 3.601807 268.6485 4.233887 269.1306 4.935234 269.6127 5.208076 270.0948 4.930786 270.5770 4.772377 271.0591 4.886818 271.5412 5.199051 272.0233 5.355515 272.5054 5.329720 272.9875 5.207108 273.4697 4.987312 273.9518 4.622330 274.4339 4.506355 274.9160 4.806412 275.3981 5.313934 275.8802 5.350197 276.3624 4.822983 276.8445 4.183212 277.3266 3.710320 277.8087 3.416794 278.2908 3.106293 278.7729 2.749802 279.2551 2.384850 279.7372 2.144386 280.2193 2.058411 280.7014 1.896263 281.1835 1.437744 281.6656 0.6908650 282.1478 0.2401810 282.6299 0.1757510 283.1120 0.2799300 283.5941 0.1790160 284.0762 0.1376270 284.5583 0.4575120 285.0405 0.6940380 285.5226 0.8517840 286.0047 0.9664840 286.4868 1.034485 286.9689 1.072983 287.4510 1.090843 287.9332 1.090225 288.4153 1.111984 288.8974 1.193230 289.3795 1.311508 289.8616 1.380714 290.3438 1.399040 290.8259 1.382286 291.3080 1.352524 291.7901 1.306168 292.2722 1.209190 292.7543 1.003006 293.2365 0.7621920 293.7186 0.7226870 294.2007 0.8894200 294.6828 1.009140 295.1649 0.7709580 295.6470 0.2865830 296.1292 7.2273001E-02 296.6113 0.1432110 297.0934 0.1089710 297.5755 0.2530140 298.0576 0.5685960 298.5397 0.9628750 299.0219 1.468376 299.5040 2.006996 299.9861 2.355362 300.4682 2.384735 300.9503 2.382202 301.4324 2.705788 301.9146 3.304207 302.3967 3.981934 302.8788 4.765930 303.3609 5.507935 303.8430 5.880379 304.3251 5.723907 304.8073 5.639153 305.2894 6.370041 305.7715 7.622124 306.2536 8.701271 306.7357 9.091438 307.2178 9.201691 307.7000 9.398445 308.1821 9.704956 308.6642 10.13802 309.1463 10.82765 309.6284 11.62910 310.1105 12.32848 310.5927 12.79817 311.0748 13.14773 311.5569 13.44811 312.0390 13.70122 312.5211 13.90566 313.0032 13.97240 313.4854 14.02817 313.9675 14.20592 314.4496 14.69571 314.9317 15.18697 315.4138 15.56749 315.8959 15.83597 316.3781 15.99765 316.8602 16.10982 317.3423 16.08382 317.8244 15.84314 318.3065 15.25378 318.7886 14.61721 319.2708 13.95145 319.7529 13.30423 320.2350 12.80869 320.7171 12.81337 321.1992 12.75045 321.6813 12.28452 322.1635 11.11518 322.6456 10.13030 323.1277 9.559082 323.6098 9.266251 324.0919 9.025269 324.5740 9.064034 325.0562 8.910255 325.5383 8.338165 326.0204 7.190163 326.5025 6.234550 326.9846 5.657204 327.4667 5.242851 327.9489 4.755127 328.4310 3.967064 328.9131 3.359329 329.3952 3.056938 329.8773 3.068916 330.3594 3.033180 330.8416 2.933525 331.3237 2.800491 331.8058 2.636597 332.2879 2.284523 332.7700 2.188293 333.2521 2.542114 333.7343 3.204010 334.2164 3.451950 334.6985 3.047913 335.1806 2.593910 335.6627 2.427109 336.1448 2.668114 336.6270 2.812714 337.1091 2.785347 337.5912 2.700226 338.0733 2.841660 338.5554 3.308952 339.0375 3.672081 339.5197 3.666855 340.0018 3.248062 340.4839 3.177277 340.9660 3.544456 341.4481 4.076385 341.9302 4.396729 342.4124 4.490395 342.8945 4.628265 343.3766 4.984200 343.8587 5.452713 344.3408 5.489075 344.8229 5.041679 345.3051 4.518723 345.7872 4.318939 346.2693 4.392120 346.7514 4.421745 347.2335 4.358765 347.7156 4.197113 348.1978 3.861366 348.6799 3.369835 349.1620 2.916832 349.6441 2.667282 350.1262 2.555771 350.6083 2.443428 351.0905 2.329262 351.5726 2.152328 352.0547 1.760963 352.5368 1.233864 353.0189 0.8231050 353.5010 0.7165600 353.9832 0.7701110 354.4653 0.8557590 354.9474 0.9692920 355.4295 0.9645460 355.9116 0.6101910 356.3937 7.7972002E-02 356.8759 0.3649520 357.3580 0.6150280 357.8401 0.7509610 358.3222 0.8134770 358.8043 0.8040700 359.2864 0.7318950 359.7686 0.5628200 360.2507 0.3522640 360.7328 0.1519320 361.2149 1.2772000E-02 361.6970 0.1923370 362.1791 0.3960570 362.6613 0.6280670 363.1434 0.8984300 363.6255 1.166191 364.1076 1.506409 364.5897 1.972183 365.0718 2.590454 365.5540 3.221741 366.0361 3.842850 366.5182 4.463089 367.0003 5.093811 367.4824 5.815010 367.9645 6.467377 368.4467 6.934669 368.9288 7.191093 369.4109 7.717262 369.8930 8.626678 370.3751 9.721291 370.8572 10.88428 371.3394 12.15755 371.8215 13.40874 372.3036 14.62330 372.7857 15.80917 373.2678 16.97016 373.7499 17.95885 374.2321 19.20255 374.7142 20.99438 375.1963 23.57352 375.6784 25.65748 376.1605 27.00486 376.6426 28.14779 377.1248 29.91273 377.6069 32.42180 378.0890 34.91841 378.5711 37.10966 379.0532 39.06353 379.5353 41.14145 380.0175 43.38950 380.4996 45.63242 380.9817 47.69826 381.4638 49.59645 381.9459 51.54239 382.4280 53.67708 382.9102 55.71994 383.3923 56.99473 383.8744 57.56288 384.3565 57.94489 384.8386 58.70395 385.3207 59.48007 385.8029 59.44887 386.2850 58.46512 386.7671 57.01792 387.2492 55.54800 387.7313 53.99156 388.2134 52.22829 388.6956 50.14766 389.1777 47.90123 389.6598 45.58456 390.1419 43.21147 390.6240 40.80856 391.1061 38.31551 391.5883 35.81226 392.0704 33.35395 392.5525 30.79276 393.0346 28.51314 393.5167 26.81810 393.9988 25.53365 394.4810 24.14848 394.9631 22.14061 395.4452 20.25491 395.9273 18.91232 396.4094 18.32190 396.8915 17.75788 397.3737 17.07149 397.8558 16.34447 398.3379 15.67788 398.8200 14.87276 399.3021 14.35014 399.7842 14.26013 400.2664 14.59970 400.7485 14.93812 401.2306 15.31171 401.7127 15.64143 402.1948 15.85130 402.6769 15.79522 403.1591 15.94118 403.6412 16.37171 404.1233 16.99292 404.6054 17.56419 405.0875 18.01609 405.5696 18.60983 406.0518 19.53300 406.5339 20.80262 407.0160 21.84367 407.4981 22.65752 407.9802 23.21798 408.4623 23.39156 408.9445 23.18803 409.4266 23.06014 409.9087 23.18977 410.3908 23.42013 410.8729 23.35526 411.3550 23.00172 411.8372 22.57182 412.3193 22.20145 412.8014 21.86581 413.2835 21.49265 413.7656 21.05744 414.2477 20.63153 414.7299 20.27920 415.2120 19.99010 415.6941 19.75154 416.1762 19.61297 416.6583 19.48302 417.1404 19.33863 417.6226 19.17607 418.1047 18.82729 418.5868 17.87842 419.0689 16.82909 419.5510 16.18123 420.0331 16.46284 420.5153 16.62383 420.9974 16.14693 421.4795 15.23058 421.9616 14.40800 422.4437 13.97508 422.9258 13.53417 423.4080 12.87592 423.8901 11.86066 424.3722 11.03061 424.8543 10.48157 425.3364 10.10425 425.8185 9.800781 426.3007 9.564346 426.7828 9.408493 427.2649 9.293549 427.7470 9.255241 428.2291 9.532684 428.7112 10.20397 429.1934 11.02364 429.6755 11.83588 430.1576 12.61664 430.6397 13.53543 431.1218 14.54527 431.6039 15.77380 432.0861 17.60255 432.5682 20.08480 433.0503 22.32215 433.5324 23.82355 434.0145 24.89314 434.4966 26.68262 434.9788 29.21192 435.4609 31.86954 435.9430 34.10303 436.4251 36.08632 436.9072 38.34838 437.3893 41.12321 437.8715 43.89082 438.3536 46.03217 438.8357 47.67868 439.3178 49.19666 439.7999 50.98300 440.2820 52.59749 440.7642 53.59253 441.2463 53.95012 441.7284 53.98717 442.2105 53.98365 442.6926 53.69779 443.1747 52.89516 443.6569 51.41269 444.1390 49.51465 444.6211 47.13974 445.1032 44.38956 445.5853 41.63460 446.0674 38.85449 446.5496 36.13969 447.0317 33.54272 447.5138 31.09837 447.9959 28.63565 448.4780 26.06323 448.9601 23.52653 449.4423 21.09405 449.9244 18.64838 450.4065 16.62070 450.8886 15.16413 451.3707 14.17547 451.8528 13.17720 452.3350 12.15955 452.8171 11.13996 453.2992 10.11030 453.7813 9.064507 454.2634 7.969910 454.7455 6.775505 455.2277 5.656219 455.7098 4.873489 456.1919 4.388832 456.6740 3.876450 457.1561 3.146614 457.6382 2.412773 458.1204 2.176056 458.6025 2.366867 459.0846 2.493988 459.5667 2.128891 460.0488 1.542084 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1.2886000E-02 1300.860 0.1196290 1301.343 0.4240190 1301.825 0.0000000E+00