#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-05-24 15:35:34 +0300 (Thu, 24 May 2018) $
#$Revision: 753 $
#$URL: svn://172.16.1.111/rod/cif/1/00/02/1000257.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000257
loop_
_publ_author_name
'Burns, P. C.'
'Roberts, A. C.'
'Stirling, J. A. R.'
'Criddle, A. J.'
'Feinglos, M. N.'
_publ_section_title
;
 Dukeite, Bi24Cr8O57(OH)6(H2O)3, a new mineral from Brejauba, Minas
 Gerais, Brazil: Description and crystal structure
;
_journal_name_full               'American Mineralogist'
_journal_page_first              1822
_journal_page_last               1827
_journal_volume                  85
_journal_year                    2000
_chemical_compound_source        R070441
_chemical_formula_sum            'Bi12 Cr4 H6 O33'
_chemical_name_mineral           Dukeite
_space_group_IT_number           159
_symmetry_space_group_name_Hall  'P 3 -2c'
_symmetry_space_group_name_H-M   'P 3 1 c'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                120
_cell_length_a                   15.067
_cell_length_b                   15.067
_cell_length_c                   15.293
_cell_volume                     3006.609
_exptl_crystal_density_diffrn    7.179
_cod_original_formula_sum        'Bi12 Cr4 O33 H6'
_cod_database_code               9002510
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 15
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R070441.rod
_rod_data_source.block           3500000
_rod_database.code               1000257
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9002510 COD http://www.crystallography.net/cod/9002510.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
140.0309 0.0000000E+00
140.5130 27.93457
140.9951 19.91260
141.4772 21.85303
141.9594 95.16895
142.4415 183.1362
142.9236 289.1973
143.4057 426.6401
143.8878 600.6279
144.3699 780.9893
144.8521 955.7808
145.3342 1113.500
145.8163 1314.889
146.2984 1580.194
146.7805 1876.885
147.2626 2141.361
147.7448 2339.935
148.2269 2552.877
148.7090 2805.130
149.1911 3118.891
149.6732 3432.278
150.1553 3742.424
150.6375 4053.962
151.1196 4376.606
151.6017 4708.568
152.0838 5058.449
152.5659 5428.539
153.0480 5825.166
153.5302 6239.999
154.0123 6670.087
154.4944 7119.298
154.9765 7590.186
155.4586 8093.077
155.9407 8605.541
156.4229 9116.956
156.9050 9523.650
157.3871 9863.818
157.8692 10246.24
158.3513 10684.00
158.8334 11061.84
159.3156 11349.61
159.7977 11564.44
160.2798 11721.97
160.7619 11836.26
161.2440 11890.97
161.7261 11894.71
162.2083 11863.76
162.6904 11721.24
163.1725 11407.85
163.6546 10965.26
164.1367 10471.25
164.6188 9931.259
165.1010 9367.863
165.5831 8790.039
166.0652 8186.592
166.5473 7593.277
167.0294 7021.170
167.5115 6474.533
167.9937 5948.049
168.4758 5445.466
168.9579 4963.913
169.4400 4501.111
169.9221 4043.831
170.4042 3619.897
170.8864 3255.920
171.3685 2949.185
171.8506 2663.146
172.3327 2371.100
172.8148 2089.596
173.2969 1842.688
173.7791 1643.442
174.2612 1478.043
174.7433 1345.477
175.2254 1244.085
175.7075 1146.172
176.1896 1020.314
176.6718 881.1216
177.1539 755.0156
177.6360 659.3589
178.1181 580.8711
178.6002 501.8218
179.0823 420.0889
179.5645 342.9126
180.0466 275.4473
180.5287 217.2939
181.0108 170.4873
181.4929 141.3398
181.9750 122.6914
182.4572 100.1133
182.9393 71.09277
183.4214 40.45215
183.9035 12.63672
184.3856 11.76562
184.8677 34.19775
185.3499 61.78857
185.8320 89.13232
186.3141 93.94531
186.7962 66.44629
187.2783 19.52393
187.7604 13.44336
188.2426 40.33887
188.7247 66.68115
189.2068 85.10059
189.6889 92.81885
190.1710 107.9331
190.6531 136.4009
191.1353 177.9971
191.6174 227.7856
192.0995 289.9141
192.5816 353.5054
193.0637 406.1138
193.5458 443.1460
194.0280 471.2334
194.5101 491.0190
194.9922 508.7441
195.4743 537.8423
195.9564 592.9395
196.4385 650.0244
196.9207 664.5146
197.4028 637.7437
197.8849 623.0464
198.3670 665.3799
198.8491 760.4146
199.3312 836.0469
199.8134 888.6890
200.2955 928.4668
200.7776 964.7373
201.2597 994.4673
201.7418 1034.216
202.2239 1094.352
202.7061 1177.073
203.1882 1254.008
203.6703 1326.183
204.1524 1390.165
204.6345 1434.798
205.1166 1454.891
205.5988 1481.030
206.0809 1532.064
206.5630 1613.268
207.0451 1679.330
207.5272 1724.354
208.0093 1757.561
208.4915 1802.312
208.9736 1863.782
209.4557 1922.883
209.9378 1968.938
210.4199 2000.618
210.9020 2026.577
211.3842 2045.627
211.8663 2060.122
212.3484 2079.910
212.8305 2110.323
213.3126 2134.360
213.7948 2140.735
214.2769 2126.334
214.7590 2106.185
215.2411 2083.063
215.7232 2055.699
216.2053 2016.813
216.6875 1962.904
217.1696 1903.967
217.6517 1846.239
218.1338 1789.416
218.6159 1734.241
219.0980 1683.026
219.5802 1634.316
220.0623 1573.209
220.5444 1496.348
221.0265 1411.268
221.5086 1325.940
221.9907 1239.908
222.4729 1152.492
222.9550 1059.111
223.4371 960.7051
223.9192 879.4961
224.4013 824.5215
224.8834 778.1196
225.3656 720.2524
225.8477 643.0581
226.3298 572.0249
226.8119 511.5566
227.2940 462.5283
227.7761 421.1338
228.2583 396.0889
228.7404 370.8223
229.2225 320.7803
229.7046 221.2612
230.1867 144.9429
230.6688 118.9727
231.1510 155.1470
231.6331 164.7539
232.1152 137.2656
232.5973 91.16064
233.0794 52.20996
233.5615 18.95117
234.0437 4.446289
234.5258 13.20605
235.0079 0.4467770
235.4900 3.302734
235.9721 29.72998
236.4542 66.56006
236.9364 91.55811
237.4185 102.6338
237.9006 105.7290
238.3827 100.2974
238.8648 80.78857
239.3469 72.16895
239.8291 77.55469
240.3112 92.53906
240.7933 111.2739
241.2754 143.6309
241.7575 163.7729
242.2396 159.6216
242.7218 119.3501
243.2039 89.57861
243.6860 71.04736
244.1681 62.81787
244.6502 64.62061
245.1323 84.10449
245.6145 101.5566
246.0966 108.8306
246.5787 101.8770
247.0608 94.40967
247.5429 84.00293
248.0250 73.81836
248.5072 73.49805
248.9893 93.34082
249.4714 106.5703
249.9535 98.48535
250.4356 51.48389
250.9177 26.66064
251.3999 34.84912
251.8820 62.08740
252.3641 71.35791
252.8462 53.27393
253.3283 32.04102
253.8104 18.87402
254.2926 17.66406
254.7747 14.06787
255.2568 4.707031
255.7389 6.597656
256.2210 7.408691
256.7031 7.375977
257.1852 24.11084
257.6674 37.46680
258.1495 50.41309
258.6316 51.02588
259.1137 33.01074
259.5958 3.979492
260.0779 11.36963
260.5601 5.601563
261.0422 0.6748050
261.5243 4.922852
262.0064 27.96582
262.4885 44.81201
262.9706 51.77783
263.4528 52.42188
263.9349 58.17822
264.4170 71.07471
264.8991 85.07715
265.3812 97.49609
265.8633 108.9565
266.3455 116.1826
266.8276 117.8281
267.3097 115.4990
267.7918 113.9150
268.2739 113.1030
268.7560 113.0361
269.2382 112.4551
269.7203 109.5757
270.2024 115.5195
270.6845 135.4434
271.1666 162.4893
271.6487 173.8438
272.1309 165.5698
272.6130 153.1387
273.0951 144.7329
273.5772 140.4209
274.0593 140.8760
274.5414 147.8037
275.0236 158.4893
275.5057 165.8896
275.9878 170.0859
276.4699 170.9985
276.9520 163.9458
277.4341 146.9141
277.9163 148.1943
278.3984 175.5522
278.8805 217.2910
279.3626 244.3911
279.8447 255.2153
280.3268 261.4985
280.8090 270.2446
281.2911 281.5571
281.7732 290.3730
282.2553 295.9058
282.7374 299.0229
283.2195 299.7837
283.7017 297.3994
284.1838 299.2690
284.6659 312.0879
285.1480 335.1992
285.6301 355.7192
286.1122 372.4985
286.5944 386.6514
287.0765 400.6196
287.5586 414.5156
288.0407 426.2393
288.5228 434.0239
289.0049 438.3901
289.4871 440.9292
289.9692 440.0156
290.4513 441.2935
290.9334 454.6665
291.4155 479.3735
291.8976 508.6978
292.3798 547.1841
292.8619 590.9492
293.3440 614.6172
293.8261 609.1836
294.3082 596.2729
294.7903 613.4219
295.2725 656.9292
295.7546 697.0513
296.2367 709.5474
296.7188 707.6260
297.2009 721.6675
297.6830 754.8081
298.1652 796.0244
298.6473 835.8716
299.1294 872.9238
299.6115 907.6904
300.0936 943.7192
300.5757 980.4385
301.0579 1009.526
301.5400 1026.300
302.0221 1049.172
302.5042 1099.973
302.9863 1171.083
303.4684 1243.029
303.9506 1301.215
304.4327 1359.428
304.9148 1435.588
305.3969 1529.718
305.8790 1638.459
306.3611 1757.619
306.8433 1886.809
307.3254 2024.726
307.8075 2175.835
308.2896 2338.838
308.7717 2502.794
309.2538 2666.223
309.7360 2850.380
310.2181 3078.483
310.7002 3341.762
311.1823 3620.925
311.6644 3901.021
312.1465 4198.160
312.6287 4518.786
313.1108 4865.015
313.5929 5236.019
314.0750 5639.176
314.5571 6069.177
315.0392 6522.734
315.5214 6990.410
316.0035 7489.399
316.4856 8026.269
316.9677 8602.025
317.4498 9211.473
317.9319 9849.430
318.4141 10512.98
318.8962 11195.53
319.3783 11906.22
319.8604 12637.03
320.3425 13384.56
320.8246 14148.80
321.3068 14937.13
321.7889 15765.15
322.2710 16601.60
322.7531 17422.86
323.2352 18222.39
323.7173 19007.05
324.1995 19781.35
324.6816 20542.25
325.1637 21276.85
325.6458 22052.86
326.1279 22751.48
326.6100 23318.28
327.0922 23695.66
327.5743 24010.01
328.0564 24287.43
328.5385 24509.65
329.0206 24612.13
329.5027 24611.93
329.9849 24478.83
330.4670 24196.63
330.9491 23714.68
331.4312 23175.25
331.9133 22583.21
332.3954 21931.08
332.8776 21193.68
333.3597 20335.86
333.8418 19450.78
334.3239 18561.42
334.8061 17658.86
335.2882 16769.93
335.7703 15891.63
336.2524 15018.07
336.7345 14148.71
337.2166 13267.01
337.6988 12407.65
338.1809 11596.51
338.6630 10823.27
339.1451 10092.30
339.6272 9398.847
340.1093 8744.473
340.5915 8144.431
341.0736 7598.534
341.5557 7078.979
342.0378 6577.460
342.5199 6097.016
343.0020 5641.228
343.4842 5214.396
343.9663 4810.861
344.4484 4432.333
344.9305 4075.745
345.4126 3742.574
345.8947 3425.848
346.3769 3133.857
346.8590 2881.245
347.3411 2666.536
347.8232 2476.557
348.3053 2302.786
348.7874 2143.897
349.2696 1991.304
349.7517 1839.212
350.2338 1695.180
350.7159 1564.924
351.1980 1449.271
351.6801 1351.166
352.1623 1282.680
352.6444 1232.463
353.1265 1179.806
353.6086 1121.427
354.0907 1059.727
354.5728 985.6328
355.0550 907.7588
355.5371 850.0073
356.0192 838.6206
356.5013 848.5303
356.9834 853.6938
357.4655 850.1157
357.9477 849.4233
358.4298 860.4878
358.9119 879.8657
359.3940 902.0830
359.8761 924.4365
360.3582 949.2969
360.8404 975.9058
361.3225 1003.882
361.8046 1042.556
362.2867 1094.388
362.7688 1159.581
363.2509 1238.366
363.7331 1341.998
364.2152 1447.830
364.6973 1543.785
365.1794 1630.908
365.6615 1731.833
366.1436 1851.988
366.6258 1987.171
367.1079 2134.640
367.5900 2308.818
368.0721 2478.420
368.5542 2631.294
369.0363 2774.150
369.5185 2938.737
370.0006 3143.285
370.4827 3352.527
370.9648 3551.908
371.4469 3741.786
371.9290 3924.678
372.4112 4095.006
372.8933 4259.345
373.3754 4431.590
373.8575 4614.131
374.3396 4804.988
374.8217 5008.847
375.3039 5228.328
375.7860 5431.304
376.2681 5618.445
376.7502 5787.104
377.2323 5927.589
377.7144 6028.323
378.1966 6153.306
378.6787 6334.580
379.1608 6561.327
379.6429 6757.728
380.1250 6922.949
380.6071 7057.015
381.0893 7150.963
381.5714 7207.712
382.0535 7257.378
382.5356 7318.343
383.0177 7368.842
383.4998 7354.767
383.9820 7275.703
384.4641 7160.917
384.9462 7015.472
385.4283 6854.337
385.9104 6715.390
386.3925 6612.427
386.8747 6508.807
387.3568 6358.632
387.8389 6172.198
388.3210 5980.676
388.8031 5810.639
389.2852 5642.409
389.7674 5454.534
390.2495 5240.126
390.7316 5017.308
391.2137 4794.836
391.6958 4572.574
392.1779 4354.076
392.6601 4130.340
393.1422 3919.359
393.6243 3735.630
394.1064 3579.316
394.5885 3426.976
395.0706 3275.763
395.5528 3121.272
396.0349 2959.717
396.5170 2790.011
396.9991 2613.865
397.4812 2416.957
397.9633 2208.598
398.4455 2025.738
398.9276 1891.286
399.4097 1769.594
399.8918 1644.544
400.3739 1517.461
400.8560 1383.560
401.3382 1235.614
401.8203 1082.061
402.3024 940.2158
402.7845 799.7104
403.2666 685.8115
403.7487 613.6812
404.2309 592.1177
404.7130 550.5708
405.1951 476.0439
405.6772 399.1431
406.1593 364.7183
406.6414 384.6514
407.1236 383.6689
407.6057 335.3159
408.0878 252.3887
408.5699 194.4985
409.0520 163.4653
409.5341 145.8560
410.0163 135.0688
410.4984 130.0645
410.9805 120.4380
411.4626 102.3716
411.9447 82.82666
412.4268 76.49316
412.9090 81.24902
413.3911 83.81836
413.8732 74.91699
414.3553 59.14844
414.8374 41.91260
415.3195 22.83398
415.8017 9.689453
416.2838 16.86914
416.7659 34.55029
417.2480 44.88818
417.7301 37.06934
418.2122 21.47314
418.6944 2.127930
419.1765 20.38965
419.6586 37.37500
420.1407 43.52832
420.6228 42.92627
421.1049 39.13037
421.5871 31.62500
422.0692 22.57666
422.5513 7.981934
423.0334 8.502930
423.5155 15.15771
423.9977 0.2661130
424.4798 17.86133
424.9619 29.26611
425.4440 32.17139
425.9261 33.89258
426.4082 35.40820
426.8904 35.65771
427.3725 32.01953
427.8546 16.56201
428.3367 10.97119
428.8188 25.48682
429.3009 59.59961
429.7831 73.87646
430.2652 60.45850
430.7473 41.66211
431.2294 37.24561
431.7115 49.39600
432.1936 57.97266
432.6758 59.96045
433.1579 57.02197
433.6400 52.69238
434.1221 46.91406
434.6042 41.64209
435.0863 39.16113
435.5685 38.47363
436.0506 35.12158
436.5327 28.66016
437.0148 21.73535
437.4969 17.10059
437.9790 14.57324
438.4612 13.37842
438.9433 11.18457
439.4254 11.43994
439.9075 22.77295
440.3896 43.49707
440.8717 56.24805
441.3539 36.26074
441.8360 8.299805
442.3181 0.2724610
442.8002 30.17480
443.2823 58.20020
443.7644 63.50000
444.2466 52.34229
444.7287 39.42236
445.2108 25.53271
445.6929 13.08691
446.1750 5.771484
446.6571 7.248535
447.1393 1.577637
447.6214 20.20703
448.1035 46.56641
448.5856 65.42041
449.0677 74.48877
449.5498 79.21826
450.0320 78.66211
450.5141 73.86230
450.9962 71.99854
451.4783 73.39893
451.9604 77.24658
452.4425 83.31299
452.9247 92.12646
453.4068 103.4771
453.8889 118.6890
454.3710 134.2520
454.8531 142.1826
455.3352 142.2236
455.8174 143.7773
456.2995 149.5317
456.7816 159.6235
457.2637 178.3696
457.7458 206.4409
458.2279 230.2031
458.7101 234.5171
459.1922 226.0972
459.6743 220.1938
460.1564 223.7539
460.6385 226.7974
461.1206 214.1733
461.6028 192.1274
462.0849 178.5137
462.5670 195.8110
463.0491 217.9590
463.5312 223.4741
464.0133 205.7466
464.4955 191.8955
464.9776 189.5874
465.4597 198.1079
465.9418 216.4512
466.4239 271.4233
466.9060 307.5283
467.3882 297.9565
467.8703 247.1006
468.3524 222.2554
468.8345 249.2324
469.3166 278.5977
469.7987 283.6187
470.2809 245.4351
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1297.111 0.0000000E+00
