#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-05-24 15:35:46 +0300 (Thu, 24 May 2018) $
#$Revision: 756 $
#$URL: svn://172.16.1.111/rod/cif/1/00/02/1000260.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000260
loop_
_publ_author_name
'Rastsvetaeva, R. K.'
'Tamazyan, R. A.'
'Pushcharovskii D Yu'
'Nadezhina, T. N.'
'Voloshin, A. V.'
_publ_section_title
;
 K-nenadkevichite, a new representative of the nenadkevichite-labuntsovite
 series
;
_journal_name_full               'Crystallography Reports'
_journal_page_first              908
_journal_page_last               914
_journal_volume                  39
_journal_year                    1994
_chemical_compound_source        'Vuoriyarvi, Kola Peninsula'
_chemical_formula_sum            'H10.3 K2.98 Na1.22 Nb2.2 O31.15 Si8 Ti1.8'
_chemical_name_mineral           Vuoriyarvite
_space_group_IT_number           8
_symmetry_space_group_name_Hall  'C -2y'
_symmetry_space_group_name_H-M   'C 1 m 1'
_cell_angle_alpha                90
_cell_angle_beta                 117.87
_cell_angle_gamma                90
_cell_length_a                   14.692
_cell_length_b                   14.164
_cell_length_c                   7.859
_cell_volume                     1445.745
_exptl_crystal_density_diffrn    2.684
_cod_original_formula_sum        'Si8 (Nb2.2 Ti1.8) K2.98 Na1.22 O31.15 H10.3'
_cod_database_code               9014345
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 15
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R070610.rod
_rod_data_source.block           3500000
_rod_database.code               1000260
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9014345 COD http://www.crystallography.net/cod/9014345.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
149.7655 0.0000000E+00
150.2476 12.16211
150.7297 1.207031
151.2118 95.22852
151.6939 258.6738
152.1760 513.6133
152.6582 763.8594
153.1403 983.4551
153.6224 1175.479
154.1045 1387.363
154.5866 1625.219
155.0687 1886.641
155.5508 2169.965
156.0330 2497.467
156.5151 2815.740
156.9972 3107.154
157.4793 3370.445
157.9614 3634.146
158.4435 3910.703
158.9257 4205.311
159.4078 4519.197
159.8899 4872.148
160.3720 5213.074
160.8541 5523.912
161.3362 5803.238
161.8184 6055.533
162.3005 6281.211
162.7826 6481.984
163.2647 6660.475
163.7468 6829.729
164.2289 6971.543
164.7111 7072.971
165.1932 7134.807
165.6753 7154.342
166.1574 7171.801
166.6395 7209.143
167.1216 7214.699
167.6038 7173.605
168.0859 7084.586
168.5680 6951.051
169.0501 6765.012
169.5322 6538.088
170.0143 6256.121
170.4965 5920.545
170.9786 5582.215
171.4607 5261.207
171.9428 4947.617
172.4249 4629.094
172.9070 4290.219
173.3892 3949.814
173.8713 3632.357
174.3534 3340.613
174.8355 3055.344
175.3176 2750.252
175.7997 2436.328
176.2819 2147.049
176.7640 1903.764
177.2461 1691.160
177.7282 1494.111
178.2103 1312.238
178.6924 1134.732
179.1745 935.1621
179.6567 720.7832
180.1388 530.9199
180.6209 401.7227
181.1030 312.9375
181.5851 198.8105
182.0672 43.90625
182.5494 114.8848
183.0315 215.6699
183.5136 262.3457
183.9957 289.6816
184.4778 321.0781
184.9599 353.6621
185.4421 375.0762
185.9242 382.8867
186.4063 379.2480
186.8884 367.2480
187.3705 346.6641
187.8526 321.5703
188.3348 299.3730
188.8169 278.3945
189.2990 242.7402
189.7811 190.8652
190.2632 121.2734
190.7453 27.80469
191.2275 89.63477
191.7096 229.8574
192.1917 394.6680
192.6738 586.1777
193.1559 788.3047
193.6380 997.9922
194.1202 1214.639
194.6023 1439.408
195.0844 1669.266
195.5665 1911.553
196.0486 2173.287
196.5307 2453.490
197.0129 2760.424
197.4950 3106.566
197.9771 3492.912
198.4592 3864.662
198.9413 4213.834
199.4234 4561.000
199.9055 4941.518
200.3877 5357.617
200.8698 5797.809
201.3519 6260.762
201.8340 6752.721
202.3161 7224.682
202.7982 7667.525
203.2804 8094.969
203.7625 8548.121
204.2446 9039.932
204.7267 9516.988
205.2088 9938.576
205.6909 10285.03
206.1731 10663.17
206.6552 11097.31
207.1373 11566.04
207.6194 11974.88
208.1015 12310.10
208.5836 12633.67
209.0658 12996.29
209.5479 13414.13
210.0300 13799.15
210.5121 14135.75
210.9942 14426.91
211.4763 14718.79
211.9585 15028.65
212.4406 15312.47
212.9227 15524.13
213.4048 15646.47
213.8869 15750.09
214.3690 15852.28
214.8512 15951.93
215.3333 16019.05
215.8154 16070.19
216.2975 16067.50
216.7796 15961.73
217.2617 15716.54
217.7439 15445.13
218.2260 15164.70
218.7081 14877.19
219.1902 14590.29
219.6723 14306.12
220.1544 14020.90
220.6366 13720.17
221.1187 13393.44
221.6008 13075.76
222.0829 12772.45
222.5650 12472.71
223.0471 12227.75
223.5293 12049.07
224.0114 11915.90
224.4935 11787.46
224.9756 11656.37
225.4577 11544.81
225.9398 11461.04
226.4220 11400.38
226.9041 11380.39
227.3862 11402.77
227.8683 11465.83
228.3504 11567.76
228.8325 11717.07
229.3147 11892.34
229.7968 12077.74
230.2789 12251.61
230.7610 12488.06
231.2431 12807.48
231.7252 13187.58
232.2074 13564.85
232.6895 13946.42
233.1716 14320.05
233.6537 14676.19
234.1358 14984.82
234.6179 15334.26
235.1001 15748.69
235.5822 16209.42
236.0643 16641.91
236.5464 17025.09
237.0285 17407.42
237.5106 17822.44
237.9928 18289.58
238.4749 18737.73
238.9570 19150.35
239.4391 19534.45
239.9212 19936.85
240.4033 20377.76
240.8855 20803.78
241.3676 21185.80
241.8497 21534.74
242.3318 21810.88
242.8139 21990.98
243.2960 22084.14
243.7782 22194.49
244.2603 22364.13
244.7424 22505.31
245.2245 22546.59
245.7066 22455.04
246.1887 22327.50
246.6708 22174.86
247.1530 21997.64
247.6351 21790.04
248.1172 21549.02
248.5993 21282.78
249.0814 20995.36
249.5635 20694.53
250.0457 20356.22
250.5278 19971.44
251.0099 19539.82
251.4920 19081.90
251.9741 18603.25
252.4562 18098.93
252.9384 17558.99
253.4205 16952.91
253.9026 16372.07
254.3847 15848.49
254.8668 15381.44
255.3489 14877.71
255.8311 14316.34
256.3132 13735.26
256.7953 13188.44
257.2774 12692.98
257.7595 12178.48
258.2416 11633.85
258.7238 11048.89
259.2059 10475.39
259.6880 9896.713
260.1701 9341.833
260.6522 8840.433
261.1343 8414.170
261.6165 7998.938
262.0986 7573.584
262.5807 7129.638
263.0628 6748.262
263.5449 6432.053
264.0270 6175.866
264.5092 5972.957
264.9913 5840.437
265.4734 5702.949
265.9555 5531.904
266.4376 5328.489
266.9197 5159.754
267.4019 5027.544
267.8840 4927.586
268.3661 4859.302
268.8482 4824.451
269.3303 4814.098
269.8124 4833.237
270.2946 4884.733
270.7767 4918.973
271.2588 4925.374
271.7409 4927.244
272.2230 4960.373
272.7051 5029.055
273.1873 5115.104
273.6694 5215.381
274.1515 5329.260
274.6336 5436.143
275.1157 5535.818
275.5978 5630.668
276.0800 5723.115
276.5621 5813.909
277.0442 5905.129
277.5263 5993.218
278.0084 6078.707
278.4905 6183.501
278.9726 6309.482
279.4547 6445.836
279.9369 6593.754
280.4190 6757.779
280.9011 6879.221
281.3832 6911.863
281.8653 6864.279
282.3474 6859.034
282.8296 6909.980
283.3117 6964.900
283.7938 6939.926
284.2759 6836.584
284.7580 6731.881
285.2401 6669.098
285.7223 6637.561
286.2044 6569.971
286.6865 6462.067
287.1686 6335.417
287.6507 6223.328
288.1328 6123.264
288.6150 6015.488
289.0971 5889.207
289.5792 5748.227
290.0613 5601.184
290.5434 5446.177
291.0255 5294.699
291.5077 5161.254
291.9898 5043.130
292.4719 4930.105
292.9540 4821.112
293.4361 4711.373
293.9182 4591.067
294.4004 4457.558
294.8825 4317.811
295.3646 4175.095
295.8467 4030.897
296.3288 3892.739
296.8109 3760.544
297.2931 3638.384
297.7752 3541.467
298.2573 3473.183
298.7394 3411.683
299.2215 3337.479
299.7036 3253.590
300.1858 3171.406
300.6679 3093.896
301.1500 3021.214
301.6321 2951.378
302.1142 2884.979
302.5963 2821.839
303.0785 2767.203
303.5606 2714.995
304.0427 2655.210
304.5248 2587.362
305.0069 2507.103
305.4890 2406.654
305.9712 2282.525
306.4533 2159.712
306.9354 2055.652
307.4175 1962.161
307.8996 1869.230
308.3817 1777.157
308.8639 1680.567
309.3460 1571.748
309.8281 1449.816
310.3102 1337.000
310.7923 1264.704
311.2744 1203.972
311.7566 1118.469
312.2387 952.5752
312.7208 792.6992
313.2029 694.4004
313.6850 660.1953
314.1671 627.2598
314.6493 575.4326
315.1314 508.6680
315.6135 432.2998
316.0956 319.1328
316.5777 222.8457
317.0598 175.9414
317.5420 178.2324
318.0241 164.6016
318.5062 95.20801
318.9883 12.27734
319.4704 48.75879
319.9525 54.69043
320.4347 64.36328
320.9168 100.7920
321.3989 162.0684
321.8810 200.6641
322.3631 186.3193
322.8452 159.6357
323.3273 149.5137
323.8094 178.7100
324.2916 202.4814
324.7737 214.7480
325.2558 216.1250
325.7379 215.3652
326.2200 210.8623
326.7021 205.4873
327.1843 201.2764
327.6664 203.2949
328.1485 199.5342
328.6306 184.5811
329.1127 161.4814
329.5948 149.6738
330.0770 159.8740
330.5591 169.8340
331.0412 165.4561
331.5233 138.2715
332.0054 114.8975
332.4875 95.44824
332.9697 80.71387
333.4518 75.07910
333.9339 82.82520
334.4160 92.13037
334.8981 98.99414
335.3802 107.0020
335.8624 98.57373
336.3445 67.51025
336.8266 23.82422
337.3087 8.994629
337.7908 29.43750
338.2729 43.84766
338.7551 51.95801
339.2372 53.06299
339.7193 65.41309
340.2014 94.57861
340.6835 127.1914
341.1656 132.0615
341.6478 106.7026
342.1299 93.65479
342.6120 123.5693
343.0941 188.8687
343.5762 234.0522
344.0583 255.4077
344.5405 267.1206
345.0226 296.6304
345.5047 339.2856
345.9868 358.7207
346.4689 315.9204
346.9510 239.8892
347.4332 204.3145
347.9153 212.1401
348.3974 239.5962
348.8795 266.1709
349.3616 293.2959
349.8438 325.2261
350.3259 365.3389
350.8080 410.2603
351.2901 458.2637
351.7722 509.2075
352.2543 556.6699
352.7365 591.9775
353.2186 620.3657
353.7007 650.1914
354.1828 685.2485
354.6649 722.5000
355.1470 760.2188
355.6292 798.4790
356.1113 838.1597
356.5934 879.1187
357.0755 923.5845
357.5576 973.2207
358.0397 1021.943
358.5219 1077.237
359.0040 1149.687
359.4861 1235.353
359.9682 1313.832
360.4503 1377.304
360.9324 1431.331
361.4146 1478.080
361.8967 1505.679
362.3788 1543.434
362.8609 1606.754
363.3430 1685.211
363.8251 1750.796
364.3073 1777.903
364.7894 1809.306
365.2715 1865.508
365.7536 1972.967
366.2357 2058.926
366.7178 2109.716
367.2000 2137.706
367.6820 2165.765
368.1642 2194.188
368.6463 2222.526
369.1284 2250.933
369.6105 2279.637
370.0926 2307.200
370.5747 2337.193
371.0569 2363.054
371.5390 2375.146
372.0211 2365.984
372.5032 2360.620
372.9853 2371.292
373.4674 2398.365
373.9496 2396.216
374.4317 2358.313
374.9138 2304.225
375.3959 2250.369
375.8780 2194.910
376.3601 2150.263
376.8423 2122.864
377.3244 2104.101
377.8065 2067.083
378.2886 2008.588
378.7707 1948.247
379.2528 1907.767
379.7350 1884.096
380.2171 1848.667
380.6992 1791.801
381.1813 1726.310
381.6634 1671.232
382.1455 1627.032
382.6277 1591.658
383.1098 1573.296
383.5919 1562.360
384.0740 1537.151
384.5561 1489.550
385.0382 1442.409
385.5204 1423.603
386.0025 1426.021
386.4846 1429.022
386.9667 1416.655
387.4488 1402.200
387.9309 1399.991
388.4131 1413.891
388.8952 1426.435
389.3773 1431.910
389.8594 1428.850
390.3415 1415.385
390.8236 1370.909
391.3058 1331.146
391.7879 1318.195
392.2700 1334.016
392.7521 1344.323
393.2342 1339.486
393.7163 1324.435
394.1985 1303.855
394.6806 1268.199
395.1627 1238.971
395.6448 1228.008
396.1269 1232.109
396.6090 1215.953
397.0912 1155.709
397.5733 1089.721
398.0554 1038.603
398.5375 1010.850
399.0196 984.3643
399.5017 962.2207
399.9839 939.8271
400.4660 901.3154
400.9481 834.4229
401.4302 772.6655
401.9123 733.6807
402.3944 726.1660
402.8766 707.5352
403.3587 677.6982
403.8408 637.5776
404.3229 583.3428
404.8050 510.8799
405.2871 448.2417
405.7693 410.7451
406.2514 395.7651
406.7335 375.9443
407.2156 351.8735
407.6977 320.4614
408.1798 273.6846
408.6620 214.4175
409.1441 159.2212
409.6262 104.8379
410.1083 62.93311
410.5904 70.76660
411.0725 124.3345
411.5547 164.9370
412.0368 134.0112
412.5189 62.86426
413.0010 7.224121
413.4831 12.01514
413.9652 28.28467
414.4473 86.53076
414.9294 168.9360
415.4116 224.2856
415.8937 200.4570
416.3758 154.4854
416.8579 129.2134
417.3400 135.0762
417.8221 147.7656
418.3043 163.4111
418.7864 177.9512
419.2685 185.3276
419.7506 186.7793
420.2327 178.1880
420.7148 153.0474
421.1970 107.7549
421.6791 73.31299
422.1612 60.37451
422.6433 56.14355
423.1254 50.26758
423.6075 53.36377
424.0897 39.93750
424.5718 0.3398440
425.0539 60.75146
425.5360 110.9028
426.0181 142.5322
426.5002 173.8765
426.9824 217.7666
427.4645 279.8027
427.9466 331.1479
428.4287 365.9854
428.9108 393.5244
429.3929 434.5103
429.8751 490.2881
430.3572 549.0449
430.8393 605.7891
431.3214 660.7432
431.8035 712.9727
432.2856 762.7319
432.7678 811.1074
433.2499 856.2236
433.7320 900.1992
434.2141 952.8730
434.6962 1025.954
435.1783 1103.860
435.6605 1159.271
436.1426 1193.902
436.6247 1228.441
437.1068 1281.038
437.5889 1341.430
438.0710 1396.224
438.5532 1438.466
439.0353 1478.987
439.5174 1519.201
439.9995 1562.292
440.4816 1617.301
440.9637 1705.761
441.4459 1793.374
441.9280 1854.811
442.4101 1870.967
442.8922 1911.620
443.3743 2013.361
443.8564 2142.502
444.3386 2252.558
444.8207 2326.910
445.3028 2395.251
445.7849 2460.545
446.2670 2522.147
446.7491 2591.776
447.2313 2673.301
447.7134 2759.653
448.1955 2843.720
448.6776 2922.431
449.1597 3010.000
449.6418 3110.517
450.1240 3219.333
450.6061 3317.900
451.0882 3403.676
451.5703 3490.216
452.0524 3592.782
452.5345 3708.269
453.0167 3792.373
453.4988 3840.721
453.9809 3863.398
454.4630 3868.887
454.9451 3858.267
455.4272 3836.766
455.9094 3802.585
456.3915 3760.530
456.8736 3720.829
457.3557 3683.117
457.8378 3632.370
458.3199 3558.767
458.8020 3466.444
459.2841 3357.267
459.7663 3217.614
460.2484 3083.265
460.7305 2979.816
461.2126 2900.210
461.6947 2822.269
462.1768 2727.820
462.6590 2641.819
463.1411 2579.691
463.6232 2555.997
464.1053 2519.836
464.5874 2444.168
465.0695 2358.148
465.5517 2299.472
466.0338 2270.966
466.5159 2267.428
466.9980 2299.223
467.4801 2364.169
467.9622 2395.380
468.4444 2366.121
468.9265 2346.449
469.4086 2397.910
469.8907 2539.800
470.3728 2647.156
470.8549 2699.647
471.3371 2721.989
471.8192 2765.006
472.3013 2827.307
472.7834 2897.623
473.2655 2971.561
473.7477 3054.184
474.2298 3154.211
474.7119 3271.267
475.1940 3391.651
475.6761 3500.936
476.1582 3603.651
476.6404 3710.132
477.1225 3829.557
477.6046 3950.742
478.0867 4062.975
478.5688 4168.272
479.0509 4271.622
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1248.026 82.46387
1248.509 71.31641
1248.991 55.75635
1249.473 41.83936
1249.955 26.54395
1250.437 29.94434
1250.919 74.49072
1251.401 115.2783
1251.883 95.24023
1252.366 56.66113
1252.848 49.85352
1253.330 78.45654
1253.812 76.88037
1254.294 42.74463
1254.776 25.81787
1255.258 68.89990
1255.740 114.6021
1256.223 119.5391
1256.705 98.22314
1257.187 73.74902
1257.669 43.24658
1258.151 25.71631
1258.633 21.60156
1259.115 23.44775
1259.597 32.17090
1260.079 39.13525
1260.562 40.34424
1261.044 35.89209
1261.526 22.65918
1262.008 0.4394530
1262.490 2.187988
1262.972 17.93555
1263.454 37.29688
1263.936 41.71143
1264.418 37.55518
1264.901 20.23047
1265.383 0.4472660
1265.865 7.799316
1266.347 35.30176
1266.829 52.60107
1267.311 48.73535
1267.793 36.07324
1268.275 15.87451
1268.758 0.8686520
1269.240 0.1147460
1269.722 0.0000000E+00
