#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-05-24 15:35:50 +0300 (Thu, 24 May 2018) $
#$Revision: 757 $
#$URL: svn://172.16.1.111/rod/cif/1/00/02/1000261.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000261
loop_
_publ_author_name
'Yakubovich, O. V.'
'Massa, W.'
'Chukanov, N. V.'
_publ_section_title
;
 Crystal structure of britvinite
 [Pb7(OH)3F(BO3)2(CO3)][Mg4.5(OH)3(Si5O14)]: A new layered silicate with
 an original type of silicon-oxygen networks Locality: Varmland, Sweden
;
_journal_name_full               'Crystallography Reports'
_journal_page_first              206
_journal_page_last               215
_journal_paper_doi               10.1134/S1063774508020077
_journal_volume                  53
_journal_year                    2008
_chemical_compound_source        R070639
_chemical_formula_sum            'C2 B3.468 F2 Mg9 O58 Pb14.144 Si10.532'
_chemical_name_mineral           Britvinite
_space_group_IT_number           2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                80.365
_cell_angle_beta                 75.816
_cell_angle_gamma                59.870
_cell_length_a                   9.3409
_cell_length_b                   9.3579
_cell_length_c                   18.8333
_cell_volume                     1378.475
_exptl_crystal_density_diffrn    5.388
_cod_original_formula_sum        'Si10.532 Mg9 Pb14.144 C2 B3.468 O58 F2'
_cod_database_code               9012668
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 15
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R070639.rod
_rod_data_source.block           3500000
_rod_database.code               1000261
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9012668 COD http://www.crystallography.net/cod/9012668.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
156.2860 0.0000000E+00
156.7682 27.26758
157.2503 37.68359
157.7324 30.99219
158.2145 25.83008
158.6966 23.66797
159.1787 36.74414
159.6609 75.06055
160.1430 90.40430
160.6251 87.48633
161.1072 70.66211
161.5893 36.40039
162.0714 14.75195
162.5536 10.57617
163.0357 11.39258
163.5178 37.29883
163.9999 65.69727
164.4820 78.69141
164.9641 74.87109
165.4463 86.27930
165.9284 140.2012
166.4105 198.8633
166.8926 227.8418
167.3747 172.3633
167.8568 98.20898
168.3390 55.63672
168.8211 60.01562
169.3032 77.83594
169.7853 89.02148
170.2674 96.64844
170.7495 116.3232
171.2317 132.2129
171.7138 157.2422
172.1959 210.4766
172.6780 272.8340
173.1601 328.2979
173.6422 346.0889
174.1244 328.4727
174.6065 309.8418
175.0886 334.2910
175.5707 376.7959
176.0528 394.3145
176.5349 370.2471
177.0171 336.5928
177.4992 327.6699
177.9813 342.3213
178.4634 363.3984
178.9455 391.5859
179.4276 419.1523
179.9098 423.2363
180.3919 389.8711
180.8740 336.1543
181.3561 284.9688
181.8382 254.5176
182.3203 229.7969
182.8025 226.8281
183.2846 235.8936
183.7667 209.1221
184.2488 170.0576
184.7309 134.6650
185.2130 106.6367
185.6951 81.44922
186.1773 71.31836
186.6594 49.28418
187.1415 15.80371
187.6236 8.164063
188.1057 5.673828
188.5878 17.39746
189.0700 30.06543
189.5521 28.67773
190.0342 21.69238
190.5163 19.18262
190.9984 20.59082
191.4805 32.29492
191.9627 59.54883
192.4448 99.76270
192.9269 130.2344
193.4090 144.5391
193.8911 147.3799
194.3732 156.8164
194.8554 174.2979
195.3375 193.7754
195.8196 212.2197
196.3017 229.8330
196.7838 240.3096
197.2659 241.3301
197.7481 234.4961
198.2302 228.0107
198.7123 221.9443
199.1944 215.7637
199.6765 210.3809
200.1586 207.4756
200.6408 197.8135
201.1229 173.0527
201.6050 133.2627
202.0871 109.2822
202.5692 105.5234
203.0513 110.3184
203.5335 103.1816
204.0156 81.08594
204.4977 58.74805
204.9798 45.61035
205.4619 45.05859
205.9440 28.28125
206.4262 13.18652
206.9083 66.23828
207.3904 95.07812
207.8725 92.89258
208.3546 85.86523
208.8367 93.76660
209.3189 125.8018
209.8010 131.1016
210.2831 91.26172
210.7652 23.21289
211.2473 7.783203
211.7294 64.33887
212.2116 134.9365
212.6937 180.4414
213.1758 205.1797
213.6579 187.4287
214.1400 38.53223
214.6221 168.6787
215.1043 282.1943
215.5864 270.7266
216.0685 213.0459
216.5506 188.0938
217.0327 208.3760
217.5148 228.3428
217.9970 237.9766
218.4791 237.3398
218.9612 230.5420
219.4433 213.4502
219.9254 194.6289
220.4075 187.3906
220.8897 200.4004
221.3718 207.6582
221.8539 200.4307
222.3360 173.7471
222.8181 150.6514
223.3002 127.8379
223.7824 111.6729
224.2645 118.8203
224.7466 169.1953
225.2287 206.8525
225.7108 203.4541
226.1929 130.9990
226.6750 99.37109
227.1572 125.2793
227.6393 187.9033
228.1214 234.4170
228.6035 261.2754
229.0856 277.1772
229.5677 282.7769
230.0499 265.0767
230.5320 269.5947
231.0141 309.0586
231.4962 372.4263
231.9783 414.4722
232.4604 424.1440
232.9426 427.1919
233.4247 438.7393
233.9068 463.7324
234.3889 486.4775
234.8710 502.5381
235.3531 513.8589
235.8353 537.7617
236.3174 581.1699
236.7995 629.7515
237.2816 672.5015
237.7637 705.2456
238.2458 739.2134
238.7280 772.9048
239.2101 806.5527
239.6922 856.6260
240.1743 934.4771
240.6564 1017.653
241.1385 1084.835
241.6207 1128.863
242.1028 1169.734
242.5849 1210.976
243.0670 1253.239
243.5491 1291.570
244.0313 1324.412
244.5134 1354.868
244.9955 1385.662
245.4776 1414.422
245.9597 1450.139
246.4418 1498.028
246.9240 1560.215
247.4061 1616.685
247.8882 1663.363
248.3703 1706.687
248.8524 1756.075
249.3345 1816.376
249.8167 1876.219
250.2988 1931.738
250.7809 1980.642
251.2630 2032.674
251.7451 2091.829
252.2272 2151.077
252.7094 2198.133
253.1915 2233.673
253.6736 2255.562
254.1557 2263.865
254.6378 2260.312
255.1199 2235.283
255.6021 2178.581
256.0842 2105.655
256.5663 2051.562
257.0484 2024.063
257.5305 2001.722
258.0126 1977.411
258.4948 1954.517
258.9769 1917.348
259.4590 1856.043
259.9411 1783.824
260.4232 1737.793
260.9053 1732.127
261.3875 1726.911
261.8696 1697.220
262.3517 1630.530
262.8338 1583.638
263.3159 1568.479
263.7980 1572.897
264.2802 1554.303
264.7623 1500.006
265.2444 1442.334
265.7265 1398.994
266.2086 1371.183
266.6907 1356.797
267.1729 1356.102
267.6550 1368.472
268.1371 1393.131
268.6192 1440.414
269.1013 1477.789
269.5834 1478.388
270.0656 1434.171
270.5477 1384.578
271.0298 1334.737
271.5119 1287.489
271.9940 1249.313
272.4761 1213.274
272.9583 1180.532
273.4404 1153.191
273.9225 1132.284
274.4046 1111.420
274.8867 1091.353
275.3688 1070.884
275.8510 1038.112
276.3331 986.0679
276.8152 943.5996
277.2973 939.1724
277.7794 976.5420
278.2615 1016.478
278.7437 1054.828
279.2258 1089.804
279.7079 1109.371
280.1900 1109.108
280.6721 1109.947
281.1542 1135.840
281.6364 1188.431
282.1185 1229.255
282.6006 1240.908
283.0827 1236.588
283.5648 1280.736
284.0469 1382.138
284.5291 1484.188
285.0112 1520.029
285.4933 1492.495
285.9754 1489.313
286.4575 1539.249
286.9396 1627.823
287.4217 1709.637
287.9038 1784.980
288.3860 1849.851
288.8681 1889.984
289.3502 1909.229
289.8323 1947.391
290.3144 2025.263
290.7965 2126.167
291.2787 2201.243
291.7608 2249.019
292.2429 2289.695
292.7250 2338.216
293.2071 2395.295
293.6892 2465.690
294.1714 2560.114
294.6535 2664.665
295.1356 2742.655
295.6177 2793.064
296.0998 2849.187
296.5819 2949.374
297.0641 3083.638
297.5462 3217.613
298.0283 3350.469
298.5104 3471.049
298.9925 3553.948
299.4746 3598.922
299.9568 3636.983
300.4389 3694.102
300.9210 3765.305
301.4031 3840.408
301.8852 3921.471
302.3673 3999.904
302.8495 4062.756
303.3316 4109.725
303.8137 4154.112
304.2958 4212.120
304.7779 4273.672
305.2600 4320.052
305.7422 4346.170
306.2243 4353.186
306.7064 4335.907
307.1885 4294.958
307.6706 4254.028
308.1527 4237.378
308.6349 4228.819
309.1170 4206.853
309.5991 4157.642
310.0812 4095.688
310.5633 4035.288
311.0454 3975.816
311.5276 3900.779
312.0097 3782.807
312.4918 3650.177
312.9739 3532.396
313.4560 3450.516
313.9381 3377.250
314.4203 3303.303
314.9024 3227.458
315.3845 3145.976
315.8666 3048.226
316.3487 2944.702
316.8308 2846.979
317.3130 2740.343
317.7951 2660.830
318.2772 2646.430
318.7593 2687.388
319.2414 2692.131
319.7235 2592.839
320.2057 2465.810
320.6878 2370.439
321.1699 2353.455
321.6520 2335.102
322.1341 2297.799
322.6162 2243.163
323.0984 2184.564
323.5805 2115.773
324.0626 2047.045
324.5447 1985.880
325.0268 1951.441
325.5089 1904.453
325.9911 1823.428
326.4732 1715.604
326.9553 1644.881
327.4374 1654.362
327.9195 1675.679
328.4016 1668.845
328.8838 1603.049
329.3659 1547.277
329.8480 1510.375
330.3301 1488.703
330.8122 1458.166
331.2943 1406.815
331.7765 1358.084
332.2586 1326.431
332.7407 1327.628
333.2228 1317.553
333.7049 1292.850
334.1870 1255.028
334.6692 1208.462
335.1513 1148.061
335.6334 1086.538
336.1155 1031.627
336.5976 984.4238
337.0797 939.6904
337.5619 900.0552
338.0440 861.6255
338.5261 812.3496
339.0082 747.7529
339.4903 686.0000
339.9724 637.4541
340.4546 602.1040
340.9367 575.9600
341.4188 560.2905
341.9009 551.3501
342.3830 544.6201
342.8651 541.5781
343.3473 529.1069
343.8294 493.3506
344.3115 436.7974
344.7936 395.7290
345.2757 371.9106
345.7578 363.2451
346.2400 370.2397
346.7221 392.2295
347.2042 415.6172
347.6863 433.2471
348.1684 446.8018
348.6505 463.2446
349.1327 483.8921
349.6148 502.0918
350.0969 505.9360
350.5790 499.0288
351.0611 495.7275
351.5432 504.9458
352.0254 521.1479
352.5075 542.0312
352.9896 569.3125
353.4717 580.5034
353.9538 544.9316
354.4359 478.6978
354.9181 414.6411
355.4002 359.5615
355.8823 317.5171
356.3644 302.0962
356.8465 313.6624
357.3286 314.3823
357.8108 268.4014
358.2929 200.0391
358.7750 139.9753
359.2571 102.1267
359.7392 73.40234
360.2213 42.30396
360.7035 10.07251
361.1856 4.032227
361.6677 34.56519
362.1498 82.46387
362.6319 102.3323
363.1140 55.99683
363.5962 8.971436
364.0783 21.85400
364.5604 37.48682
365.0425 45.81079
365.5246 45.97192
366.0067 41.09961
366.4889 33.14941
366.9710 8.951172
367.4531 2.723389
367.9352 5.973877
368.4173 30.79834
368.8994 53.34497
369.3815 76.58228
369.8636 94.36621
370.3458 103.0244
370.8279 93.40063
371.3100 91.50439
371.7921 107.2771
372.2742 128.7317
372.7563 121.9453
373.2385 62.00073
373.7206 15.01465
374.2027 14.80981
374.6848 79.76562
375.1669 112.9683
375.6490 103.5750
376.1312 73.75562
376.6133 62.16675
377.0954 74.58008
377.5775 81.56104
378.0596 65.82349
378.5417 28.68994
379.0239 18.47705
379.5060 41.63672
379.9881 72.35156
380.4702 76.50293
380.9523 55.06177
381.4344 32.74219
381.9166 20.27441
382.3987 12.54517
382.8808 9.780518
383.3629 47.54858
383.8450 84.39209
384.3271 96.83325
384.8093 94.21606
385.2914 106.7695
385.7735 153.4429
386.2556 209.8733
386.7377 236.1050
387.2198 236.2468
387.7020 242.3765
388.1841 282.6108
388.6662 340.9622
389.1483 396.6038
389.6304 442.9448
390.1125 487.6082
390.5947 540.0161
391.0768 596.8955
391.5589 646.4663
392.0410 678.5918
392.5231 703.9270
393.0052 729.4402
393.4874 754.5737
393.9695 784.2271
394.4516 822.6584
394.9337 866.7136
395.4158 910.6357
395.8979 947.8911
396.3801 988.7290
396.8622 1041.145
397.3443 1113.647
397.8264 1168.692
398.3085 1179.316
398.7906 1176.997
399.2728 1199.903
399.7549 1273.818
400.2370 1345.305
400.7191 1404.580
401.2012 1451.015
401.6833 1495.648
402.1655 1539.196
402.6476 1579.960
403.1297 1615.498
403.6118 1642.627
404.0939 1672.515
404.5760 1704.937
405.0582 1741.188
405.5403 1792.388
406.0224 1865.112
406.5045 1932.429
406.9866 1972.806
407.4688 1984.787
407.9509 1994.622
408.4330 2002.465
408.9151 2012.940
409.3972 2039.735
409.8793 2082.770
410.3615 2123.249
410.8436 2145.449
411.3257 2156.170
411.8078 2181.874
412.2899 2227.839
412.7720 2273.189
413.2542 2284.605
413.7363 2273.153
414.2184 2271.943
414.7005 2305.470
415.1826 2352.960
415.6647 2393.103
416.1469 2424.927
416.6290 2447.046
417.1111 2458.649
417.5932 2459.629
418.0753 2449.821
418.5574 2411.838
419.0396 2378.161
419.5217 2373.924
420.0038 2393.624
420.4859 2400.730
420.9680 2374.270
421.4501 2333.876
421.9323 2292.855
422.4144 2255.021
422.8965 2215.282
423.3786 2161.084
423.8607 2103.766
424.3428 2074.193
424.8250 2113.243
425.3071 2146.895
425.7892 2146.097
426.2713 2091.073
426.7534 2052.330
427.2355 2041.981
427.7177 2040.400
428.1998 2016.391
428.6819 1956.045
429.1640 1907.433
429.6461 1886.389
430.1282 1891.947
430.6104 1886.885
431.0925 1872.859
431.5746 1853.674
432.0567 1826.370
432.5388 1786.661
433.0209 1760.164
433.5031 1760.177
433.9852 1775.551
434.4673 1774.398
434.9494 1755.729
435.4315 1731.565
435.9136 1710.452
436.3958 1693.129
436.8779 1676.238
437.3600 1657.380
437.8421 1638.393
438.3242 1621.842
438.8063 1610.203
439.2885 1606.050
439.7706 1619.265
440.2527 1634.205
440.7348 1634.229
441.2169 1615.581
441.6990 1600.670
442.1812 1607.020
442.6633 1622.360
443.1454 1632.149
443.6275 1630.136
444.1096 1623.496
444.5917 1613.856
445.0739 1601.158
445.5560 1586.392
446.0381 1570.051
446.5202 1551.760
447.0023 1531.180
447.4844 1504.811
447.9666 1480.745
448.4487 1460.700
448.9308 1442.753
449.4129 1421.534
449.8950 1397.604
450.3771 1370.673
450.8592 1338.630
451.3413 1299.395
451.8235 1270.694
452.3056 1256.203
452.7877 1246.403
453.2698 1228.805
453.7519 1203.251
454.2340 1172.053
454.7162 1132.022
455.1983 1087.598
455.6804 1053.742
456.1625 1030.641
456.6446 1012.192
457.1267 995.0776
457.6089 978.5464
458.0910 958.3682
458.5731 931.8396
459.0552 905.2346
459.5373 889.3215
460.0194 880.8171
460.5016 868.3137
460.9837 845.9814
461.4658 816.5613
461.9479 780.8040
462.4300 737.7024
462.9121 695.3765
463.3943 658.1201
463.8764 624.4192
464.3585 592.9014
464.8406 573.3521
465.3227 545.9231
465.8048 497.8730
466.2870 429.2378
466.7691 373.5264
467.2512 338.5459
467.7333 314.2087
468.2154 294.4668
468.6975 282.3191
469.1797 269.9351
469.6618 257.1519
470.1439 244.0955
470.6260 230.4314
471.1081 213.7056
471.5902 202.1428
472.0724 202.2930
472.5545 215.4207
473.0366 216.3511
473.5187 201.7622
474.0008 185.1350
474.4829 182.4912
474.9651 192.3667
475.4472 204.3318
475.9293 220.9070
476.4114 235.2429
476.8935 227.2522
477.3756 201.0337
477.8578 180.0481
478.3399 188.3413
478.8220 210.9675
479.3041 226.4600
479.7862 231.6147
480.2683 226.9814
480.7505 201.9316
481.2326 167.9851
481.7147 148.3965
482.1968 169.1018
482.6789 192.1155
483.1610 194.5420
483.6432 171.7156
484.1253 158.7888
484.6074 180.6638
485.0895 209.2705
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1251.173 130.1821
1251.655 132.7250
1252.137 113.1772
1252.619 84.61279
1253.101 62.15405
1253.583 46.87524
1254.065 42.41772
1254.547 50.30676
1255.030 57.50061
1255.512 63.43054
1255.994 66.80652
1256.476 66.91125
1256.958 64.74805
1257.440 62.56848
1257.922 58.81335
1258.404 49.29138
1258.886 29.70630
1259.369 24.41980
1259.851 38.06348
1260.333 47.78748
1260.815 41.07812
1261.297 28.23169
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1262.261 18.54468
1262.743 14.20142
1263.226 6.831177
1263.708 4.086182
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1265.154 5.038940
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1266.118 1.122192
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1270.939 13.67163
1271.422 23.31616
1271.904 19.28198
1272.386 2.864746
1272.868 25.77515
1273.350 44.85779
1273.832 25.92798
1274.314 6.206787
1274.796 13.88574
1275.278 33.39917
1275.761 40.03064
1276.243 34.25269
1276.725 28.38647
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1282.028 22.64478
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1282.992 31.81165
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1286.367 20.66589
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1287.813 74.77734
1288.296 80.60693
1288.778 66.62512
1289.260 36.13989
1289.742 26.56641
1290.224 29.92346
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1292.635 34.09497
1293.117 33.82336
1293.599 24.69397
1294.081 30.27771
1294.563 55.17737
1295.045 55.60291
1295.527 54.29663
1296.010 48.51758
1296.492 38.93262
1296.974 29.65723
1297.456 12.39050
1297.938 0.0000000E+00
