#\#CIF_2.0 #------------------------------------------------------------------------------ #$Date: 2018-05-24 15:35:50 +0300 (Thu, 24 May 2018) $ #$Revision: 757 $ #$URL: svn://172.16.1.111/rod/cif/1/00/02/1000261.rod $ #------------------------------------------------------------------------------ # # This file is available in the Raman Open Database (ROD), # http://solsa.crystallography.net/rod/ # # All data on this site have been placed in the public domain by the # contributors. # data_1000261 loop_ _publ_author_name 'Yakubovich, O. V.' 'Massa, W.' 'Chukanov, N. V.' _publ_section_title ; Crystal structure of britvinite [Pb7(OH)3F(BO3)2(CO3)][Mg4.5(OH)3(Si5O14)]: A new layered silicate with an original type of silicon-oxygen networks Locality: Varmland, Sweden ; _journal_name_full 'Crystallography Reports' _journal_page_first 206 _journal_page_last 215 _journal_paper_doi 10.1134/S1063774508020077 _journal_volume 53 _journal_year 2008 _chemical_compound_source R070639 _chemical_formula_sum 'C2 B3.468 F2 Mg9 O58 Pb14.144 Si10.532' _chemical_name_mineral Britvinite _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 80.365 _cell_angle_beta 75.816 _cell_angle_gamma 59.870 _cell_length_a 9.3409 _cell_length_b 9.3579 _cell_length_c 18.8333 _cell_volume 1378.475 _exptl_crystal_density_diffrn 5.388 _cod_original_formula_sum 'Si10.532 Mg9 Pb14.144 C2 B3.468 O58 F2' _cod_database_code 9012668 _raman_determination_method experimental _raman_measurement_device.location 'Arizona University' _raman_measurement_device.company 'Thermo Scientific' _raman_measurement_device.model 'Nicolet Almega XR' _raman_measurement_device.optics_type microscope _raman_measurement_device.microscope_system dispersive _raman_measurement_device.microscope_objective_magnification 50 _raman_measurement_device.microscope_numerical_aperture 0.5 _raman_measurement_device.excitation_laser_type other _raman_measurement_device.excitation_laser_wavelength 532 _raman_measurement_device.configuration simple _raman_measurement_device.resolution 4 _raman_measurement_device.power_on_sample 15 _raman_measurement_device.direction_polarization unoriented _raman_measurement_device.spot_size 1 _raman_measurement_device.diffraction_grating 400 _raman_measurement.environment Air _raman_measurement.environment_details ; The sample was measured in air. ; _raman_measurement.temperature 300 _raman_measurement.pressure 100 _raman_measurement.background_subtraction no _raman_measurement.background_subtraction_details ; No background subtraction method was applied. ; _raman_measurement.baseline_correction no _raman_measurement.baseline_correction_details ; No baseline correction method was applied. ; _raman_measurement.integration_time 10 _rod_data_source.file R070639.rod _rod_data_source.block 3500000 _rod_database.code 1000261 loop_ _raman_complementary.id _raman_complementary.method 1 XRD loop_ _raman_measurement_device_calibration.id _raman_measurement_device_calibration.standard 1 neon_lamp loop_ _rod_related_entry.id _rod_related_entry.code _rod_related_entry.database _rod_related_entry.uri _rod_related_entry.description 1 9012668 COD http://www.crystallography.net/cod/9012668.html ; XRD analysis data was done. ; loop_ _raman_spectrum.raman_shift _raman_spectrum.intensity 156.2860 0.0000000E+00 156.7682 27.26758 157.2503 37.68359 157.7324 30.99219 158.2145 25.83008 158.6966 23.66797 159.1787 36.74414 159.6609 75.06055 160.1430 90.40430 160.6251 87.48633 161.1072 70.66211 161.5893 36.40039 162.0714 14.75195 162.5536 10.57617 163.0357 11.39258 163.5178 37.29883 163.9999 65.69727 164.4820 78.69141 164.9641 74.87109 165.4463 86.27930 165.9284 140.2012 166.4105 198.8633 166.8926 227.8418 167.3747 172.3633 167.8568 98.20898 168.3390 55.63672 168.8211 60.01562 169.3032 77.83594 169.7853 89.02148 170.2674 96.64844 170.7495 116.3232 171.2317 132.2129 171.7138 157.2422 172.1959 210.4766 172.6780 272.8340 173.1601 328.2979 173.6422 346.0889 174.1244 328.4727 174.6065 309.8418 175.0886 334.2910 175.5707 376.7959 176.0528 394.3145 176.5349 370.2471 177.0171 336.5928 177.4992 327.6699 177.9813 342.3213 178.4634 363.3984 178.9455 391.5859 179.4276 419.1523 179.9098 423.2363 180.3919 389.8711 180.8740 336.1543 181.3561 284.9688 181.8382 254.5176 182.3203 229.7969 182.8025 226.8281 183.2846 235.8936 183.7667 209.1221 184.2488 170.0576 184.7309 134.6650 185.2130 106.6367 185.6951 81.44922 186.1773 71.31836 186.6594 49.28418 187.1415 15.80371 187.6236 8.164063 188.1057 5.673828 188.5878 17.39746 189.0700 30.06543 189.5521 28.67773 190.0342 21.69238 190.5163 19.18262 190.9984 20.59082 191.4805 32.29492 191.9627 59.54883 192.4448 99.76270 192.9269 130.2344 193.4090 144.5391 193.8911 147.3799 194.3732 156.8164 194.8554 174.2979 195.3375 193.7754 195.8196 212.2197 196.3017 229.8330 196.7838 240.3096 197.2659 241.3301 197.7481 234.4961 198.2302 228.0107 198.7123 221.9443 199.1944 215.7637 199.6765 210.3809 200.1586 207.4756 200.6408 197.8135 201.1229 173.0527 201.6050 133.2627 202.0871 109.2822 202.5692 105.5234 203.0513 110.3184 203.5335 103.1816 204.0156 81.08594 204.4977 58.74805 204.9798 45.61035 205.4619 45.05859 205.9440 28.28125 206.4262 13.18652 206.9083 66.23828 207.3904 95.07812 207.8725 92.89258 208.3546 85.86523 208.8367 93.76660 209.3189 125.8018 209.8010 131.1016 210.2831 91.26172 210.7652 23.21289 211.2473 7.783203 211.7294 64.33887 212.2116 134.9365 212.6937 180.4414 213.1758 205.1797 213.6579 187.4287 214.1400 38.53223 214.6221 168.6787 215.1043 282.1943 215.5864 270.7266 216.0685 213.0459 216.5506 188.0938 217.0327 208.3760 217.5148 228.3428 217.9970 237.9766 218.4791 237.3398 218.9612 230.5420 219.4433 213.4502 219.9254 194.6289 220.4075 187.3906 220.8897 200.4004 221.3718 207.6582 221.8539 200.4307 222.3360 173.7471 222.8181 150.6514 223.3002 127.8379 223.7824 111.6729 224.2645 118.8203 224.7466 169.1953 225.2287 206.8525 225.7108 203.4541 226.1929 130.9990 226.6750 99.37109 227.1572 125.2793 227.6393 187.9033 228.1214 234.4170 228.6035 261.2754 229.0856 277.1772 229.5677 282.7769 230.0499 265.0767 230.5320 269.5947 231.0141 309.0586 231.4962 372.4263 231.9783 414.4722 232.4604 424.1440 232.9426 427.1919 233.4247 438.7393 233.9068 463.7324 234.3889 486.4775 234.8710 502.5381 235.3531 513.8589 235.8353 537.7617 236.3174 581.1699 236.7995 629.7515 237.2816 672.5015 237.7637 705.2456 238.2458 739.2134 238.7280 772.9048 239.2101 806.5527 239.6922 856.6260 240.1743 934.4771 240.6564 1017.653 241.1385 1084.835 241.6207 1128.863 242.1028 1169.734 242.5849 1210.976 243.0670 1253.239 243.5491 1291.570 244.0313 1324.412 244.5134 1354.868 244.9955 1385.662 245.4776 1414.422 245.9597 1450.139 246.4418 1498.028 246.9240 1560.215 247.4061 1616.685 247.8882 1663.363 248.3703 1706.687 248.8524 1756.075 249.3345 1816.376 249.8167 1876.219 250.2988 1931.738 250.7809 1980.642 251.2630 2032.674 251.7451 2091.829 252.2272 2151.077 252.7094 2198.133 253.1915 2233.673 253.6736 2255.562 254.1557 2263.865 254.6378 2260.312 255.1199 2235.283 255.6021 2178.581 256.0842 2105.655 256.5663 2051.562 257.0484 2024.063 257.5305 2001.722 258.0126 1977.411 258.4948 1954.517 258.9769 1917.348 259.4590 1856.043 259.9411 1783.824 260.4232 1737.793 260.9053 1732.127 261.3875 1726.911 261.8696 1697.220 262.3517 1630.530 262.8338 1583.638 263.3159 1568.479 263.7980 1572.897 264.2802 1554.303 264.7623 1500.006 265.2444 1442.334 265.7265 1398.994 266.2086 1371.183 266.6907 1356.797 267.1729 1356.102 267.6550 1368.472 268.1371 1393.131 268.6192 1440.414 269.1013 1477.789 269.5834 1478.388 270.0656 1434.171 270.5477 1384.578 271.0298 1334.737 271.5119 1287.489 271.9940 1249.313 272.4761 1213.274 272.9583 1180.532 273.4404 1153.191 273.9225 1132.284 274.4046 1111.420 274.8867 1091.353 275.3688 1070.884 275.8510 1038.112 276.3331 986.0679 276.8152 943.5996 277.2973 939.1724 277.7794 976.5420 278.2615 1016.478 278.7437 1054.828 279.2258 1089.804 279.7079 1109.371 280.1900 1109.108 280.6721 1109.947 281.1542 1135.840 281.6364 1188.431 282.1185 1229.255 282.6006 1240.908 283.0827 1236.588 283.5648 1280.736 284.0469 1382.138 284.5291 1484.188 285.0112 1520.029 285.4933 1492.495 285.9754 1489.313 286.4575 1539.249 286.9396 1627.823 287.4217 1709.637 287.9038 1784.980 288.3860 1849.851 288.8681 1889.984 289.3502 1909.229 289.8323 1947.391 290.3144 2025.263 290.7965 2126.167 291.2787 2201.243 291.7608 2249.019 292.2429 2289.695 292.7250 2338.216 293.2071 2395.295 293.6892 2465.690 294.1714 2560.114 294.6535 2664.665 295.1356 2742.655 295.6177 2793.064 296.0998 2849.187 296.5819 2949.374 297.0641 3083.638 297.5462 3217.613 298.0283 3350.469 298.5104 3471.049 298.9925 3553.948 299.4746 3598.922 299.9568 3636.983 300.4389 3694.102 300.9210 3765.305 301.4031 3840.408 301.8852 3921.471 302.3673 3999.904 302.8495 4062.756 303.3316 4109.725 303.8137 4154.112 304.2958 4212.120 304.7779 4273.672 305.2600 4320.052 305.7422 4346.170 306.2243 4353.186 306.7064 4335.907 307.1885 4294.958 307.6706 4254.028 308.1527 4237.378 308.6349 4228.819 309.1170 4206.853 309.5991 4157.642 310.0812 4095.688 310.5633 4035.288 311.0454 3975.816 311.5276 3900.779 312.0097 3782.807 312.4918 3650.177 312.9739 3532.396 313.4560 3450.516 313.9381 3377.250 314.4203 3303.303 314.9024 3227.458 315.3845 3145.976 315.8666 3048.226 316.3487 2944.702 316.8308 2846.979 317.3130 2740.343 317.7951 2660.830 318.2772 2646.430 318.7593 2687.388 319.2414 2692.131 319.7235 2592.839 320.2057 2465.810 320.6878 2370.439 321.1699 2353.455 321.6520 2335.102 322.1341 2297.799 322.6162 2243.163 323.0984 2184.564 323.5805 2115.773 324.0626 2047.045 324.5447 1985.880 325.0268 1951.441 325.5089 1904.453 325.9911 1823.428 326.4732 1715.604 326.9553 1644.881 327.4374 1654.362 327.9195 1675.679 328.4016 1668.845 328.8838 1603.049 329.3659 1547.277 329.8480 1510.375 330.3301 1488.703 330.8122 1458.166 331.2943 1406.815 331.7765 1358.084 332.2586 1326.431 332.7407 1327.628 333.2228 1317.553 333.7049 1292.850 334.1870 1255.028 334.6692 1208.462 335.1513 1148.061 335.6334 1086.538 336.1155 1031.627 336.5976 984.4238 337.0797 939.6904 337.5619 900.0552 338.0440 861.6255 338.5261 812.3496 339.0082 747.7529 339.4903 686.0000 339.9724 637.4541 340.4546 602.1040 340.9367 575.9600 341.4188 560.2905 341.9009 551.3501 342.3830 544.6201 342.8651 541.5781 343.3473 529.1069 343.8294 493.3506 344.3115 436.7974 344.7936 395.7290 345.2757 371.9106 345.7578 363.2451 346.2400 370.2397 346.7221 392.2295 347.2042 415.6172 347.6863 433.2471 348.1684 446.8018 348.6505 463.2446 349.1327 483.8921 349.6148 502.0918 350.0969 505.9360 350.5790 499.0288 351.0611 495.7275 351.5432 504.9458 352.0254 521.1479 352.5075 542.0312 352.9896 569.3125 353.4717 580.5034 353.9538 544.9316 354.4359 478.6978 354.9181 414.6411 355.4002 359.5615 355.8823 317.5171 356.3644 302.0962 356.8465 313.6624 357.3286 314.3823 357.8108 268.4014 358.2929 200.0391 358.7750 139.9753 359.2571 102.1267 359.7392 73.40234 360.2213 42.30396 360.7035 10.07251 361.1856 4.032227 361.6677 34.56519 362.1498 82.46387 362.6319 102.3323 363.1140 55.99683 363.5962 8.971436 364.0783 21.85400 364.5604 37.48682 365.0425 45.81079 365.5246 45.97192 366.0067 41.09961 366.4889 33.14941 366.9710 8.951172 367.4531 2.723389 367.9352 5.973877 368.4173 30.79834 368.8994 53.34497 369.3815 76.58228 369.8636 94.36621 370.3458 103.0244 370.8279 93.40063 371.3100 91.50439 371.7921 107.2771 372.2742 128.7317 372.7563 121.9453 373.2385 62.00073 373.7206 15.01465 374.2027 14.80981 374.6848 79.76562 375.1669 112.9683 375.6490 103.5750 376.1312 73.75562 376.6133 62.16675 377.0954 74.58008 377.5775 81.56104 378.0596 65.82349 378.5417 28.68994 379.0239 18.47705 379.5060 41.63672 379.9881 72.35156 380.4702 76.50293 380.9523 55.06177 381.4344 32.74219 381.9166 20.27441 382.3987 12.54517 382.8808 9.780518 383.3629 47.54858 383.8450 84.39209 384.3271 96.83325 384.8093 94.21606 385.2914 106.7695 385.7735 153.4429 386.2556 209.8733 386.7377 236.1050 387.2198 236.2468 387.7020 242.3765 388.1841 282.6108 388.6662 340.9622 389.1483 396.6038 389.6304 442.9448 390.1125 487.6082 390.5947 540.0161 391.0768 596.8955 391.5589 646.4663 392.0410 678.5918 392.5231 703.9270 393.0052 729.4402 393.4874 754.5737 393.9695 784.2271 394.4516 822.6584 394.9337 866.7136 395.4158 910.6357 395.8979 947.8911 396.3801 988.7290 396.8622 1041.145 397.3443 1113.647 397.8264 1168.692 398.3085 1179.316 398.7906 1176.997 399.2728 1199.903 399.7549 1273.818 400.2370 1345.305 400.7191 1404.580 401.2012 1451.015 401.6833 1495.648 402.1655 1539.196 402.6476 1579.960 403.1297 1615.498 403.6118 1642.627 404.0939 1672.515 404.5760 1704.937 405.0582 1741.188 405.5403 1792.388 406.0224 1865.112 406.5045 1932.429 406.9866 1972.806 407.4688 1984.787 407.9509 1994.622 408.4330 2002.465 408.9151 2012.940 409.3972 2039.735 409.8793 2082.770 410.3615 2123.249 410.8436 2145.449 411.3257 2156.170 411.8078 2181.874 412.2899 2227.839 412.7720 2273.189 413.2542 2284.605 413.7363 2273.153 414.2184 2271.943 414.7005 2305.470 415.1826 2352.960 415.6647 2393.103 416.1469 2424.927 416.6290 2447.046 417.1111 2458.649 417.5932 2459.629 418.0753 2449.821 418.5574 2411.838 419.0396 2378.161 419.5217 2373.924 420.0038 2393.624 420.4859 2400.730 420.9680 2374.270 421.4501 2333.876 421.9323 2292.855 422.4144 2255.021 422.8965 2215.282 423.3786 2161.084 423.8607 2103.766 424.3428 2074.193 424.8250 2113.243 425.3071 2146.895 425.7892 2146.097 426.2713 2091.073 426.7534 2052.330 427.2355 2041.981 427.7177 2040.400 428.1998 2016.391 428.6819 1956.045 429.1640 1907.433 429.6461 1886.389 430.1282 1891.947 430.6104 1886.885 431.0925 1872.859 431.5746 1853.674 432.0567 1826.370 432.5388 1786.661 433.0209 1760.164 433.5031 1760.177 433.9852 1775.551 434.4673 1774.398 434.9494 1755.729 435.4315 1731.565 435.9136 1710.452 436.3958 1693.129 436.8779 1676.238 437.3600 1657.380 437.8421 1638.393 438.3242 1621.842 438.8063 1610.203 439.2885 1606.050 439.7706 1619.265 440.2527 1634.205 440.7348 1634.229 441.2169 1615.581 441.6990 1600.670 442.1812 1607.020 442.6633 1622.360 443.1454 1632.149 443.6275 1630.136 444.1096 1623.496 444.5917 1613.856 445.0739 1601.158 445.5560 1586.392 446.0381 1570.051 446.5202 1551.760 447.0023 1531.180 447.4844 1504.811 447.9666 1480.745 448.4487 1460.700 448.9308 1442.753 449.4129 1421.534 449.8950 1397.604 450.3771 1370.673 450.8592 1338.630 451.3413 1299.395 451.8235 1270.694 452.3056 1256.203 452.7877 1246.403 453.2698 1228.805 453.7519 1203.251 454.2340 1172.053 454.7162 1132.022 455.1983 1087.598 455.6804 1053.742 456.1625 1030.641 456.6446 1012.192 457.1267 995.0776 457.6089 978.5464 458.0910 958.3682 458.5731 931.8396 459.0552 905.2346 459.5373 889.3215 460.0194 880.8171 460.5016 868.3137 460.9837 845.9814 461.4658 816.5613 461.9479 780.8040 462.4300 737.7024 462.9121 695.3765 463.3943 658.1201 463.8764 624.4192 464.3585 592.9014 464.8406 573.3521 465.3227 545.9231 465.8048 497.8730 466.2870 429.2378 466.7691 373.5264 467.2512 338.5459 467.7333 314.2087 468.2154 294.4668 468.6975 282.3191 469.1797 269.9351 469.6618 257.1519 470.1439 244.0955 470.6260 230.4314 471.1081 213.7056 471.5902 202.1428 472.0724 202.2930 472.5545 215.4207 473.0366 216.3511 473.5187 201.7622 474.0008 185.1350 474.4829 182.4912 474.9651 192.3667 475.4472 204.3318 475.9293 220.9070 476.4114 235.2429 476.8935 227.2522 477.3756 201.0337 477.8578 180.0481 478.3399 188.3413 478.8220 210.9675 479.3041 226.4600 479.7862 231.6147 480.2683 226.9814 480.7505 201.9316 481.2326 167.9851 481.7147 148.3965 482.1968 169.1018 482.6789 192.1155 483.1610 194.5420 483.6432 171.7156 484.1253 158.7888 484.6074 180.6638 485.0895 209.2705 485.5716 220.2046 486.0537 187.9854 486.5359 162.8293 487.0180 153.1758 487.5001 154.8940 487.9822 144.8159 488.4643 112.0287 488.9464 87.73486 489.4286 90.65588 489.9107 127.4344 490.3928 148.7622 490.8749 152.5391 491.3570 146.8208 491.8391 141.5833 492.3213 136.3872 492.8034 128.2258 493.2855 113.9695 493.7676 96.83862 494.2497 86.52002 494.7318 83.76233 495.2140 81.68176 495.6961 71.33765 496.1782 57.94934 496.6603 53.27466 497.1424 64.19080 497.6245 76.00000 498.1067 77.97339 498.5888 71.91223 499.0709 62.04517 499.5530 39.14600 500.0351 21.32727 500.5172 21.87830 500.9994 45.07544 501.4815 62.49243 501.9636 62.27881 502.4457 56.00793 502.9278 54.24060 503.4099 65.82520 503.8921 71.67603 504.3742 66.09302 504.8563 53.03235 505.3384 50.08667 505.8205 62.37610 506.3026 75.29907 506.7848 81.75720 507.2669 80.94250 507.7490 80.33728 508.2311 80.33008 508.7132 79.75500 509.1953 75.41760 509.6775 67.91003 510.1596 63.77478 510.6417 66.47046 511.1238 73.00415 511.6059 77.93213 512.0880 81.27600 512.5701 83.94629 513.0522 85.59875 513.5344 87.23425 514.0165 90.23499 514.4986 95.09888 514.9807 100.5050 515.4628 103.5773 515.9449 106.9600 516.4271 115.1449 516.9092 133.5764 517.3913 153.4009 517.8734 174.6588 518.3555 197.7084 518.8376 209.3184 519.3198 203.0996 519.8019 188.4581 520.2840 169.2069 520.7661 135.3507 521.2482 118.2738 521.7303 127.0598 522.2125 148.9432 522.6946 153.7266 523.1767 137.2053 523.6588 121.4388 524.1409 116.9762 524.6230 121.8427 525.1052 120.4227 525.5873 112.6381 526.0694 99.13025 526.5515 74.73413 527.0336 44.75659 527.5157 24.95410 527.9979 20.87769 528.4800 26.10327 528.9621 42.95776 529.4442 65.15759 529.9263 74.45667 530.4084 47.36694 530.8906 13.91772 531.3727 6.350830 531.8548 11.56384 532.3369 6.831299 532.8190 25.21790 533.3011 57.06116 533.7833 63.25549 534.2654 0.3969730 534.7475 39.59546 535.2296 39.56628 535.7117 10.29126 536.1938 11.20605 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